| 3-氨基-4-氯-N-(3-氯-2-甲基苯基)苯甲酰胺的合成 |
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| 引用本文： | 崔新义,于凯,张哲.3-氨基-4-氯-N-(3-氯-2-甲基苯基)苯甲酰胺的合成[J].染料与染色,2005,42(3):40-42. |
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| 作者姓名： | 崔新义 于凯 张哲 |
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| 作者单位： | 乐斯化学有限公司,乐清,325600;沈阳化工研究院,沈阳,110021 |
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| 摘 要： | 以3-硝基-4-氟苯甲酸、3-氟-2-甲基苯胺为原料,经3步合成3-氨基-4-氯-N-(3-氯-2-甲基苯基)苯甲酰胺,该工艺条件温和,操作简单,适合工业化生产。并利用红外、质谱、液相、元素分析对产品进行了鉴定。
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| 关 键 词： | 苯甲酰胺 3-硝基-4-氯苯甲酸 有机颜料 |
| 文章编号： | 1672-1179(2005)03-0040-3 |
| 修稿时间： | 2004年11月1日 |
Synthesis of 3-Amino-4-chloro-N-(3-chloro-2-methylphenyl)benzamide |
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| CUI Xin-yi,YU Kai,ZHANG Zhe.Synthesis of 3-Amino-4-chloro-N-(3-chloro-2-methylphenyl)benzamide[J].Ranliao yu Ranse,2005,42(3):40-42. |
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| Authors: | CUI Xin-yi YU Kai ZHANG Zhe |
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| Abstract: | 3-Amino-4-chloro-N-(3-chloro-2-methylphenyl)benzamide was synthesized by three steps reactions from 3-nitro-4-chlorobenzoic acid and 3-chloro-2-methylaniline. The product was easy obtained under moderate reaction conditions, and the process was suitable for industrial production,The product was characterized by IR, MS,HPLC and Element Analysis. |
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| Keywords: | benzamide 3-nitro-4-chlorobenzoic acid organic pigment |
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