| 30%三唑磷微乳剂的气相色谱法分析 |
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| 引用本文： | 伍翔,魏晓林,魏方林,朱国念,任新国,柏连阳.30%三唑磷微乳剂的气相色谱法分析[J].现代农药,2005,4(5):18-19. |
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| 作者姓名： | 伍翔 魏晓林 魏方林 朱国念 任新国 柏连阳 |
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| 作者单位： | 1. 湖南农业大学生物安全科技学院,长沙,410128
2. 浙江大学农药与环境毒理研究所,杭州,310029 |
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| 基金项目： | 国家“十五”科技攻关项目(2004BA308A25–5) |
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| 摘 要： | 采用气相色谱分析30%三唑磷微乳剂,选用1.5%SE–30为固定液,邻苯二甲酸二环己酯为内标,对有效成分进行分析和定量。三唑磷色谱峰与内标色谱峰的分离度为3.0。方法的相关系数为0.9996,标准偏差为0.1567,变异系数为0.52%,平均回收率为99.1%。
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| 关 键 词： | 三唑磷 微乳剂 气相色谱法 |
| 文章编号： | 1671-5284（2005）05-0018-02 |
| 收稿时间： | 2005-05-12 |
| 修稿时间： | 2005-08-03 |
Analysis of 30% Triazophos Micro-emulsion by Gas Chromatography |
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| WU Xiang,WEI Xiao-lin,WEI Fang-lin,ZHU Guo-nian,REN Xin-guo,BAI Lian-yang.Analysis of 30% Triazophos Micro-emulsion by Gas Chromatography[J].Modern Agrochemicals,2005,4(5):18-19. |
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| Authors: | WU Xiang WEI Xiao-lin WEI Fang-lin ZHU Guo-nian REN Xin-guo BAI Lian-yang |
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| Affiliation: | 1. Academy of Bio-safety and Scientist Technology, Hunan Agricultural University, Changsha 410007, China; 2. Institute of Pesticide and Environmenta Toxicology, Zhejiang University, Hangzhou 310029, China |
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| Abstract: | An GC method was developed for determination of 30% triazophos micro-emulsion with a 1.5% SE-30 packed glass column. Dicyclohexyl-o-phthalate was selected as internal standard. The resolution of peaks between triazophos and dicyclo- hexyl-o-phthalate was 3.0. Linear correlation, standard deviation, coefficient of variation and average recovery were 0.9996, 0.156 7, 0.52% and 99.1%, respectively. |
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| Keywords: | triazophos micro-emulsion GC |
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