| 3-戊胺的合成新方法 |
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| 引用本文： | 杨晓亮,阮班锋.3-戊胺的合成新方法[J].安徽化工,2014(2):17-18. |
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| 作者姓名： | 杨晓亮 阮班锋 |
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| 作者单位： | 安徽省烟草公司质量监督检测站,安徽合肥,230022;合肥工业大学医学工程学院,安徽合肥,230009 |
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| 摘 要： | 为了避免高温加氢对设备的要求以及高温下的副反应,通过在常压下多个平行反应进行对比,提出改进的合成3-戊胺的Leuckart反应体系,收到了良好的效果,反应条件温和,鲜有焦化氧化现象,单次转化率71.8%,循环反应收率92.2%。
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| 关 键 词： | 3-戊胺 Leuckart反应 合成 |
A New Synthethic Method of 3-Pentyl Amine |
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| YANG Xiao-liang,RUAN Ban-Feng.A New Synthethic Method of 3-Pentyl Amine[J].Anhui Chemical Industry,2014(2):17-18. |
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| Authors: | YANG Xiao-liang RUAN Ban-Feng |
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| Affiliation: | 1. Anhui Tobacco Quality Supervision and Test Station, Hefei 230022, China; 2. School of Medical Engineering, Hefei Universitry of Technology, Hefei 230009, China) |
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| Abstract: | In order to avoid the demand of equipment for hydrogenation and reduce the generation of byproducts in high temperature reported in the previous, a series of reactions designed for synthesis of 3-aminopentane were carried out and contrasted. Modified Leuckart Reaction system gave nice outcome when optimized system of toluene dehydration exhibited best result, with single cycle yield of 71.8%and total yield of 92.2%. |
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| Keywords: | 3-aminopentane Leuckart reaction synthesis |
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