| 端羟基聚丁二烯官能度及分布的测定 |
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| 引用本文： | 王波,赵传富,吴晓红,贺湘辉,王勇.端羟基聚丁二烯官能度及分布的测定[J].化学推进剂与高分子材料,2009,7(5):57-61. |
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| 作者姓名： | 王波 赵传富 吴晓红 贺湘辉 王勇 |
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| 作者单位： | 黎明化工研究院,河南洛阳,471000 |
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| 摘 要： | 用凝胶渗透色谱法（GPC）测定端羟基聚丁二烯（HTPB）官能度分布。将HTPB用3，5-二硝基苯甲酰氯在一定条件下进行衍生化反应，衍生化后的HTPB经GPC的示差／紫外（RI／UV）双检测器进行检测，所得的色谱图经数据处理，得到HTPB的官能度及其分布。
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| 关 键 词： | 端羟基聚丁二烯 官能度 相对分子质量 凝胶渗透色谱 |
Determination of Functionality and Its Distribution of Hydroxy-Terminated Polybutadiene |
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| WANG Bo,ZHAO Chuan-fu,WU Xiao-hong,HE Xiang-hui,WANG Yong.Determination of Functionality and Its Distribution of Hydroxy-Terminated Polybutadiene[J].Chemical Propellants & Polymeric Materials,2009,7(5):57-61. |
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| Authors: | WANG Bo ZHAO Chuan-fu WU Xiao-hong HE Xiang-hui WANG Yong |
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| Affiliation: | Liming Research Institute of Chemical Industry;Luoyang 471000;China |
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| Abstract: | The functionality distribution of hydroxy-terminated polybutadiene(HTPB) was determined by gel permeation chromatography(GPC). Derivative reaction of the HTPB was carried out by using 3,5-dinitrobenzoyl chloride under specific conditions. The derivation products of HTPB were determined by GPC with double detectors of refractive index/ultraviolet(RI/UV). The functionality and its distribution of HTPB were obtained via data processing of the obtained chromatogram. |
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| Keywords: | hydroxy-terminated polybutadiene functionality relative molecular mass gel permeation chromatogram |
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