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Synthesizing nano LaAlO3 powders via co-precipitation method
Affiliation:1. Chemistry Department, Faculty of Science, King Abdulaziz University, P.O. Box 80200, Jeddah, 21589, Saudi Arabia;2. Nanomaterials and Nanotechnology Department, Advanced Materials Division, Central Metallurgical R&D Institute (CMRDI), P.O. Box 87, Helwan, 11421, Cairo, Egypt;3. Department of Mechanical Engineering, Graduate School of Engineering, The University of Tokyo, 7 Chome-3-1 Hongō, Bunkyō-ku, Tōkyō-to, 113-0033, Tokyo, Japan;1. Postgraduate Program in Chemistry, Federal University of Rio Grande Do Norte – UFRN, 59078-970, Natal, RN, Brazil;2. Academic Department of Chemistry, Federal Institute of Education, Science and Technology of Maranhão – IFMA, 65030-005, São Luís, MA, Brazil;3. Postgraduate Program in Materials Science and Engineering, Federal University of Rio Grande Do Norte – UFRN, 59078-970, Natal, RN, Brazil;4. Postgraduate Program in Petroleum Science and Engineering, Federal University of Rio Grande Do Norte – UFRN, 59078-970, Natal, RN, Brazil;5. Agricultural School of Jundiaí, Federal University of Rio Grande Do Norte – UFRN, 59280-000, Macaíba, RN, Brazil;6. Postgraduate Program in Materials Engineering, Federal Institute of Education, Science and Technology of Maranhão – IFMA, 65030-005, São Luís, MA, Brazil;1. Institute of Low Temperature and Structure Research, Polish Academy of Sciences, ul. Okólna 2, P.O.Box 1410, 50-950, Wroclaw, Poland;2. Institute of Physics, University of Zielona Góra, ul. Prof. Szafrana 4a, 65-516, Zielona Góra, Poland
Abstract:Co-preparation method has been applied to synthesize nano LaAlO3 powders. By using La(NO3)3 and Al(NO3)3 as raw materials and keeping the pH≈9, the co-preparation process could be finished at room temperature. Pure LaAlO3 nano powders with a size of about 50 nm could be obtained after calcining at 700–800 °C. These nano LaAlO3 powders could be sintered at 1550 °C for 4 h, a high relative density of about 97% could be reached.
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