基于PSO的间歇生产鲁棒统计过程监控

间歇过程广泛应用于精细化工产品、生物化工产品等高附加值产品的制备.为提高间歇生产的可重复性,提高批次之间产品的一致性,多向主元分析法(MPCA)广泛应用于间歇生产过程的监控.针对MPCA统计监控模型容易受到建模数据中离群点影响的不足,提出了一种基于微粒群优化算法(PSO)的鲁棒MPCA分析方法,并进一步给出了相应鲁棒监控统计量的计算方法.对于链霉素发酵过程的监控表明,相对于普通MPCA,鲁棒MPCA在建模数据中存在离群点时仍能够给出正确的统计监控模型,从而有效减少了建模过程对数据的要求.     

一种基于改进MPCA的间歇过程监控与故障诊断方法

针对基于不同展开方式的多向主元分析(MPCA)方法在线应用时各自存在的缺陷,提出一种改进的基于变量展开的MPCA方法,实现间歇过程的在线监控与故障诊断。该方法采用随时间更新的主元协方差代替固定的主元协方差进行T²统计量的计算,充分考虑了主元得分向量的动态特性;同时引入主元显著相关变量残差统计量,避免SPE统计量的保守性,且该统计量能提供更详细的过程变化信息,对正常工况改变或过程故障引起的T²监控图变化有一定的识别能力;最后提出一种随时间变化的贡献图计算方法用于在线故障诊断。该方法和MPCA方法的监控性能在一个青霉素发酵仿真系统上进行了比较。仿真结果表明：该方法具有较好的监控性能,能及时检测出过程存在的故障,且具有一定的故障识别和诊断能力。     

基于多向核熵成分分析的微生物发酵过程多阶段划分及故障监测

针对多向核主元分析法(MKPCA)在监控动态非线性和多模态间歇生产过程故障的不足,提出一种基于物理信息熵的多阶段多向核熵成分分析(multiple sub-stage multi-way kernel entropy component analysis,MSMKECA)的新方法用于故障监控。该方法首先通过核映射将数据从低维空间映射到高维特征空间;其次在高维特征空间依据熵结构信息计算每个时刻数据矩阵的相似度指标进行阶段划分,将间歇过程划分为各稳定阶段和各过渡阶段,并在过渡阶段用时变的协方差代替固定协方差;最后在划分的阶段里分别建立模型进行间歇过程监测解决间歇过程的动态非线性和多阶段特性;将所提出的算法应用于青霉素发酵仿真系统的在线监测,验证了该方法的有效性。     

MPCA在间歇反应过程故障诊断中的应用

将多方向主元分析(MPCA)理论应用到一个实际的PVC间歇反应过程的性能监测与故障诊断中。由于间歇反应的特点,数据具有多维性,应用传统的主元分析将使过程的统计建模与故障诊断难以实现。MPCA可将间歇过程的多维数据沿时间轨迹分割,使得多批次的数据可以在各时间序列轨迹上建立相应的PCA模型,从而完成对间歇过程的实时监视及故障诊断。     

基于仿射传播聚类子集主元分析的间歇过程监测方法

针对间歇过程固有的多阶段特性,也为了克服传统阶段划分方法严格按照物理时刻顺序将采样点硬性分割而不能使其寻找数据特征最为相近的聚类中心的严重缺陷,提出基于仿射传播聚类(AP)的子集多向主元分析(subset-MPCA)监测新方法:采用全新的乱序聚类思想,将时间片矩阵打乱用AP进行无约束乱序聚类,使样本突破时间顺序的约束自由找寻与其特征最为相近的聚类中心,获得聚类子集,建立精确的子集MPCA监控模型。在线监控时,引入信息度传递实现实时采样点的阶段归属判断,解决阶段不等长批次的最佳模型选择问题。对青霉素仿真数据的实验表明,该方法较传统方法可有效降低故障的漏报和误报,有着更加可靠的监控性能。     

基于多阶段多向核熵成分分析的间歇过程故障检测方法

针对间歇过程的非线性、多阶段特性,提出一种基于多阶段多向核熵成分分析（multistage-MKECA,MsMKECA）的故障检测方法。针对间歇过程的多阶段特性,建立一种时序核熵主元关联度的矩阵相似性阶段划分方法,实现对间歇生产过程的多阶段划分;针对传统批次展开方式在线监控需要预估批次未来值的缺陷,进一步引入一种批次-变量三维数据展开方式建立每个阶段的MKECA非线性统计模型,实现对间歇过程的分阶段监控。最后对盘尼西林发酵过程开展仿真研究,结果表明所提方法能够比传统MKECA方法更为快速地进行故障检测。     

基于多阶段多向核熵成分分析的间歇过程故障检测方法

针对间歇过程的非线性、多阶段特性,提出一种基于多阶段多向核熵成分分析(multistage-MKECA,Ms MKECA)的故障检测方法。针对间歇过程的多阶段特性,建立一种时序核熵主元关联度的矩阵相似性阶段划分方法,实现对间歇生产过程的多阶段划分;针对传统批次展开方式在线监控需要预估批次未来值的缺陷,进一步引入一种批次-变量三维数据展开方式建立每个阶段的MKECA非线性统计模型,实现对间歇过程的分阶段监控。最后对盘尼西林发酵过程开展仿真研究,结果表明所提方法能够比传统MKECA方法更为快速地进行故障检测。     

基于MPCA-MDPLS的间歇过程的故障诊断

针对间歇过程的故障诊断问题,提出了一种新的混合模型方法——MPCA-MDPLS.这种方法包括两个模型：多向主元分析(MPCA)模型和多向判别部分最小二乘(MDPLS)模型.这两个模型的建模数据不仅包括正常工况的数据,而且还包含了各种已知故障数据.因此,MPCA模型具有检测未知故障的能力.给出了MDPLS模型故障诊断限,对经MPCA模型检测不是未知故障的故障做进一步诊断.如果故障是未知的,可以采取其他的方法来分析新的故障,并按不同类别存入到数据库中.当多次出现这种故障之后（一般≥5次）,把新的故障数据加入到建模数据中,并重新建立MPCA-MDPLS模型.通过对实际工业链霉素发酵过程数据的分析,表明了提出的算法是可行的、有效的,并具有识别未知新故障的能力.     

一种基于聚类方法的多阶段间歇过程监控方法

针对阶段不等长的多阶段间歇过程,提出了一种基于k-均值聚类方法的阶段分段策略,可以将不等长的阶段准确分类。首先,将间歇过程的三维训练数据按变量方向展开成二维矩阵,再通过k-均值聚类的方法按照相关性将数据聚成多类并运用主元分析（PCA）方法分别对每一类建立模型。在线监控时,通过计算样本与模型之间的相似系数以选择最合适的模型进行在线监控。此方法可以将不同批次在同一采样时刻的过程数据按照相关性分到多个阶段,更符合生产过程中常见的过程数据阶段不等长的情况。最后利用青霉素仿真验证了该方法的有效性。     

PDPSO优化多阶段AR-PCA间歇过程监测方法

针对间歇过程固有的多阶段特性和动态性,提出基于种群多样性的自适应惯性权重粒子群算法（PDPSO）优化的多阶段自回归主元分析（AR-PCA）间歇过程监测方法。该方法引入了PDPSO算法指导AP聚类偏向参数的选取,避免了传统方法依据聚类评价指标选取参考度时的盲目性。对PDPSO优化AP聚类的多阶段发酵过程的数据样本建立AR-PCA模型能够消除各阶段的动态性及变量之间的自相关和互相关影响。最后,对自回归（AR）模型的残差矩阵建立主成分分析（PCA）模型用于发酵过程监测。将该方法应用到青霉素发酵过程,并与传统方法进行对比,结果表明,该方法能够有效进行间歇过程阶段划分并降低故障的漏报和误报。     

自适应MPCA方法在链霉素过程监控中的应用

Multi-way principal component analysis (MPCA) had been successfully applied to monitoring the batch and semi-batch process in most chemical industry. An improved MPCA approach, step-by-step adaptive MPCA (SAMPCA), using the process variable trajectories to monitoring the batch process is presented in this paper. It does not need to estimate or fill in the unknown part of the process variable trajectory deviation from the current time until the end. The approach is based on a MPCA method that processes the data in a sequential and adaptive manner. The adaptive rate is easily controlled through a forgetting factor that controls the weight of past data in a summation. This algorithm is used to evaluate the industrial streptomycin fermentation process data and is compared with the traditional MPCA. The results show that the method is more advantageous than MPCA, especially when monitoring multi-stage batch process where the latent vector structure can change at several points during the batch.     

On-line batch process monitoring using a consecutively updated multiway principal component analysis model

Batch processes lie at the heart of many industries; hence the effective monitoring and control of batch processes is crucial to the production of high-quality materials. Multiway principal component analysis (MPCA) has been widely used for batch monitoring and has proved to be an effective method for monitoring many industrial batch processes. However, because MPCA is a fixed-model monitoring technique, it gives false alarms when it is used to monitor real processes whose normal operation involves slow changes. In this paper, we propose a simple on-line batch monitoring method that uses a consecutively updated MPCA model. The key to the proposed approach is that whenever a batch successfully remains within the bounds of normal operation, its batch data are added to the historical database of normal data and a new MPCA model is developed based on the revised database. The proposed method was applied to monitoring fed-batch penicillin production, and the results were compared with those obtained using conventional MPCA. The simulation results clearly show that the ability of the proposed method to adapt to new normal operating conditions eliminates the many false alarms generated by the fixed model and provides a reliable monitoring chart.     

在线自适应批次过程监视的双滑动窗口MPCA方法

Online monitoring of chemical process performance is extremely important to ensure the safety of a chemical plant and consistently high quality of products. Multivariate statistical process control has found wide applications in process performance analysis, monitoring and fault diagnosis using existing rich historical database. In this paper, we propose a simple and straight forward multivariate statistical modeling based on a moving window MPCA （multiway principal component analysis） model along the time and batch axis for adaptive monitoring the progress of batch processes in real-time. It is an extension to minimum window MPCA and traditional MPCA. The moving window MPCA along the batch axis can copy seamlessly with variable run length and does not need to estimate any deviations of the ongoing batch from the average trajectories. It replaces an invariant fixed-model monitoring approach with adaptive updating model data structure within batch-to-batch, which overcomes the changing operation condition and slows time-varying behaviors of industrial processes. The software based on moving window MPCA has been successfully applied to the industrial polymerization reactor of polyvinyl chloride （PVC） process in the Jinxi Chemical Company of China since 1999.     

基于Fisher子空间特征提取的间歇过程监控和故障诊断

1 INTRODUCTION Process monitoring and fault diagnosis are the most important tasks that determine the successful operation and the final product quality. In batch proc- ess, small changes in the operating conditions may impact the final product quality, which is often exam- ined off-line in a laboratory. If the quality variable does not satisfy a specified criterion, then it is not possible to examine the causes of fault and the time of its occurrence[1]. Therefore, early fault detection …     

基于分片化MPCA模型的多阶段批次过程阶段分析与阶段辨识方法(英文)

Multi-way principal component analysis (MPCA) is the most widely utilized multivariate statistical process control method for batch processes. Previous research on MPCA has commonly agreed that it is not a suitable method for multiphase batch process analysis. In this paper, abundant phase information is revealed by way of partitioning MPCA model, and a new phase identification method based on global dynamic information is proposed. The application to injection molding shows that it is a feasible and effective method for multiphase batch process knowledge understanding, phase division and process monitoring.     

Dynamic model-based batch process monitoring

An integrated framework consisting of a multivariate autoregressive (AR) model and multi-way principal component analysis (MPCA) is described for the monitoring of the performance of a batch process. After pre-processing the data, i.e., batch data unfolding, mean-centring and scaling, the data are then filtered using an AR model to remove the auto- and cross-correlation inherent within the pre-processed batch data. Model order is determined using Akaike information criterion and the model parameters are estimated through the application of partial least squares to attain a stable solution. MPCA is then applied to the residuals from the AR model. Three monitoring statistics are considered for the detection of the onset of process abnormalities in the batch process. The main advantage of the proposed approach is that it can monitor batch dynamics along the mean trajectory without the requirement to estimate future observed values. The proposed AR model-based approach is illustrated through its application to two polymerization processes. The case studies indicate that it gives better monitoring results in terms of sensitivity and time to fault detection than the approaches proposed by Nomikos and MacGregor [1994. Monitoring batch processes using multi-way principal components. A.I.Ch.E. Journal 40(8), 1361-1375] and Wold et al. [1998. Modelling and diagnostics of batch processes and analogous kinetic experiments. Chemometrics and Intelligent Laboratory Systems 44, 331-340].     

On-line batch process monitoring using dynamic PCA and dynamic PLS models

Producing value-added products of high-quality is the common objective in industries. This objective is more difficult to achieve in batch processes whose key quality measurements are not available on-line. In order to reduce the variations of the product quality, an on-line batch monitoring scheme is developed based on the multivariate statistical process control. It suggests using the past measured process variables without real-time quality measurement at the end of the batch run. The method, referred to as BDPCA and BDPLS, integrates the time-lagged windows of process dynamic behavior with the principal component analysis and partial least square respectively for on-line batch monitoring. Like traditional MPCA and MPLS approaches, the only information needed to set up the control chart is the historical data collected from the past successful batches. This leads to simple monitoring charts, easy tracking of the progress in each batch run and monitoring the occurrence of the observable upsets. BDPCA and BDPLS models only collect the previous data during the batch run without expensive computations to anticipate the future measurements. Three examples are used to investigate the potential application of the proposed method and make a comparison with some traditional on-line MPCA and MPLS algorithms.