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通过热压烧结技术,SiC、AlN和Y2O3粉末混合体在1920 ̄2050℃、Ar气氛下形成了致密的复相陶瓷。在室温下SiC-AlN-Y2O3复相材料的抗弯强度和断裂韧性分别达到600MPa和7MPa·m^1/2以上。运用XRD、SEM和TEM分析致密样品的断裂裂纹、形貌和组成。SiC-AlN-Y2O3复相陶瓷在1370℃氧化试验30h,其氧化产物为莫来石。 相似文献
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碳化硅陶瓷及其复合材料的热等静压烧结研究 总被引:2,自引:0,他引:2
本文通过采用热等静压(HIP)这一先进的烧结工艺,研究了Al2O3添加量对SiC陶瓷之显微结构与力学性能的影响。并成功地制备出Si3N4粒子以及SiC晶须补强的SiC基复合材料,结果表明:Al2O3是HIP烧结SiC陶瓷及其复合材料的有效添加剂,当添加3wt%Al2O3时,采用HIP烧结工艺在1850℃温度和200MPa压力下烧结1h就可获得密度分别高达97.3%、99.4%和97.0%的SiC的 相似文献
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共沉淀法制备Al_2O_3-YAG复相陶瓷及其显微结构研究 总被引:1,自引:0,他引:1
用共沉淀法制备了Al2O3-YAG复合粉体,YAG的结晶温度在1000℃左右.共沉淀法 制备的Al2O3-YAG复合粉体经1550℃热压烧结,获得致密烧结体,YAG的加入量对烧结温度 的影响不大. Al2O3-5vol%YAG复合材料的抗弯强度为604MPa,断裂韧性为5.0MPam1/2; Al2O3-25vol%YAG复合材料的抗弯强度为611MPa,断裂韧性为45MPam1/2.所有这些数据 都高于单相Al2O3陶瓷的力学性能,说明YAG的加入有利于A12O3陶瓷力学性能的提高. 通过显微结构观察发现:大的YAG颗粒位于Al2O3晶界上,小的YAG颗粒位于Al2O3晶粒 内.在 Al2O3-5vol%YAG复合材料中,许多小的白色区域存在于 Al2O3晶粒内,这可能和较低 的Y2O3含量有关. 相似文献
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研究了烧结助剂AIN 和B对Cf/SiC复合材料力学性能的影响。结果表明:B含量较低时(小于0.5w t% ),B的增加能有效地提高复合材料的抗弯强度与断裂韧性,继续增加B的用量至1w t% ,虽能大幅度提高复合材料的强度,但使复合材料的断裂韧性大大降低。AIN 与SiC高温反应形成固溶体,能起到强化和细化基体SiC晶粒以及改善SiC晶界结构的作用,但对复合材料内纤维与基体间界面的结合影响较小,因此与B的作用相比,AIN 对复合材料密度和力学性能的影响较小。烧结助剂为5w t% AIN-0.5w t% B,经1850℃和25MPa 热压烧结后的Cf/SiC复合材料具有较佳的综合力学性能,其抗弯强度与断裂韧性值分别为526.6MPa 和17.14MPa·m 1/2。 相似文献
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本文以SiC板粒、ZrOCl2-8H2O、AlCl3和Y(MO)3为原料,利用共沉淀和热压烧结工艺,制备SiC板粒/Y-TZP和(含Al2O3)SiC板粒/Y-TZP复合材料.测试了材料的室温和高温力学性能.研究了添加Al2O3对SiC板粒/Y-TZO复合材料的影响.结果表明,SiC板粒/Y-TZP复合材料与Y-TZP陶瓷相比,其室温强度和韧性出现明显下降,高温强度也没有改善;而在SiC板粒与Y-TZP复合的基础上,添加Al2O3可明显提高材料的强度和断裂韧性,同时,材料的高温强度也获得显著改善. 相似文献
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添加剂对热压钛酸铝陶瓷性能与结构的影响 总被引:2,自引:0,他引:2
MgO-Al2O3-SiO2、Al2O3-SiO2、Si3N4、SiC四种添加剂对热压钛酸铝陶瓷力学与热学性能的影响。结果表明:引入添加剂后钛酸铝陶瓷的抗弯强度得到极大的改善,同时,由于陶瓷结构的变化,其热膨胀系数也明显增加。X射线衍射结果表明:添加剂在热压条件下与钛酸铝陶瓷发生了反应并形成固溶体。 相似文献
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《International journal for numerical methods in engineering》2018,113(9):1488-1506
In this paper, we present a new method for inserting several triangulated surfaces into an existing tetrahedral mesh generated by the meccano method. The result is a conformal mesh where each inserted surface is approximated by a set of faces of the final tetrahedral mesh. First, the tetrahedral mesh is refined around the inserted surfaces to capture their geometric features. Second, each immersed surface is approximated by a set of faces from the tetrahedral mesh. Third, following a novel approach, the nodes of the approximated surfaces are mapped to the corresponding immersed surface. Fourth, we untangle and smooth the mesh by optimizing a regularized shape distortion measure for tetrahedral elements in which we move all the nodes of the mesh, restricting the movement of the edge and surface nodes along the corresponding entity they belong to. The refining process allows approximating the immersed surface for any initial meccano tetrahedral mesh. Moreover, the proposed projection method avoids computational expensive geometric projections. Finally, the applied simultaneous untangling and smoothing process delivers a high‐quality mesh and ensures that the immersed surfaces are interpolated. Several examples are presented to assess the properties of the proposed method. 相似文献
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Steffen Müller-Probandt 《材料科学与工程:中英文B版...》2018,(4):161-177
We associate a variety of innovations with the term "Industry 4.0". The pioneer of many 4.0 modifications forms the basisfor the trend towards the integrated di... 相似文献
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Janet Lang 《Materials and Manufacturing Processes》2017,32(7-8):857-866
ABSTRACTThe production of ferrous metal increased during the Roman Late Republican period, Principate and Empire. The direct bloomery process was used to extract the metal from its ores using slag-tapping and slag-pit furnaces. The fuel was charcoal and an air blast was introduced by bellows-operated tuyères. Iron formed as a bloom, often as a spongy mass of metal, which contained impurities from the smelting process, including unreacted ore, fuel, slag and fragments from the furnace walls, while the metal was often inhomogeneous with varied carbon contents. Blooms were either smithed directly into bars or ingots or they were broken up, which also allowed the removal of gross impurities and a selection of pieces with similar properties to be made. These could then be forge-welded together and formed into characteristically shaped ingots. Making steel in the furnace seems to have been achieved: it depended on the ore and the furnace and conditions within it. Surface carburization was also carried out. Iron and steel were used extensively in construction and for tools and weapons. Fire welding was often used to add pieces of steel to make the edges of tools and weapons, which could be heat-treated by quenching to harden them. 相似文献
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A four-ball tester was used to evaluate the anti-wear performance of three kinds of organomolybdemun compounds in the engine oils, i. e., molybdenum dialkyldithiophosphate (MoDDP), molybdenum dialkyldithiocarbamate ( MoDTC), and sulphur and phosphorus freeorganomolybdeum (Molybdate). The results indicate that a low concentration of MoDDP doesn' t improve the anti-wear properties of the commercial engine oils, but a high concentration of MoDDP can obviously improve the anti-wear properties and the load-carrying capacity of the engine oils. MoDTC doesn' t improve the antiwear properties of the engine oils, but worsens the anti-wear properties of the oils. Signifi can timprove ment of frictional and wear characteristics is obtained with Molybdate added in the commercial engine oils and the formulated oils. 相似文献
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Standards are the basis for production enterprises to organize production ex-factory inspection trade 《中国标准化(英文版)》2008,25(1):24-25
Standards are the basis for production enterprises to organize production, ex-factory inspection, trade (delivery) and technical exchanges, product certification, quality arbitration and supervision.…… 相似文献
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A flow calorimeter for enthalpy increment measurements on condensed gases is presented. A better knowledge of the properties of the liquefied natural gas is needed, and therefore a liquid loop has been designed for our flow calorimeter. The fluid loop in the calorimeter is designed in order to avoid the two-phase region, since two phases would give compositional disturbances in the measurements. The avoidance of the two-phase region is made possible by increasing the pressure of the test fluid after the measurement section, then heating the fluid at super-critical pressure past the critical point. Finally, the fluid is throttled to the low-pressure gas state at the inlet condition of the compressor that circulates the fluid. To perform the pressure increase, a new cryogenic pump has been designed. To evaluate the new equipment, measurements were taken on liquid ethane over the temperature range 146–256 K at pressure between 0.9 and 5.1 MPa. 相似文献
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S. K. Malhotra Paramanand Singh A. Thirunavukkarasu 《Materials and Manufacturing Processes》2006,21(7):652-657
Al2O3-ZrO2 nanocomposites were developed starting with the solgel process. Composite alumina-zirconia nanopowders were synthesized from metallorganic precursors (Aluminium secondary butoxide and zirconium Iso propoxide) using the solgel process. The parameters affecting the synthesis—solvent, concentration of precursor, R/H ratio (i.e., dilution of water in solvent)—were varied as also the temperature and pH. BET and TEM were used to measure nanosize. Diffuse reflectance spectroscopy and also qualitative optical absorption led to identical particle size estimate. The variation of process parameters was used to study the effect and interdependence of process parameters. Artificial Neural Networks was used to rigorously analyze the process. Although this led to confirmation of interdependence of parameters, the presence of a single overwhelming solvent variable was also established. Then the optimal process was used to synthesize more nanopowder. To produce bulk nanocomposite the nanopowders were sintered by varying the temperature and time period. The sintered lithoids were probed with a vickers hardness tester to measure elastic modulus, hardness, and fracture toughness. The results showed high elastic modulus, modest hardness, and very high fracture toughness. 相似文献
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On November 30, 2007, the China Association for Standardization (CAS) held a press conference at Beijing Diaoyutai State Guest House. Leaders from the China Household Electric Appliance Research Institute, the China Household Electric Appliance Association, and the China Consumers' Association attended and made speeches.…… 相似文献
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Friction Stir Processing Strategies for Uniform Distribution of Reinforcement in a Surface Composite
Vipin Sharma Yashpal Gupta Ujjwal Prakash 《Materials and Manufacturing Processes》2016,31(10):1384-1392
Friction stir processing (FSP) is an important technique for preparing surface composites. Fabricating defect-free surface composites with uniform particle distribution by FSP is a challenging task. In this study, silicon carbide particles reinforced AA5083 alloy surface composites was fabricated using different FSP strategies including variation in process parameters, dual-tool processing and tool offset overlapping. Material flow of the processed material with reinforcement particles demonstrated that the distribution of particles was influenced by the stirring action of the probe as well as the extrusion of the plasticized material due to the movement of the tool. Process parameters, particularly rotational speed, showed a dominant influence on the distribution of silicon carbide particles. 相似文献