2A12/SiCp陶瓷基复合材料伪半固态触变成形研究

在粉末冶金的基础上，结合半固态金属加工技术和21世纪陶瓷基复合材料成形的发展趋势，从而提出了陶瓷基复合材料伪半固态触变成形工艺，并且应用该工艺将2A12铝合金粉末和基体SiC颗粒按不同比例混合而得到的复合材料制备出卫星角框架制件。通过金相分析、拉伸等试验，证明了用该工艺成形陶瓷基复合材料是可行的。结果表明，该工艺成形的零件微观组织比较均匀，硬度比较高并且具有一定的塑性，为陶瓷复合材料以及高熔点材料在更多领域中的应用起到推进作用，同时为该工艺的进一步研究奠定了基础。     

Al/SiCp陶瓷基复合材料伪半固态触变成形

在粉末冶金的基础上，结合半固态金属加工技术和陶瓷成形的发展，提出陶瓷基复合材料伪半固态触变成形工艺并且以SiCp为基体，A[σ（Al）=30%]为增塑相，通过该工艺成形卫星角框架制件。结果表明，该工艺成形的零件微观组织比较均匀，HV可达6.43Gpa，应变ε约为0.5%，抗拉强度约为300 MPa，为陶瓷复合材料以及高熔点材料在更多领域中的应用起到推进作用。     

陶瓷基复合材料加工技术及其表面亚表面损伤机制研究进展

综述了陶瓷基复合材料的传统机械加工、超声辅助加工、激光加工、多能场复合加工等加工方式的研究进展,并简述了几种加工方式的优缺点.对陶瓷基复合材料的表面及亚表面损伤机制进行了总结和分析,包括材料表面亚表面损伤形式、材料表面亚表面理论及模型研究.提出了传统的陶瓷基复合材料加工技术需要进一步优化刀具材料、开发新的刀具结构、优化工艺参数等,以减少加工缺陷.研究了复合加工中材料去除率最大条件下的损伤容限条件、材料加工后的性能保持性等,同时探究了高效高质量的多能场复合加工新方法及其应用理论,以及研究探索了在复杂载荷及动载荷(如动态切削力、高温切削及超声动态冲击载荷)耦合作用下陶瓷基复合材料的内在损伤机理及演化问题.     

选区激光熔化3D打印钛基复合材料研究进展

选区激光熔化(SLM)3D打印技术是近年来快速发展的金属增材制造技术,因其可设计性、快速净成形复杂构件、高表面质量等优势,拥有广泛应用前景。基于SLM工艺制造的钛基复合材料通常可得到纳米级陶瓷增强相,获得比钛合金更优异的性能,成形构件力学性能优于铸件锻件水平。本文综述了近年来基于SLM工艺制备钛基复合材料的发展现状,以陶瓷增强体的选择为切入点,阐述其典型微观组织特征及演化规律,探讨其性能表现,分析其特有的强化机制,并在此基础上,对未来尚需解决的关键性学术问题和发展方向进行了展望。     

3D打印金属基金刚石复合材料的试验研究

传统方法制造金属基金刚石复合材料工具时,存在胎体对金刚石包镶强度不够、金刚石有效出刃高度小和难以制造具有特殊复杂结构的金刚石工具等问题,而3D打印技术为金属基金刚石复合材料的设计与制造提供了新的发展契机。本研究从金属材料、激光选区熔化（selective laser melting,SLM）成型工艺参数和金刚石参数3方面进行优选,开展SLM成型金属基复合材料的可行性试验,并进一步开展金属基金刚石复合材料的SLM成型试验。结果表明:采用SLM成型技术可提高金属基金刚石复合材料的性能。但同时,新技术的应用也还存在一些不足之处,需要针对性的深入研究。      

卫星角框件伪半固态触变成形及初步实验研究

在粉末冶金的基础上,结合半固态金属加工技术和21世纪陶瓷基复合材料成形的发展方向,提出陶瓷基复合材料伪半固态触变成形工艺。并且对Alp/SiCp不同体积分数混合得到的复合材料应用该工艺制备出卫星角框架制件。通过金相分析、拉伸等试验方法验证该工艺的可行性。结果表明,该工艺成形的零件微观组织比较均匀,硬度比较高。为陶瓷复合材料以及高熔点材料在更多领域中的应用起到推进作用,同时为该工艺的进一步的研究奠定了基础。     

高强度铝合金微等离子体电解氧化陶瓷质膜层影响因素

微等离子体电解氧化是在阳极氧化基础上发展起来的直接在轻合金表面原位生成γ-Al2 O3和α-Al2 O3陶瓷质膜的一项表面工程新技术.α-Al2 O3对陶瓷质膜层的性能起决定性作用,最大限度地促进α-Al2 O3的形成,是改善铝合金表面综合性能的关键.经过对国内近20个单位的调研,发现该技术在军工、航空、航天、机械等领域有着迫切的需求和广泛的应用前景,有望部分替代硬质氧化膜实现大规模生产.本文从基体材料、溶液特性及电参数三方面分析铝合金微等离子体氧化膜层的影响因素,重点分析基体合金元素对陶瓷质膜层的影响.指出该技术在高强度铝合金应用领域的发展方向并对其前景进行了展望.     

SiC泡沫陶瓷增强ZL205A铝合金复合材料的制备与性能研究

本实验通过挤压浸渗工艺成功制备了SiC泡沫陶瓷增强ZL205A铝合金复合材料,并研究了不同孔隙率的泡沫陶瓷增强相对复合材料性能的影响。通过微观结构分析,制备的复合材料两相间结合紧密,没有裂纹及其他缺陷产生。多孔陶瓷作为增强相可以有效地细化ZL205A合金的晶粒,多孔陶瓷孔隙率的降低,孔结构越小,合金晶粒越细小。对制备的复合材料进行力学性能测试,复合材料的硬度和抗弯强度最高能够达到127.6HV和415MPa。对制备的复合材料进行摩擦磨损测试,结果表明,连续陶瓷相的存在将铝基体严重的粘着磨损和剥落磨损转变为较轻的磨粒磨损,极大提升了复合材料的摩擦磨损性能,为其用于耐磨领域提供了理论依据。     

激光超声技术在先进复合材料无损检测中的应用研究

为实现航空航天先进复合材料的非接触、高精度检测,研究激光超声技术在复合材料无损检测中的应用。制备预埋人工缺陷的碳纤维树脂基复合材料和陶瓷基复合材料试样,利用自主研制的激光激励、激光探测的全光学激光超声无损检测系统进行试验研究,实现碳纤维复合材料层压结构模拟分层缺陷检测,层压复合材料紧固孔边沿分层检测,以及陶瓷基复合材料分层检测。研究结果表明:激光超声检测技术可以有效检出碳纤维树脂基复合材料内部直径2 mm以上分层型缺陷,可检出碳纤维复合材料紧固孔边沿的小尺寸分层,可表征C/SiC复合材料内部直径5 mm以上分层,在航空航天工程领域应用前景广阔。     

具有蜂窝型陶瓷芯板的复合材料的制备研究

研制了蜂窝型结构的陶瓷·芯板并采用普通铸渗工艺制备了具有蜂窝型陶瓷芯板复合层的高铬铸铁基复合材料.利用SEM对陶瓷芯板的表面形貌及成形原理进行了分析研究,测试了陶瓷芯板抗高温热冲击性能;通过金相显微镜、XRD等分析手段研究了复合材料界面结构及物相组成.蜂窝型陶瓷芯板在高温铁液的冲刷下完整保持了原有形貌,且基体与增强颗粒之间形成了良好的冶金结合.     

The first matrix cracking behavior of fiber-reinforced ceramic matrix composites

First matrix cracking stress in fiber reinforced ceramic composites is an important design parameter as it signifies the onset of mechanical damage and subsequent degradation of fiber and interface properties due to oxidation and corrosion. In this study, the influence of variation in the matrix crack length and fiber volume fraction on the first matrix cracking stress of ceramic matrix composites is investigated. To this end, zircon matrix composites uniaxially reinforced with silicon carbide fibers and monolithic zircon were fabricated. The monolithic and composite samples were microindented to create flaws of controlled size on the surface, and were then tested in 3-point flexure to obtain the matrix cracking stress. The results obtained from this study clearly indicated the non-steady state (short crack) and steady state (long crack) matrix cracking behaviors in ceramic matrix composites. The experimental results are compared with the theoretical results based on the fracture mechanics analyses published previously.     

Interfacial microstructure of 20% SO2/Al matrix composites reinforced with in situ formation ceramic phases

Al matrix composites reinforced with in situ ceramic phases by adding 20% SiO2 were fabricated by powder metallurgy process.The interfacial microstructure of the composites was studied by means of SEM and HREM.It was shown that the ceramic phases mainly composed of spinel MgAl2O4 are formed in situ in the original SiO2 particle and the size of small MgAl2O4 crystallites is about dozens of nanometers,which can adjacent to Al and Si.MgO could not found in original SiO2 particle but a little in matrix and may exist with Si,Mg2Si and Al.Si is mostly distributed in matrix and forms some segregation zones.The size of Mg2Si is about 50-100nm and can usually be seen in the matrix.     

MICROSTRUCTURE AND MECHANICAL PROPERTIES OF SiC W/BAS (BaAl 2Si 2O 8) GLASS CERAMIC COMPOSITE

１．ＩｎｔｒｏｄｕｃｔｉｏｎＢＡＳ（ＢａＯＡｌ２Ｏ３ＳｉＯ２）ｇｌａｓｓｃｅｒａｍｉｃｓｗｉｔｈｃｅｌｓｉａｎａｓｍａｉｎｃｒｙｓｔａｌｌｉｎｅｐｈａｓｅａｒｅｐｏｔｅｎｔｉａｌｍａｔｒｉｃｅｓｏｆｒｅｆｒａｃｔｏｒｙｆｉｂｅｒｏｒｗｈｉｓｋｅｒｒｅｉｎｆｏｒｃｅｄｃｏｍｐｏｓｉｔｅｓｄｕｅｔｏｔｈｅｈｉｇｈｍｅｌｔｉｎｇｐｏｉｎｔ（１７６０℃）ａｎｄｇｏｏｄｏｘｉｄａｔｉｏｎｒｅｓｉｓｔａｎｃｅｏｆｃｅｌｓｉａｎ．Ｃｅｌｓｉａｎｗｉｔｈｍｏｎｏｃｌｉｎｉｃｓｔｒｕｃｔｕｒｅｉｓｓｔａｂ…     

The abrasive wear properties of Al-Mg-Si3N4 metal matrix composites

One kind of three-dimensional network structure, reinforced aluminum magnesium matrix composites, has been prepared by pressure-assisted and vacuum-driven infiltration technology. The composites interpenetrated with ceramic have higher wear resistance than the metal matrix owing to their special topology structure. The reinforcement volume fraction has a large effect on abrasive wear. The wear rate decreases with the increase of the volume fraction of reinforcement and increases with the increase of sliding time and applied load. The wear mechanism of the composites (abrasive wear) differs greatly from the matrix alloy (adhesive wear).     

Fabrication and abrasive wear properties of metal matrix composites reinforced with three-dimensional network structure

1. Introduction Metal matrix composites (MMCs) have some re- inforcements such as particle, whisker, and fiber [1-3] as well as the three-dimensional network structure [4]. In recent years, metal matrix compos- ites reinforced with three-dimensional network structure (3DNRMMCs) have been paid consider- able attention, since they possess a rather high spe- cific strength, stiffness, and wear-resistance and can be attractive candidates for structural and functional materials [5]. There are s…     

Simulation and experimental study on thermal deep drawing of carbon fiber woven composites

Carbon fiber woven composites are composed of carbon fiber woven and resin matrix. To reduce the manufacture cost, thermal stamping, a new forming technology, was proposed and investigated to fabricate composite part. The mechanical properties of carbon fiber have great influence on the deformation of carbon fiber composites. In this study, shear angle–displacement curves and shear load–shear angle curves were obtained from picture frame test. Thermal deep drawing experiments and simulation were conducted, and the shear load–displacement curves under different forming temperatures and shear angle–displacement curves were obtained. The results show the compression and shear between fiber bundles are the main deformation mechanism of carbon fiber woven composite. The maximum shear angle for the composites in this study is 33°. In the drawing process, the forming temperature affects the drawing force, which drops rapidly with the increasing temperature. The suitable forming temperature in deep drawing of the carbon fiber woven composite is approximately 170 °C.     

Pseudo-semi-solid thixoforging of cup shell with Al/Al2O3

1 Introduction The composite has high strength and high hardness when some ductile metal is added into the ceramics, at the same time the fracture toughness can be improved availably[1?4]. We also know that the increase of toughness is because of the bri…     

SiC颗粒增强Al基复合材料成形极限的研究

采用损伤演变方程结合有限元模拟技术和实验结果 ,分析了 PRMMCs锻造过程中损伤场的分布及易出现裂纹的危险点 ,绘制了该材料的成形极限图 (FL D)。研究结果显示 ,该方法能为合理制定塑性加工工艺规范、控制成形产品质量提供理论依据。     

国外多孔基体氧化铝/氧化铝复合材料工程应用进展

氧化铝/氧化铝复合材料(Al2O3/Al2O3)是20世纪90年代兴起的一类连续陶瓷纤维增强陶瓷基复合材料,已经发展为与SiC/SiC、C/SiC等非氧化物陶瓷基复合材料并列的一类陶瓷基复合材料。与非氧化物陶瓷基复合材料相比,Al2O3/Al2O3具有长时抗氧化、高温耐腐蚀、低成本等独特优势,已经在航空发动机、地面燃气轮机等军民两用热结构材料领域展现出广阔的应用前景。本文从材料应用的角度出发,系统分析阐述了目前在Al2O3/Al2O3占主导地位的多孔基体Al2O3/Al2O3(P-Al2O3/Al2O3)的增韧机制、成型工艺和性能特点,重点归纳了国外近年来P-Al2O3/Al2O3的工程化应用进展及前景,最后指出了P-Al2O3/Al2O3存在的局限性并展望了未来发展方向,旨在为国内Al2O3/Al2O3体系发展提供借鉴和参考。     

Mechanical properties of aluminide matrix composites fabricated by reactive hot-pressing in several environments

The mechanical properties of Ni and Fe alminide matrix composites with low volume fraction of ceramic particles and fibers, fabricated by reactive hot-pressing, were evaluated. These composites reveal particular mechanical behaviors depending on characteristics of these matrix alloys. FeAl and Ni₃Al matrix composites with ceramic particles exhibit significant loading rate dependence of toughness due to the moisture induced environmental embrittlement at ambient temperatures. The ultimate strength of the composites with ceramic continuous fibers, which exhibit the multiple fracture of fibers prior to the matrix cracking, also depends on the environmental embrittlement. Although the ductility and toughness of these composites at ambient temperatures is improved by the B doping, those of Ni₃Al composites drastically decrease at intermediate temperatures due to dynamic oxygen embrittlement, deterioration of grain boundary cohesion and unique behavior of dislocations. On the other hand, NiAl composites are insensitive to the chemical effect of environmental factors because the matrix is inherently brittle. The alloy design for the matrix needs to be adequately applied to develop high performance intermetallic matrix composites.