焊接速度对 7A52 铝合金 FSW 组织及力学性能的影响

目的在保证搅拌速度一定时,针对8 mm厚的7A52铝合金,在不同焊接速度下采用搅拌摩擦焊(FSW)进行焊接试验,研究其焊接接头的显微组织及力学性能。方法利用搅拌摩擦焊机进行对接焊接,焊后制取金相试样观察焊接接头宏观形貌和显微组织,并测定其力学性能。结果7A52铝合金FSW焊接接头焊核区的面积随着焊接速度的增大而增大,当焊接速度为250mm/min时,焊接接头的焊核区面积最大,焊核区的显微组织都为细小的等轴晶,焊接接头横截面的焊核区呈明显"洋葱环"的形貌,而热力影响区的结构特征则呈现出了较高的塑性变形流线层。焊接接头显微硬度分布都呈现出"W"形变化,在焊接速度为150 mm/min时,焊接接头的平均抗拉强度能达到452 MPa,达到了母材抗拉强度的89%。结论通过对不同焊接速度下7A52铝合金FSW焊接接头的组织和性能进行研究,得到了不同焊接速度下焊接接头组织和力学性能。     

6082铝合金FSW焊接接头的组织与力学性能研究

通过拉伸、弯曲、硬度试验以及金相分析等对6082铝合金FSW焊接接头的力学性能与显微组织进行了研究.结果表明,以转速1500r/min、焊速600mm/min的参数焊接6082铝合金时,其接头具有较好的抗拉性能,板厚6mm和3mm焊接接头的抗拉强度分别为母材的77.23%和78.86%;正弯断裂位置集中在HAZ处,角度约90°,背弯断裂位置集中在焊缝中心,角度较小;硬度试验显示两侧热影响区处均软化;6082铝合金FSW焊接接头焊核区和轴肩影响区发生了动态再结晶,形成了细小的等轴晶组织,热机影响区组织发生了较大程度的变形;热影响区仅受热循环的作用,组织略有粗化.     

6005A铝合金挤压型材搅拌摩擦焊接头的疲劳性能

对6005A-T6铝合金挤压型材进行焊速为1000 mm/min的搅拌摩擦高焊速焊接,研究了对接面机械打磨对接头组织和力学性能的影响。结果表明,与生产中常用的焊前打磨处理相比,尽管对接面未机械打磨的接头焊核区的“S”线更明显,但是两种接头的硬度分布和拉伸性能相当,拉伸时都在最低硬度区即热影响区断裂。高周疲劳实验结果表明,两种接头的疲劳性能也基本相当,疲劳强度分别为105 MPa和110 MPa;在高应力幅下样品断裂于母材,在低应力幅下断裂于热影响区且出现两个裂纹源。两种接头的疲劳断口有裂纹源区、扩展区、最终断裂区,都呈现出典型疲劳断口特征。研究结果表明,焊前是否进行机械打磨对FSW接头的静态拉伸和动态疲劳性能没有明显的影响。     

2219铝合金TIG和FSW接头力学及疲劳性能

目的 研究钨极氩弧焊(TIG)和搅拌摩擦焊(FSW)对2219铝合金(母材)力学及疲劳性能的影响。方法 通过拉伸试验,得到了母材、TIG和FSW接头的抗拉强度和伸长率;通过疲劳性能试验测试了母材、TIG和FSW接头在不同应力下相应的疲劳寿命,根据疲劳试验结果绘制了其试样的S-N曲线;使用扫描电子显微镜观察并分析了疲劳断口的形貌特征。结果 未焊接的铝合金母材抗拉强度和伸长率最高,分别为506 MPa和15.92%;TIG接头抗拉强度和伸长率分别为330 MPa和7.65%,FSW接头抗拉强度和伸长率分别为310 MPa和8.74%。母材、TIG和FSW接头等3种疲劳试样在2×10⁶次循环下的疲劳强度分别为129、108、115 MPa,其疲劳断口均可分为裂纹源区、裂纹扩展区和瞬间断裂区,疲劳裂纹分别起始于试样表面的局部变形区、第二相夹杂物和“吻接”缺陷。疲劳裂纹扩展区的主要形貌为疲劳辉纹和二次裂纹,瞬间断裂区以脆性断裂为主。结论 TIG和FSW等2种焊接工艺均导致了2219铝合金的强度、塑韧性和疲劳性能降低,其接头表面的第二相夹杂物和“吻接”缺陷促进了疲劳裂纹的萌生。     

铝合金搅拌摩擦对接焊接头组织与性能研究

研究了5083铝合金搅拌摩擦焊(FSW)焊接接头组织与性能,采用金相显微镜观察焊接接头各区域的微观组织,并对接头显微硬度和力学性能进行了测定。结果表明,5083铝合金搅拌摩擦焊焊核组织为动态再结晶生成的细小组织,强化相均匀分布;热机影响区由于动态再结晶和焊接热循环的双重作用,组织变化较大,晶粒有一定程度的长大,强化相有所细化;热影响区仅仅受到热循环作用,使得晶粒粗化和强化相出现聚集现象。搅拌摩擦焊接接头中心硬度与母材基本相当,热机影响区和热影响区由于焊接热输入的原因,使得硬度有所降低。搅拌摩擦焊室温拉伸性能和冲击性能不低于母材的,其中拉伸试样均断裂于母材,焊核室温冲击值达到母材的1.5倍以上,热影响区冲击值与母材的相当。     

厚板铝合金搅拌摩擦焊匙孔补焊接头组织与性能

研究了35mm厚板铝合金搅拌摩擦焊匙孔补焊工艺,应用光学显微镜、扫描电镜、显微硬度仪及电子拉伸试验机等对接头的组织与性能进行了研究。结果表明,采用铝合金块材填充匙孔后进行FSW焊接,获得成型良好、表面光滑的焊缝;未加填充材料的匙孔位置,焊缝表面出现沟槽缺陷。FSW焊接一次接头的前进侧焊核区与热力影响区之间存在"吻接"缺陷;FSW焊接二次和三次接头的前进侧和后退侧过渡区均连接良好,二者组织无明显差别;FSW焊接一次和二次接头显微硬度分布呈W型,硬度最低值均出现在前进侧热影响区分别为56HV和60HV;采用搅拌头旋转速率为720r/min,焊接速率为180mm/min焊接工艺条件下,FSW焊接一次、二次和三次接头抗拉强度分别达到173、210和205MPa。     

转速对水下搅拌摩擦焊接7A04-T6铝合金组织与性能的影响

对7A04-T6铝合金板进行水下搅拌摩擦焊接(FSW),研究转速对水下FSW接头组织和力学性能的影响。结果表明:水下FSW接头的硬度最小值均位于热机械影响区。高转速条件下(950r/min)接头的硬度分布呈现"W"形,焊核区平均硬度值高于低转速条件下(475,600,750r/min)接头的硬度值。当焊速恒定为235mm/min,转速从475r/min提高到750r/min时,接头焊核区的析出相随转速的增大逐渐粗化,接头抗拉强度系数从89.71%降低到82.33%;当转速升高到950r/min时,析出相发生固溶时效,呈现细小弥散的分布特征,接头的强度系数提高到89.04%。接头具有较高的应变硬化能力,塑性伸长率较高。水下FSW接头的拉伸断口均呈现微孔聚合和解理混合断裂特征。     

6082-T6/7075-T6异种铝合金搅拌摩擦焊接接头的疲劳性能研究

为提高异种高强度铝合金焊接接头在复杂交变载荷作用下的服役可靠性,采用疲劳极限测量、疲劳断口形貌分析、金相分析和显微硬度测试等方法,研究了6 mm厚的6082-T6/7075-T6异种铝合金搅拌摩擦焊接接头疲劳性能及疲劳断裂的影响因素.结果 表明,1200 r/min、80 mm/min条件下,焊接接头疲劳极限为107.5 MPa.110 MPa疲劳载荷下,疲劳裂纹起源于前进侧(6082-T6)的焊核区与热机械影响区(TMAZ)交界位置的试样棱边尖角附近.这是由于焊接热循环导致β"相转变为β'相并粗化形成软化区、试样表面存在脆性第二相、2种材料在焊核区与热机械影响区交界处混合不均匀引起的应力集中,以及试样棱边尖角引起的应力集中等几种因素共同叠加作用所致.     

铝合金厚板静止轴肩搅拌摩擦焊接头组织及性能

采用8.5 mm厚度2A14-T4铝合金和自主研制搅拌工具进行静止轴肩搅拌摩擦焊（stationary shoulder friction stir welding,SSFSW）实验,探讨焊接工艺参数对接头组织和力学性能的影响规律。结果表明：只有在低转速工艺参数范围内（转速ω=400~600 r/min与焊接速率v=60~120 mm/min）可获得焊缝表面光滑、无缺陷厚板铝合金SSFSW焊接接头。SSFSW焊缝区主要由焊核区（NZ）组成,周围热力影响区（TMAZ）及热影响区（HAZ）宽度明显减小,焊核区与搅拌针形状类似且由两种不同尺寸细小等轴晶构成,前进侧NZ晶粒比后退侧NZ更为细小。接头显微硬度呈"W"状分布,NZ硬度值可达到母材硬度80%~90%,TMAZ与HAZ交界处存在软化区,硬度最低为母材硬度72%左右。在给定ω=500 r/min,v=140 mm/min焊接参数下,SSFSW接头抗拉强度可达到母材的88%,断裂位置多位于后退侧TMAZ与HAZ交界处软化区,具有韧性断裂特征。     

5083铝合金搅拌摩擦焊接头拉伸行为研究

目的 研究5083铝合金搅拌摩擦焊接（FSW）的组织、力学性能和拉伸应变,分析接头的拉伸行为。方法 采用数码相机、光学显微镜、电子扫描显微镜等表征分析方法,对焊缝的表面宏观成形、微观组织、断口形貌进行分析;利用拉伸机、三维数字动态散斑应变测量分析系统和显微维氏硬度计对接头的力学性能和拉伸应变进行测试。结果 不同焊接工艺参数下FSW接头的最低抗拉强度为305 MPa,断后延伸率达到了14%以上;焊核区拉伸应变沿板厚方向呈现上高下低和上宽下窄的不均匀梯度分布,发生了较大程度的变形强化,直到拉伸应力达到抗拉强度。断裂失效前300/120接头的最大拉伸应变在晶粒粗大的母材区,500/120和500/200接头的最大拉伸应变则位于晶粒尺寸差异较大的后退侧焊核区与热力影响区交界处。接头拉伸断口宏观上均为45°剪切韧性断裂,微观上均以韧窝韧性断裂为主,而高热输入500/120接头出现脆性断裂特征,其延伸率明显降低。结论 高热力耦合输入使铝合金FSW接头薄弱区发生转变,强韧性降低。     

Insertion of triangulated surfaces into a meccano tetrahedral discretization by means of mesh refinement and optimization procedures

In this paper, we present a new method for inserting several triangulated surfaces into an existing tetrahedral mesh generated by the meccano method. The result is a conformal mesh where each inserted surface is approximated by a set of faces of the final tetrahedral mesh. First, the tetrahedral mesh is refined around the inserted surfaces to capture their geometric features. Second, each immersed surface is approximated by a set of faces from the tetrahedral mesh. Third, following a novel approach, the nodes of the approximated surfaces are mapped to the corresponding immersed surface. Fourth, we untangle and smooth the mesh by optimizing a regularized shape distortion measure for tetrahedral elements in which we move all the nodes of the mesh, restricting the movement of the edge and surface nodes along the corresponding entity they belong to. The refining process allows approximating the immersed surface for any initial meccano tetrahedral mesh. Moreover, the proposed projection method avoids computational expensive geometric projections. Finally, the applied simultaneous untangling and smoothing process delivers a high‐quality mesh and ensures that the immersed surfaces are interpolated. Several examples are presented to assess the properties of the proposed method.     

From Industry 4.0 to Research 4.0. Development of High Performance Fibers in the Light of Digitization

We associate a variety of innovations with the term ＂Industry 4.0＂. The pioneer of many 4.0 modifications forms the basisfor the trend towards the integrated di...     

The Research of Anti-Wear Properties of Organomolybdenum Compounds in the Engine Oils

A four-ball tester was used to evaluate the anti-wear performance of three kinds of organomolybdemun compounds in the engine oils, i. e., molybdenum dialkyldithiophosphate (MoDDP), molybdenum dialkyldithiocarbamate ( MoDTC), and sulphur and phosphorus freeorganomolybdeum (Molybdate). The results indicate that a low concentration of MoDDP doesn' t improve the anti-wear properties of the commercial engine oils, but a high concentration of MoDDP can obviously improve the anti-wear properties and the load-carrying capacity of the engine oils. MoDTC doesn' t improve the antiwear properties of the engine oils, but worsens the anti-wear properties of the oils. Signifi can timprove ment of frictional and wear characteristics is obtained with Molybdate added in the commercial engine oils and the formulated oils.     

Roman iron and steel: A review

ABSTRACT

The production of ferrous metal increased during the Roman Late Republican period, Principate and Empire. The direct bloomery process was used to extract the metal from its ores using slag-tapping and slag-pit furnaces. The fuel was charcoal and an air blast was introduced by bellows-operated tuyères. Iron formed as a bloom, often as a spongy mass of metal, which contained impurities from the smelting process, including unreacted ore, fuel, slag and fragments from the furnace walls, while the metal was often inhomogeneous with varied carbon contents. Blooms were either smithed directly into bars or ingots or they were broken up, which also allowed the removal of gross impurities and a selection of pieces with similar properties to be made. These could then be forge-welded together and formed into characteristically shaped ingots. Making steel in the furnace seems to have been achieved: it depended on the ore and the furnace and conditions within it. Surface carburization was also carried out. Iron and steel were used extensively in construction and for tools and weapons. Fire welding was often used to add pieces of steel to make the edges of tools and weapons, which could be heat-treated by quenching to harden them.     

Certification Institutions Expected to Update and Transfer Information on Present Standards

Standards are the basis for production enterprises to organize production, ex-factory inspection, trade (delivery) and technical exchanges, product certification, quality arbitration and supervision.……     

Flow calorimeter for enthalpy increment measurements on condensed gases

A flow calorimeter for enthalpy increment measurements on condensed gases is presented. A better knowledge of the properties of the liquefied natural gas is needed, and therefore a liquid loop has been designed for our flow calorimeter. The fluid loop in the calorimeter is designed in order to avoid the two-phase region, since two phases would give compositional disturbances in the measurements. The avoidance of the two-phase region is made possible by increasing the pressure of the test fluid after the measurement section, then heating the fluid at super-critical pressure past the critical point. Finally, the fluid is throttled to the low-pressure gas state at the inlet condition of the compressor that circulates the fluid. To perform the pressure increase, a new cryogenic pump has been designed. To evaluate the new equipment, measurements were taken on liquid ethane over the temperature range 146–256 K at pressure between 0.9 and 5.1 MPa.     

Synthesis of Alumina-Zirconia Nanocomposites by Solgel Process

Al₂O₃-ZrO₂ nanocomposites were developed starting with the solgel process. Composite alumina-zirconia nanopowders were synthesized from metallorganic precursors (Aluminium secondary butoxide and zirconium Iso propoxide) using the solgel process. The parameters affecting the synthesis—solvent, concentration of precursor, R/H ratio (i.e., dilution of water in solvent)—were varied as also the temperature and pH. BET and TEM were used to measure nanosize. Diffuse reflectance spectroscopy and also qualitative optical absorption led to identical particle size estimate. The variation of process parameters was used to study the effect and interdependence of process parameters. Artificial Neural Networks was used to rigorously analyze the process. Although this led to confirmation of interdependence of parameters, the presence of a single overwhelming solvent variable was also established. Then the optimal process was used to synthesize more nanopowder. To produce bulk nanocomposite the nanopowders were sintered by varying the temperature and time period. The sintered lithoids were probed with a vickers hardness tester to measure elastic modulus, hardness, and fracture toughness. The results showed high elastic modulus, modest hardness, and very high fracture toughness.     

Certification Becomes Important for the I Quality; and Safety Supervision of the Chinese Liquor Sector

The end of 2007, over 200 unit products of more than 80 Chinese firms have passed the quality grade certification for liquor products. These products involve distilled spirits, beer, wine, yellow wine, fruit syrup wine and others, and cover over 80% of the national top-branded liquor products.……     

Deposition and Coating Properties on CVD Tungsten

Surface characterization and microstructure studies are performed on chemical vapor deposited (CVD) tungsten coating. There is about 2 μm thickness diffusion layer of tungsten in the molybdenum substrate. The thermal shock test shows tungsten coating has good adhesion with molybdenum substrate, but the elements of oxygen and carbon in the tungsten coating have the bad affection to the adhesion. The result of high-temperature diffusion experiment is the diffusion rate from molybdenum substrate to tungsten coating is faster.