27SiMn钢相变规律与强韧化热处理

通过研究连续冷却和等温相变规律,确定了27Si Mn钢贝氏体相变的条件,设计了其两段淬火+低温回火热处理工艺,从而获得贝氏体组织。结果表明:当过冷奥氏体以3~40℃/s连续冷却时,存在贝氏体相变,并且随着冷速增加,贝氏体量先逐渐增加然后逐渐减少;贝氏体等温相变温度区间为390~450℃。910℃加热30 min,油冷至(450±10)℃再空冷至室温分段淬火,然后250℃回火低温40 min,27Si Mn钢获得贝氏体组织,其抗拉强度890 MPa,屈服强度693 MPa,断后伸长率28.0%,断面收缩率67.0%,冲击功64 J,具有良好的强度、塑性和韧性匹配。     

3379BA1汽轮机叶片钢的热处理工艺优化

采用正交试验方法研究了3379BA1汽轮机叶片钢热处理工艺与力学性能之间的关系。结果表明:影响试验钢力学性能的因素先后顺序为回火温度、淬火温度、回火时间、淬火时间,得出了最优热处理工艺参数为1050 ℃淬火(保温60 min,油冷)后在700 ℃回火(保温120 min,空冷)。通过试验验证,经最优热处理工艺处理后试验钢可以满足各项性能要求,较工艺优化前冲击吸收能量平均值提升约10 J,屈强比达87.3%。     

热处理工艺对1.25Cr0.5MoSi钢组织和力学性能的影响

通过Gleeble-3800热模拟和热处理试验研究了热处理工艺对1.25Cr0.5Mo Si钢组织和性能的影响。结果表明:钢在950℃保温140 min后淬火水冷(冷却速率3~20℃/s),然后710℃保温245 min回火,空冷可获得回火贝氏体组织和优良的综合力学性能。钢板试样经模拟焊后热处理组织为回火贝氏体,钢板在690℃模拟焊后热处理0~32 h后,屈服强度达到400~470 MPa,抗拉强度560~600 MPa。当冲击温度低于-20℃时,冲击功急剧下降。随着模拟焊后热处理时间的延长,碳化物逐渐变粗大并沿晶界分布,导致钢板强度和低温冲击韧性大幅下降。     

高品质60Si2MnA弹簧钢的热处理工艺优化

进行了60Si2MnA弹簧钢的奥氏体粗化温度和热处理正交试验,模拟了余热淬火工艺,并确定了最佳热处理工艺.试验结果表明,采用950℃保温20min,随后冷至880℃出炉进行油淬,在400℃回火90min,其综合力学性能最佳,Rm=1810MPa,Rp0.2=1640MPa,A=6.9%,Z=29.1%,AK=19.2J,硬度54.3HRC,均显著超过高品质60Si2MnA弹簧钢的性能指标.将试验得出的余热淬火热处理优化工艺应用于铁道部I型60Si2MnA钢弹条的卷制余热淬火,其各项性能指标均能满足目前高速铁路用弹簧的技术要求.     

稀土改性超高强度耐磨钢的热处理工艺北大核心CSCD

以自主设计的稀土改性Si-Mn-B系贝氏体-马氏体复相耐磨钢为研究对象,利用正交试验研究了不同淬火温度、淬火保温时间、回火温度、回火时间对材料强度、冲击功的影响,以确定最佳热处理工艺,并利用XRD、OM、SEM、TEM方法对其最佳热处理工艺组织进行分析。结果表明:淬火温度对抗拉强度影响最大,回火温度对屈服强度的影响最大,淬火保温时间对冲击功的影响最大。最优热处理方案为:900℃×1.5 h油淬+300℃×3 h回火处理。按此方案热处理后有较好的强韧配合:抗拉强度为1903 MPa,屈服强度为1591 MPa,洛氏硬度为51.4 HRC,无缺口冲击功为267 J。采用彩色金相-化学腐蚀法,组织为下贝氏体(49.6%)、板条马氏体(43.9%)和少量残留奥氏体(6.5%)。     

37CrMnMo钢热处理工艺研究与优化

运用正交试验方法和回归分析研究了37Cr Mn Mo钢热处理工艺参数与力学性能的关系。结果表明,影响材料力学性能的主次因素顺序为:回火温度回火时间淬火保温时间淬火温度。通过回归分析得出材料力学性能和热处理工艺参数之间的关系,并获得最优工艺参数为淬火温度890℃,淬火保温时间50 min,回火温度580℃,回火时间60 min。经试验验证,优化后的热处理工艺使材料力学性能得到较大提高。回归值与实测值吻合较好。     

稀土改性超高强度耐磨钢的热处理工艺

以自主设计的稀土改性Si-Mn-B系贝氏体-马氏体复相耐磨钢为研究对象,利用正交试验研究了不同淬火温度、淬火保温时间、回火温度、回火时间对材料强度、冲击功的影响,以确定最佳热处理工艺,并利用XRD、OM、SEM、TEM方法对其最佳热处理工艺组织进行分析。结果表明:淬火温度对抗拉强度影响最大,回火温度对屈服强度的影响最大,淬火保温时间对冲击功的影响最大。最优热处理方案为:900℃×1.5 h油淬+300℃×3 h回火处理。按此方案热处理后有较好的强韧配合:抗拉强度为1903 MPa,屈服强度为1591 MPa,洛氏硬度为51.4 HRC,无缺口冲击功为267 J。采用彩色金相-化学腐蚀法,组织为下贝氏体(49.6%)、板条马氏体(43.9%)和少量残留奥氏体(6.5%)。     

回火工艺对钒氮超低碳贝氏体钢组织性能的影响

为了探索V-N微合金化在低碳贝氏体钢中的应用,利用扫描电镜(SEM)、透射电镜(TEM)、能谱仪(EDS)等实验方法,研究了不同回火温度对轧后保温与直接淬火两种工艺生产的钒氮超低碳贝氏体钢组织性能的影响.结果表明:随着回火温度的升高,屈服强度先升高后降低,直接淬火后600℃回火,材料的屈服强度为805 MPa,较轧态提高200 MPa,而直接淬火回火比轧后保温回火强度高65 MPa;回火后伸长率始终高于轧态.600℃回火时贝氏体基体上存在大量纳米级V(C,N)析出颗粒,对屈服强度的提高起了决定性作用;直接淬火钢回火后组织稳定性更高,析出物更加细小弥散.     

超超临界机组叶片用KT5331钢的热处理工艺

用热处理正交实验方法研究了淬火工艺与回火工艺对KT5331(10Cr11Co3W3Ni Mo VNb NB)钢力学性能的影响。结果表明,KT5331钢的最佳热处理工艺为1080℃保温60 min淬火,680℃保温2 h以上回火,组织为板条状的回火马氏体;淬火和回火参数中,回火温度是影响KT5331钢热处理后力学性能的最主要因素,淬火温度及回火温度对冲击功影响最为明显。淬火温度由1080℃升高至1120℃时奥氏体晶粒出现明显长大;随回火温度升高,材料屈服强度、抗拉强度和硬度明显降低,而冲击功显著升高。     

基于07MnNiMoDR钢热处理工艺窗口的热处理工艺

研究了07MnNiMoDR钢淬火和回火制度与晶粒尺寸和多边形铁素体含量的关系,建立了淬火保温时奥氏体尺寸窗口和回火保温时多边形铁素体含量窗口,确定了更为精准的热处理工艺。结果表明:奥氏体晶粒尺寸随淬火温度的升高、保温时间的延长而变大,均匀性存在最佳区间,合理的淬火制度为加热温度(940±10) ℃保温(80±10) min;随回火温度升高,约650 ℃出现多边形铁素体,其含量随回火温度的升高、保温时间的延长而增加,合理的回火制度为:加热温度(665±5) ℃、保温时间(165±15) min。优选后最佳热处理工艺为940 ℃×80 min淬火和660 ℃×180 min回火,最终性能测试结果表明:伸长率、冲击吸收能量和屈服强度相比国标分别提升了40.88%、206.25%和12.1%。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

THERMODYNAMICS STUDY ON THE DECOMPOSITION OF CHROMITE WITH KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

INFLUENCE OF HEAT TREATMENT ON DAMPING BEHAVIOUR OF THE MAGNESIUM WROUGHT ALLOY AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

A STUDY OF TEMPERATURE-DEPENDENT VALENCE BOND STRUCTURE OF TITANIUM

On the basis of energy and shape method for the determination of the valence bond (VB) structures of crystal, the valence bond structure of titanium is redetermined at room temperature and calculated in the whole temperature range of 0-1943K. The outer shell electronic distribution of Ti is e_c~(2.9907) · (s_c~(0.4980) d_c~(2.4927)) ef1.0093 in crystal. The temperature dependences of the VB structures of hcp and bcc phases are the same. The VB structures of hcp and bcc phases monotonically increase or decrease with the increase in temperature, but show discontinuous changes at the phase-transformation temperature 1155K.