超低碳Ti+Nb-IF钢组织与性能的研究

在实验室条件下研究了Ti+Nb-IF钢再结晶温度与时间以及退火制度对组织与性能的影响.实验结果表明:Ti+Nb-IF钢再结晶开始温度为680 ℃,在800 ℃退火温度下,再结晶完成时间为60 s.当退火温度为870 ℃时,综合力学性能最好,其抗拉强度为313 MPa,屈服强度为156 MPa,伸长率50.8%,n值为0.281,r值为2.07.退火织构特征表现为较强的γ纤维织构和较弱的α纤维织构,γ纤维织构主要为{111}<110>和{111}<112>,最强织构组分在{111}<112>.     

冷轧Ti-IF超深冲钢罩式退火机理及织构变化规律的研究

在480~750℃条件下,模拟罩式退火,利用光学显微镜、X射线衍射和金相显微硬度计研究了冷轧Ti-IF超深冲钢晶粒结构的变化,通过取向密度函数分析了再结晶过程织构演变规律。研究表明:冷轧Ti-IF超深冲钢的再结晶温度约为630℃,再结晶过程能够在660℃条件下2 h之内完成;冷轧后该钢主要有4种织构,分别是{001}〈110〉、{111}〈110〉、{111}〈112〉和{112}〈110〉;在退火再结晶过程中,{111}逐渐转变为γ-{111},当退火温度升至720℃时,{001}〈110〉和{112}〈110〉转变为纤维织构γ-{111},最终{111}〈110〉和{111}〈112〉成为主要织构类型。     

电场对08Al深冲钢板退火织构的影响

利用三维取向分析术(ODF)研究了电场对冷轧08Al深冲钢板退火过程中升温阶段和保温阶段退火织构的影响.结果表明,在退火的升温过程中,电场降低了α纤维织构的强度,提高了γ纤维织构的强度.在退火的保温过程中,当保温时间较短时,电场有利于降低再结晶α纤维织构的强度和提高再结晶γ纤维织构的强度;当保温时间较长时,电场对再结晶织构的影响不明显.电场促进α纤维织构向再结晶γ纤维织构转变以及γ纤维织构中的{111}<112>取向向{111}<110>取向的转变.     

IF钢罩式退火过程中再结晶组织与织构的演变

研究了IF钢(/%:0.005C、0.02Si、0.16Mn、0.011P、0.004S、0.042Als、0.061Ti、0.003 1 N)0.8 mm冷轧板在500～800℃退火时的再结晶组织及织构,采用X射线衍射技术结合微观组织观察分析了IF钢罩式退火过程中{111}再结晶织构形成机制和显微组织演变规律。结果表明,随退火温度的升高,再结晶数量逐渐增多,640℃为实验钢实际再结晶温度,同时{111}再结晶织构强度亦逐渐增大,{111}取向的晶粒主要在再结晶过程中形成,并在{111}取向晶粒长大过程中,γ纤维织构之间也发生相互转化,主要由{111}〈112〉织构转变为{111}〈110〉织构。     

取向硅钢27Q110初次再结晶退火对组织和织构的影响

通过检测取向硅钢27Q110一次冷轧板再结晶温度退火试验后的硬度及显微组织,确定取向硅钢脱碳退火(初次再结晶)阶段最佳退火温度为850℃。对冷轧硅钢厂取向硅钢27Q110脱碳退火后显微组织和织构进行检测和分析。结果表明,取向硅钢27Q110脱碳最佳退火温度为850℃,且主要织构γ在{111}<112>处最强     

冷轧压下率对无抑制剂取向硅钢初次再结晶退火的影响

对无抑制剂取向硅钢不同压下率下初次再结晶退火后的显微组织、宏观织构和微观织构进行了研究.结果表明,冷轧板织构主要为α取向线{001}＜110＞、{112}＜110＞和{111}＜110＞织构以及γ取向线{111}＜110＞织构.初次再结晶退火后,α取向线织构减弱,织构主要为γ取向线{111}＜112＞织构.随冷轧压下率的增加,冷轧和初次再结晶织构强度增加.当压下率为88％时,初次再结晶退火后 Goss 织构和{111}＜112＞织构强度最高,最有利于发生二次再结晶.EBSD 分析显示,Goss 取向晶粒大多与{111}＜112＞取向晶粒相邻.提高冷轧压下率,Goss取向晶粒和{111}＜112＞取向晶粒都增加,Goss 取向晶粒偏离理想取向角度减少.     

430不锈钢冷轧板高温退火过程中再结晶织构的定量分析

在750、800、825和850℃温度下,利用Gleeble1500热模拟试验机对430不锈钢冷轧薄板的等温退火过程进行了详细的实验研究,分析了退火过程中再结晶织构和组织的变化规律,并对关键织构体积分数的演变进行了定量分析.结果发现:随着退火过程的进行,α取向线上的织构强度逐渐减弱,而γ取向线上的织构强度则略有加强,并保持在较高的值;再结晶过程中,{111}和{112}<110>织构的体积分数逐渐降低,而{100}和随机取向晶粒的体积分数逐渐增加.定量分析表明,退火温度越低,完全再结晶后材料内部关键织构的体积分数越偏离冷轧态.最后,针对{111}、{112}<110>、{100}和随机取向织构的体积分数在再结晶过程中的演变规律,建立了JMAK型再结晶织构演变动力学模型.      

Ti、Nb对超低碳Cr18铁素体不锈钢冷轧板再结晶织构的影响

研究了添加Ti、Nb对超低碳Cr18铁素体不锈钢冷轧板再结晶织构的影响。试验结果表明,Nb单稳定化和Ti、Nb双稳定化的冷轧板试样在850℃下,随退火保温时间的延长,{111}面织构取向密度增加,而Ti单稳定的冷轧板在退火2min时{111}面织构取向密度值达到最大,然后随保温时间延长{111}面织构密度下降。Ti、Nb双稳定化的冷轧板经退火360s后得到最大的{111}<112>织构取向密度强度,Nb单稳定化Cr18不锈钢冷轧板再结晶织构{111}取向密度低于其它两种钢。     

冷轧压下率和再结晶退火温度对Ti-IF钢织构和成型性能的影响

采用背散射衍射技术(EBSD)研究了3.13 mm热轧板的冷轧压下量(65%~80%)和再结晶退火温度(660~780℃)对0.64~1.10 mm Ti-IF钢冷轧板(/%:0.02C、0.01Si、0.10Mn、0.013P、0.011S、0.064 Ti、0.028Al、0.002 0N)的织构和成型性能应变硬化指数(n)、塑性应变比(r)的影响。结果表明,Ti-IF钢冷轧板在冷轧压下率为75%时{111}织构含量最大,成型性能最佳;在740℃以下再结晶退火时材料{111}<110>织构含量高,高于740℃时材料{111}<112>织构含量高;在660~780℃再结晶退火随温度增高,材料{111}织构含量增加,成型性能提高。     

退火工艺对3.15 % Si冷轧无取向硅钢组织和织构的影响

试验研究了退火温度（850~950℃）和时间（5~18 min）对2.3 mm热轧硅钢板（/%:0.036C,3.15Si,0.21Mn,0.005P,0.007S,0.032Al）6道次轧制的0.35 mm冷轧板组织和织构的影响。结果表明,退火温度越高,晶粒平均尺寸越大,900℃5 min退火时平均晶粒尺寸41.39μm,试样织构主要集中在γ取向线上的{111}＜112＞;织构组分和{111}＜110＞;织构组分;900℃18 min退火时平均晶粒尺寸为48.08μm,试样的{111}面织构和{112}面织构密度都明显减弱,{001}面织构增强,磁性能较优。     

合金工具钢SKS51的动态再结晶行为

采用Gleeble-1500热模拟机单道次热压缩实验,研究了变形温度850～1 000℃和变形速率0.1～10s^-1条件下合金工具钢SKS51(/%:0.78C、0.20Si、0.40Mn、1.5Ni、0.30Cr)的动态再结晶行为。实验结果显示SKS51钢动态再结晶在高的变形温度和低的变形速率情况下更易发生,回归法得出动态再结晶的变形激活能和应力指数分别为336.79 kJ/mol和4.26,并在此基础上建立了动态再结晶峰值应变(ε_p)、稳态应变(ε_s)及临界应变(ε_c)模型。     

Recrystallization behavior of twin roll cast low carbon steel strip

The dynamic and static recrystallization behaviors of twin roll cast low carbon steel strip were investigated with an attempt to provide guiding deformation parameters for the on line hot rolling.In order to investigate dynamic recrystallization behavior,as cast strip was reheated and soaked with austenite grain size similar to the width level of the as cast columnar structure.Tensile test was used and the deformation temperature is in the range of 900℃to 1 100℃and strain rates are 0.01 s^-1,0.1 s^-1,1 s^-1.The activation energy and stress exponent were determined as 306kJ/mol and 4.69 respectively.The ratio of critical strain to the peak strain is 0.65,and that of critical stress to the peak stress is 0.92.The dependence of the peak strain on the initial grain size and Zener - Hollomon parameters Z isε_p =9.1×10^-4×D₀^0.48Z^0.13.The kinetics of the dynamic recrystallization and recrystallized grain size was predicted using models published.The as cast coarse austenite were dramatically refined after complete dynamic recrystallization.For static recrystallization,the tensile test was carried out on Gleeble -3500 thermo - mechanical simulator.The deformation temperature is in the range of 800℃to 1 200℃with strain rate 0.01 s^-1 to 1s^-1.The pre strain is fixed at 0.04 to 0.12 and the inter-hit delay time varies from 1 s to 3 000 s.The activation energy and Avrami exponent of static recrystallization were determined as 241 kJ/mol and 0.54 respectively.A kinetics model was proposed to describe the static recrystallization kinetics.The predicted results were in good agreement with the experimental results.     

两种高等级管线钢的奥氏体热变形行为

利用MMS300热模拟试验机在温度为850~1 150℃,应变速率为5 s-1,道次间隔时间为1~400 s的条件下进行了X80及X100管线钢双道次压缩变形试验,测定了不同间隔时间、不同变形温度条件下的软化率。研究结果表明：当道次间隔时间相同时,随变形温度升高,X80及X100管线钢静态再结晶分数均增加,再结晶进程加...     

Static Recrystallization Kinetics and Crystallographic Texture of Nb-Stabilized Ferritic Stainless Steel Based on Orientation Imaging Microscopy

In the present study, Nb-stabilized ferritic stainless steel was prepared with annealing (430-A) and without annealing (430-NA) annealing, and the microstructure of the resulting samples was examined. The steel was then subjected to cold rolling and isothermal annealing in order to analyze its recrystallization kinetics and texture evolution. Microstructural characterization was performed by scanning and transmission electron microscopies. Recrystallization kinetics were evaluated by measuring the microhardness of the samples, and analyzing their kernel average misorientation and grain orientation spread via electron backscatter diffraction. The Avrami exponent data revealed that one-dimensional grain growth occurred owing to the migration of high-angle grain boundaries. The mean activation energies for recrystallization for 430-NA and 430-A was found to be 365 and 419 kJ mol⁻¹, respectively. The recrystallization texture was influenced by oriented nucleation and selected growth mechanisms, as well as by the Nb carbonitride distribution and grain boundary energy. The recrystallized and growing grains with the {554}〈225〉 orientation showed a dimensional advantage over the other recrystallized components. The coincident site lattice boundaries were attributed to the progression of recrystallization since the CSL numeric fraction increased as the temperature increased. The {554}〈225〉 component was associated with the ∑19a boundary, which exerted a significant control on the selective growth during the recrystallization.

     

无取向电工钢的高温塑性变形流动应力

 以指导无取向电工钢热轧工艺为目的,采用Gleeble 1500热模拟试验机进行高温等温压缩,在应变速率为0.01~10s-1和变形温度500~1200℃条件下,对试样进行试验研究。结果表明：随着变形温度的升高,在回复与再结晶过程中发生α-Fe向γ-Fe相的?洌贾挛忍鞅溆αΤ氏帧耙斐！北浠２捎肁rrhenius关系模型,模型参数能很好的与试验结果相吻合。利用模型分别计算得500~800℃时,应力水平因子α=0.0390MPa-1,应力指数n=7.93,结构因子A=1.9×1018 s-1,热变形激活能Q=334.8kJ/mol;1050~1200℃时,应力水平因子α=0.1258MPa-1,应力指数n=5.29,结构因子A=1.0×1028 s-1,热变形激活能Q=769.9kJ/mol。     

Evolution of recrystallization and recrystallization texture in continuous-cast AA 3015 aluminum alloy

The evolution of recrystallization and recrystallization texture during annealing after cold rolling of a continuous-cast (CC) AA 3015 aluminum alloy with and without pretreatment was investigated in detail. It was found that the preheat treatment prior to cold rolling significantly affected the recrystallization kinetics, the shape and size of recrystallized grains, and the resulting texture of the CC AA 3015 aluminum alloy. In the case of the alloy without pretreatment, annealing at low temperatures resulted in coarse elongated recrystallized grains and a very strong P texture. As the annealing temperature increased, the size of the recrystallized grains dramatically decreased, the recrystallized grains became equiaxed, and the strength of the P texture decreased. The transition behavior could be attributed to the effect of Zener-particle pinning caused by concurrent precipitation. In contrast, the recrystallization texture of the CC AA 3015 aluminum alloy with pretreatment was characterized by a major cube component and a minor R component, and the annealing temperature did not affect the recrystallization texture. Moreover, concurrent precipitation retarded markedly the recrystallization of the CC AA 3015 aluminum alloy, decreased the Johnson-Mehl-Avrami-Kolmogorov (JMAK) exponent from 2.0 to 0.5, and increased the activation energy for recrystallization from 225 to 539 kJ/mol.     

Surface recrystallization of a single crystal nickel-base superalloy

The recrystallization behavior of a single crystal nickel-base superalloy was investigated by shot peening and subsequent annealing. Two kinds of recrystallization microstructures, which are intensively dependent on the annealing temperature, are shown in the nickel-base superalloy after shot peening and subsequent annealing. Surface recrystallized grains are obtained when the superalloy is anparticles occurs. Cellular recrystallization is observed after annealing at lower temperatures. Cellular structures induced by high diffusivity of the shot-peened alloy annealed at 1050℃ accords with the Johnson-Mehl-Avrami-Kolmogorov equation. The low Avrami exponent is caused by the inhomogeneous distribution of stored energy, the decreasing of stored energy during recovery, and the strong resistance of boundary migration yb γ' particles.     

Static Recrystallization Behavior of Twin Roll Cast Low-Carbon Steel Strip

 The static recrystallization kinetics of low-carbon steel cast strip was investigated by means of interrupted hot tensile tests. As-cast strip was reheated and soaked and its austenite grain size was similar to the width level of the as-cast columnar structure. The tests were carried out on Gleeble-3500 thermomechanical simulator. The deformation temperature is in the range of 800 to 1200 ℃ with strain rate of 001 to 1 s-1. The prestrain is fixed at 004 to 012, and the inter-hit delay time varies from 1 to 3000 s. Effect of deformation conditions and initial microstructure on static recrystallization behavior was investigated. The activation energy (Qsrx) and Avrami exponent (n) of static recrystallization were determined to have 241 kJ/mol and 054 respectively by linear regression of the experimental results. A kinetics model was proposed to describe the static recrystallization kinetics in low-carbon steel cast strip. The predicted softening fractions are in good agreement with the experimental results, indicating that the proposed equations can give an accurate estimate of the softening behaviors for the low-carbon steel cast strip.     

Effect of Strain-Induced Precipitation on the Recrystallization Kinetics in a Model Alloy

The effects of Nb addition on the recrystallization kinetics and the recrystallized grain size distribution after cold deformation were investigated by using Fe-30Ni and Fe-30Ni-0.044 wt pct Nb steel with comparable starting grain size distributions. The samples were deformed to 0.3 strain at room temperature followed by annealing at 950 °C to 850 °C for various times; the microstructural evolution and the grain size distribution of non- and fully recrystallized samples were characterized, along with the strain-induced precipitates (SIPs) and their size and volume fraction evolution. It was found that Nb addition has little effect on recrystallized grain size distribution, whereas Nb precipitation kinetics (SIP size and number density) affects the recrystallization Avrami exponent depending on the annealing temperature. Faster precipitation coarsening rates at high temperature (950 °C to 900 °C) led to slower recrystallization kinetics but no change on Avrami exponent, despite precipitation occurring before recrystallization. Whereas a slower precipitation coarsening rate at 850 °C gave fine-sized strain-induced precipitates that were effective in reducing the recrystallization Avrami exponent after 50 pct of recrystallization. Both solute drag and precipitation pinning effects have been added onto the JMAK model to account the effect of Nb content on recrystallization Avrami exponent for samples with large grain size distributions.