Bainite Transformation of Low-carbon and Boron-containing Steel under Continuous Cooling

The effects of deformation temperature and strain on bainite transformation of low carbon steel and boroncontaining steel were investigated under continuous cooling conditions by means of dilatometric measurement and microstructure observation.The results show that with decreasing the deformation temperature from 1 000to 800 ℃and increasing strains,bainite start temperature for boron-containing low carbon steel increases,whereas it decreases for low carbon steel under the same condition.The bainite microstructures are easily obtained for boron-containing steel deformed at different temperatures and different strains compared with plain low carbon steel.With increasing the continuous cooling rate,the bainite start temperature under deformed condition is about 20 ℃ higher than that under undeformed condition for boron-containing steel,but it changes slightly when the cooling rate is 20℃/s or more.     

高温变形和过冷度对中碳钢贝氏体相变的影响

摘要：一般认为低温相变提高贝氏体相变量,而高温奥氏体预变形抑制贝氏体相变。通过热模拟实验膨胀曲线、扫描电镜微观组织和X射线衍射图谱等,研究了高温奥氏体预变形和过冷度对贝氏体相变和组织的综合影响。结果表明,高温变形对贝氏体相变的阻碍程度取决于相变温度,随着相变温度的升高,对贝氏体相变的阻碍作用逐渐减小。此外,无变形试样中,相变温度最低（300℃）时的贝氏体相变初始速率最大,而对于变形试样,相变温度最高（450℃）时贝氏体相变初始速率最大。同时,在同一相变温度下,由于高温变形导致过冷奥氏体的机械稳定化,变形试样中的马氏体/奥氏体组织比无变形试样粗大,且变形试样中残余奥氏体含量增加。     

变形参数对低碳微合金钢奥氏体相变规律的影响

利用Gleeble-3800热/力模拟试验机,研究了1种低碳微合金钢的形变奥氏体连续冷却转变行为以及终轧温度、终轧变形量对相变组织形态的影响。结果表明,实验钢在研究的冷速范围内均可得到一定量的贝氏体组织。随着冷速的增加,冷速达到50℃/s时,贝氏体组织由粒状贝氏体逐渐过渡到板条状贝氏体。在较快的冷速下,随终轧温度的降低或终轧变形量的减小,贝氏体转变开始与结束温度均降低,获得的贝氏体具有不同的组织形态。     

低于Ms温度变形对等温贝氏体相变动力学和组织的影响

摘要：变形和等温热处理是高强贝氏体钢主要生产工艺,已有研究表明低于马氏体相变起始温度（Ms）的等温热处理可以促进贝氏体相变动力学,低温奥氏体预变形也可以加速贝氏体相变。研究了低于Ms温度变形对后续等温贝氏体相变动力学和组织的影响,结果表明,并未出现预想的加速相变叠加效应,反而,变形温度低于Ms温度时,贝氏体相变动力学减弱,等温贝氏体相变孕育期延长。低于Ms温度等温相变时,贝氏体铁素体与母相奥氏体位向关系接近K-S关系,变形试样虽然获得了一部分先马氏体,且能提高贝氏体形核率,但并非所有的胚核都能发生长大,变形改变母相奥氏体取向,使贝氏体原本的位向关系遭受破坏,导致有效形核率降低。     

不同硼含量微合金钢的连续冷却相变行为

 利用热模拟试验技术对实验室制备的含硼微合金钢连续冷却转变形为进行了试验研究,利用光学显微镜研究冷却速度、变形对试验钢显微组织的影响,探讨了硼对转变行为的影响规律。结果表明：适量硼延缓多边形铁素体生成,有利于获得贝氏体组织;无硼及wB=00020%时,分别在1~25及05~25℃/s的冷速都能得到贝氏体组织;wB=00030%时,冷速在2℃/s 以上能得到贝氏体组织;与未变形相比,变形导致试验钢贝氏体冷速区间变窄。在同一冷速下,随硼含量增加贝氏体开始转变温度先降低再升高,显微硬度随硼含量增加先增加而后降低。     

奥氏体形变对50CrV4钢相变行为的影响

利用Thermecmastor-Z型热模拟试验机,结合金相显微镜(OM)、扫描电镜(SEM)、维氏硬度计等,系统研究了奥氏体区变形对50CrV4钢连续冷却相变和等温相变规律的影响。建立了试验钢动态CCT曲线。研究结果表明,奥氏体变形能促进连续冷却转变过程中铁素体-珠光体、贝氏体转变,但亦可提高奥氏体的机械稳定性,进而抑制马氏体转变,Ms点由331.6℃(奥氏体未变形)降低至291℃(950℃下变形50%+890℃下变形50%,变形速率均为5s-1,变形后冷速为20℃/s)。当轧后冷速小于0.5℃/s时,试验钢中可获得铁素体+珠光体组织。此外,在研究不同变形量对试验钢等温相变规律影响时发现,650℃等温时,试验钢中发生铁素体-珠光体相变。随着变形量的增加(由30%增加至50%),其等温相变动力学加快(相变完成时间由197.6s减小至136.5s),铁素体体晶粒尺寸、珠光体片层间距减小,硬度增加。     

The Effect of Pre-Deformation at Elevated Temperatures on the Microstructure and Hardness of Boron Steel 22MnB5

To investigate the effects of the pre-deformation and deformation temperature on the microstructure and hardness of boron steel 22MnB5,isothermal tensile tests were carried out on the Gleeble 3800 system when the temperatures are 700℃,750℃,800℃,respectively.Three specimens were employed to obtain different deformation levels at each temperature.The cooling rate before and after deformation was 30℃/s.Then the microstructures of the specimens were observed and the harness of each specimen was measured.The results show the martensitic fraction decreases and the ferrite fraction increases with decreasing the deformation temperature or increasing the deformation level.The specimens deformed at higher temperature have greater hardness.The hot plastic deformation of austenite shortens the incubation period of ferrite transformation and accelerates the transformation rate.In addition,the isothermally holding time is longer in the case of a larger deformation amount,more austenite will transform to ferrite.Especially,the specimen deformed at 700℃ and with large deformation has almost full massive ferrite microstructure with larger size.     

贝氏体形态对细晶铁素体/贝氏体双相钢室温力学性能的影响

基于过冷奥氏体动态相变的思想,通过两道次压缩变形结合控制冷却的热模拟轧制工艺,获得不同贝氏体含量及形态的细晶铁素体贝氏体双相钢。通过显微组织观察及力学性能测试,考察了第二相贝氏体特征对双相钢室温拉伸变形行为的影响。研究结果表明,形变后快速冷却可获得无碳板条状贝氏体,较慢的冷速或在贝氏体转变区保温处理可获得粒状贝氏体。贝氏体体积分数大于20%左右的细晶铁素体/贝氏体双相钢具有低的屈服强度,高的抗拉强度,高的伸长率,低屈强比以及连续屈服特性。屈服强度既与铁素体晶粒尺寸相关,也与贝氏体形态和数量相关。板条贝氏体引起的屈服强度提高大于粒状贝氏体,粒状贝氏体具有比板条贝氏体更好的塑性。     

含Mo低碳贝氏体钢形变奥氏体连续冷却相变规律研究

在Gleeble-1500热力模拟试验机上,利用热膨胀法测定了两种含Mo低碳贝氏体钢在850℃变形30%后再以不同冷却速度冷却到室温的连续冷却相变曲线(CCT曲线),在Axiovert 200 MAT光学显微镜下检测冷却后的组织.结果表明,奥氏体化的低碳钢低速冷却后的组织主要由粗大的铁素体和少量颗粒状珠光体组成;提高连...     

Computer Model of Phase Transformation From Hot-Deformed Austenite in Niobium Microalloyed Steels

Based on thermodynamics and kinetics, a new mathematical model was developed to calculate the CCT diagrams and the transformation kinetics in low carbon niobium steels, in which the effect of deformation on the degree of supercooling was taken into account. The undercooling caused by deformation is the major reason for the increase of the starting transition temperature during continuous cooling. The critical cooling rate of bainite formation is within 2--5 ℃s for the studied niobium steels and deformation is suitable for the occurrence of pearlite. The ferrite volume fraction increases with the increase of the austenite boundary area, and decreases with the increase of the cooling rate. The calculated CCT diagrams and the volume fraction of each phase are in good agreement with the measurements.     

中碳Cr-Mo-V钢连续冷却时的组织转变规律

采用Formastor-FⅡ全自动相变仪实现不同冷却速度,利用金相显微镜、扫描电子显微镜和透射电子显微镜,研究了45CrMoV钢在不同冷却速度下的组织转变规律以及回火温度对组织的影响。结果表明,随着冷却速度的变慢,45CrMoV钢的组织由马氏体变为马氏体、先共析铁素体、下贝氏体和粒状贝氏体的混合物。冷却速度进一步变慢,先共析铁素体数量增多,下贝氏体和粒状贝氏体总量减少,材料硬度不断下降;45CrMoV钢中的粒状贝氏体为岛状、颗粒状,也有不规则形状,下贝氏体铁素体板条比低碳钢和超低碳钢中的板条更宽,分布更分散,板条形态不规则;随着回火温度的升高,45CrMoV钢中的渗碳体由细针状变为细条状,最后长大为椭球状,材料强度下降,韧性上升。     

Ti微合金化高强度热轧带钢组织性能及强化机理

The continuous cooling transformation behavior, the effect of coiling temperature on microstructure and mechanical properties, and strengthening mechanisms of Ti microalloyed high strength hot strip steel were systematically investigated by thermal simulation testing machine, laboratory rolling mill, SEM and HR-TEM. The dynamic CCT curve was established. The results show that the austenite to ferrite and pearlite transformation takes place when the cooling rate is less than 1??/s. The austenite to bainite transformation accompanied with austenite to ferrite and pearlite transformation takes place when the cooling rate is in the range of 5 ??/s to 10 ??/s. The bainitic transformation temperature is about 600??. The amount of granular bainite decreases, while the amount of lath bainite increases with the increase of cooling rate in the range of 20??/s to 50??/s. Furthermore, the study on the effect of coiling temperature on the microstructure and mechanical properties of experimental steel has shown that the strength and plasticity of tested steel are improved with decreasing the coiling temperature. When the coiling temperature is 550?棬the experimental steel possesses optimal mechanical properties owing to the grain refinement and precipitation of nano-scale TiC particles. And the tensile strength, yield strength and elongation of tested steel were 742MPa, 683MPa and 22??5%, respectively.     

热变形参数对0.05C-0.13Nb钢相变组织影响

利用Thermecomastor-Z热模拟试验机,研究了含铌0.13%微合金低碳钢奥氏体未再结晶区(超过50%、发生再结晶)变形、并以0.1～50℃/s的冷却速度连续冷却过程的相变。研究了热变形参数对相变组织的影响。结果表明,在未再结晶区变形,在连续冷却条件下,冷却速度≥5℃/s时,90%以上组织为粒状贝氏体;在相同变形温度情况下,随着变形量的增加,先共析铁素体的量增加,贝氏体的量随之减少。     

低碳贝氏体钢连续冷却相变规律研究

利用Gleeble1500热/力模拟实验机,研究了抗拉强度为700 MPa级的低碳贝氏体钢的相变规律,分析了不同冷却速率对钢组织及性能的影响。结果表明：轧后试样在1℃/s～30℃/s较宽的冷却速度范围内均可得到贝氏体组织,并随着冷却速度的增加,显微组织以粒状贝氏体为主转变为以性能优良的板条贝氏体和马氏体为主,在不降低韧性指标的前提下,提高了强度,为700 MPa级的低碳贝氏体钢工艺制度的制订提供了依据。     

Study on transformation behavior of hot- rolled microalloyed TRIP steel

Effects of deformation mode, deformation temperature, deformation rate, cooling rate and slow- cooling stop temperature on the transformation behavior of hot- rolled microalloyed TRIP steel were studied by means of MMS- 300 thermomechanical simulator. The results show that for the samples subjected to the single or double pass deformation, ferrite transformation area is expanded, pearlite transformation area appears, and martensite transformation area disappears in the continuous cooling transformation diagrams. Transformation temperatures of Ar3, Bs and Bf decrease, diffusional transformation is prevented and intermediate temperature transformation is promoted with the increase of deformation temperature or cooling rate. When deformation temperature is 850??, transformation temperatures of Ar3, Bs and Bf increase, the amount of ferrite also increases, and the amount of bainite decreases in the microstructure with the increase of deformation rate. With the decrease of slow- cooling stop temperature, ferrite amount increases, ferrite grains grow and retained austenite amount first increases and then decreases.     

TMCP工艺对低碳Ni-Nb钢组织转变和力学性能的影响

 为了研究TMCP工艺对低碳Ni-Nb钢显微组织转变类型和晶粒尺寸的影响规律，研究了不同TMCP工艺下的显微组织特征及其对力学性能的作用机理。结果表明，在未变形轧制情况下，当冷却速度小于5 ℃/s时，显微组织为铁素体和珠光体，铁素体晶粒尺寸随着冷却速度的增大而减小；在变形轧制情况下，随着冷却速度的增加，组织中的铁素体晶粒尺寸明显减小；当冷却速度增大到5 ℃/s时，微观组织中出现了大量粒状贝氏体。试制钢板试验表明，当冷却速度为4 ℃/s时，试验钢的组织为准多边形铁素体，可以有效提高钢的低温韧性；当冷却速度达到6 ℃/s时，试验钢微观组织中出现大量粒状贝氏体，明显降低钢的低温韧性。     

Nb-Ti微碳深冲双相钢的连续冷却转变规律

摘要：通过连续冷却实验研究了Nb Ti微碳深冲双相钢在不同冷却速率下的显微组织变化规律。并结合显微组织、热膨胀曲线以及实验钢的硬度值绘制出实验钢的CCT曲线。结果表明,实验钢的CCT曲线由铁素体、珠光体与贝氏体区组成,其中铁素体和贝氏体的区域较大,覆盖冷却速度范围较广。实验冷却速率下未出现马氏体组织。在05～1℃/s的慢冷速下,组织由铁素体和珠光体组成;当冷速增加至3℃/s时,贝氏体开始出现,珠光体消失。当冷速在5～10℃/s范围内时,获得铁素体+贝氏体双相组织;当冷速大于10℃/s时,铁素体相变消失,此时为纯贝氏体转变。热处理过程中若想获得一定量的马氏体组织,退火温度宜设置在820～900℃双相区较低温度范围,使合金元素充分富集于少量奥氏体中,在随后冷却过程中此奥氏体转变为马氏体组织。     

变形温度对CSP热轧65Mn带钢相变行为的影响

利用ThermecMastor-Z型热模拟试验机模拟CSP工艺条件,辅以金相显微镜(OM)、扫描电镜(SEM)和维氏硬度计等,研究65Mn钢的连续冷却转变规律及变形温度对其等温相变的影响。绘制了65Mn钢的动态CCT曲线。结果表明,当轧后冷速小于2℃/s时,试验钢可获得铁素体和珠光体组织。随着冷速的增大,试验钢中将出现贝氏体和马氏体组织,硬度增大。当冷速大于40℃/s时,试验钢中的组织全为马氏体,硬度达到678.05HV。此外,在研究不同变形温度对65Mn钢等温相变的影响时发现,第2道次变形温度为920℃时,珠光体组织多呈片层状,硬度为271.86HV;随着变形温度的降低,试验钢中铁素体含量增加,珠光体球化趋势明显,粒状珠光体含量增多。当变形温度下降至860℃时,试验钢的硬度降低至252.21HV,有利于其后续深加工。     

铜对中碳硅锰钢连续冷却相变的影响

 为了探索含铜中碳硅锰钢连续冷却转变过程中的相变规律,采用DIL805L型膨胀仪研究了铜对中碳硅锰钢连续冷却过程中显微组织和硬度的影响,借助高分辨透射电镜研究了连续冷却过程中含铜相的析出行为。结果表明,在中碳硅锰钢的连续冷却过程中,铜的加入使得铁素体转变的孕育期延长,且降低贝氏体和马氏体开始转变温度。富铜颗粒在铁素体中弥散析出,细化连续相变组织。冷却速度小于21 ℃/s时,含铜中碳硅锰钢由于富铜颗粒析出以及贝氏体和马氏体组织增加引起显微硬度增加。当冷却速度大于21 ℃/s时,铜反而会降低钢中贝氏体和马氏体组织的显微硬度。     

Nb-V-Ti微合金化高强度钢08MnCr连续冷却转变曲线和组织

利用ThermecMaster-Z热模拟实验机测定了一种Nb-V-Ti微合金化高强度钢08MnCr(S2)在910～1 200℃不变形(静态)和变形(动态)奥氏体0.05～30℃/s冷速下连续冷却转变(CCT)曲线,并分析和观察了对应的相变及组织。实验结果表明,提高轧后的冷却速度使Ar₃降低,导致钢的晶粒进一步细化;冷却速度大于10℃/s开始出现贝氏体转变。提高加热温度时相变温度降低,变形奥氏体相变温度较不变形奥氏体相变温度高。冷速较低时,铁素体晶粒呈多边形;冷速高时,铁素体晶粒多呈尖角形。