AZ31镁合金热变形规律的研究

利用等温压缩试验方法,研究了AZ31镁合金在应变速率为0.001~1 s-1,变形温度为473K~623K的条件下的变形行为.动态再结晶是该试验条件下晶粒细化的主要机制,通过分析显微组织的变化来研究动态再结晶的机制,同时研究孪晶对再结晶机制的影响.     

镁锂合金热加工图建立和塑性失稳因素的研究

通过对LAZ532镁锂合金在125~250℃,应变速率为10-4~10-1s-1条件下拉伸变形行为研究.构建LAZ532镁锂合金失稳图和加工图.研究结果表明:在变形温度低于180℃时合金出现塑性失稳,导致塑性失稳的主要原因是变形孪晶;合金较适宜加工区域为变形温度(t)220℃,应变速率0.001 s-1处,该区域的功率耗散效率较高,合金能发生动态再结晶,并具有较好的塑性.     

形变和热处理温度对纯铌管材组织和性能的影响

通过对纯铌挤压管坯和冷变形管材的显微组织及力学性能的分析,研究了形变程度和热处理温度对材料的组织和性能的影响.试验结果表明,经800～850℃挤压的纯铌管坯,完全再结晶退火温度约为1 150℃,挤压管坯经87%冷变形后,完全再结晶退火温度约为1 100℃;纯铌管材完全再结晶退火温度随着形变总加工率的增加,基本呈下降趋势,且影响比较明显.     

微量Zr对Cu—Zn合金再强晶的影响

制备了Ｃｕ１３Ｚｎ,Ｃｕ１３Ｚｎ０．０１３Ｚｒ和Ｃｕ１３Ｚｎ０．０９Ｚｒ３种合金（质量分数,％）,通过对这些合金在不同处理态处的硬度测定和显微组织观察,分析了Ｚｒ对这类合金的再结晶的影响。结果表明：添加微量Ｚｒ（０．０１３％,质量分数）明显细化Ｃｕ－Ｚｎ合金热变形和冷变形后的退火再结晶晶粒;进一步提高Ｚｒ的含量（０．０９％）,可有效地抑制合金的动态和静态再结晶,合金的完全再结晶温度提高到５００℃以     

挤压-拉拔工艺对铌-锆合金线组织与性能的影响

为了研究铌-锆合金线的组织和性能,以电子束熔炼的铌-锆合金(wZr=0.940 0%)铸锭为原料,研究挤压开坯和拉拔的生产工艺及其过程中冷变形量和退火过程对铌-锆合金线组织和性能的影响.结果表明,由于挤压时铸锭内外层和前后端变形不均匀,导致沿长度和断面上挤压所得棒材的组织与性能不够均匀;冷变形量越大,铌-路线的强度和硬度越高,而延伸率在30%冷变形后变化不大;冷变形量越大,则再结晶温度越低;随着退火温度升高,铌-锆线强度呈先下降后升高趋势,延伸率呈先升高后下降趋势.     

挤压温度对固相再生ZM6镁合金组织和性能的影响

利用固相再生方法在挤压比为25：1的条件下,将ZM6镁合金屑分别在350℃、400℃、450℃和500℃温度下制备成试样,进行微观组织观察和力学性能测试。结果表明：当挤压温度为400℃时,ZM6耐热镁合金没有发生再结晶,合金中金属化合物在挤压过程中被打碎,均匀分布在基体中;当挤压温度为450℃和500℃时,ZM6镁合金发生部分动态再结晶;随着挤压温度的提高,合金的抗拉强度和延伸率提高;在挤压温度为500℃,合金的抗拉强度、屈服强度和延伸率分别为300．2MPa、142．9MPa和30％。合金室温拉伸断口主要表现为穿晶韧窝断裂。     

AZ31镁合金在不同挤压比和挤压温度下的织构演变

采用工业挤压机研究了挤压比和挤压温度对AZ31镁合金织构的影响.结果表明,在相同的挤压温度下,随挤压比增加,以{01(-1)0}面织构为代表的变形织构由强到弱;而以{06(-6)1}、{02(-2)1}面为代表的再结晶织构由弱到强.主要织构组分在挤压比为16处形成拐点,形变织构降至最低,随后再结晶织构逐渐增强,表明在拐点附近再结晶完成.挤压比相同时,低温度变形的织构组分以{01(-1)0}面形变纤维织构为主.当挤出温度增至258℃时,达到完全动态再结晶,温度再增高将形成高漫散度的{01(-1)0}再结晶织构.     

热挤压对AM50-1%Gd合金组织与性能的影响

针对镁合金高温力学性能差的问题,通过采用热挤压、时效处理、力学性能测试及组织形貌观察等方法,研究了热挤压处理对AM50-1%Gd合金组织与性能的影响.结果表明：AM50-1%Gd合金组织结构由α Mg、Mg₁₇Al₁₂和Mg₂Gd相组成.热挤压可明显提高AM50-1%Gd合金的抗拉强度和屈服强度,并随着挤压温度的降低,合金的强度值增大.而经时效处理后,挤压态合金在室温及高温的抗拉强度和屈服强度可再次提高.挤压态AM50-1%Gd合金中的细小晶粒来自于热挤压期间发生的动态再结晶,热挤压能提高合金抗拉强度的主要原因是形变强化和细晶强化,而细晶强化和细小第二相沿晶界弥散析出是时效态合金综合力学性能好的主要原因.     

热处理对挤压变形AM50镁合金疲劳行为的影响

采用低周疲劳试验研究了固溶处理和时效处理对挤压变形AM50镁合金在疲劳加载条件下的变形行为和疲劳寿命的影响.结果表明，固溶和时效处理均可改变挤压变形AM50镁合金的循环应力响应行为和循环应力-应变行为，并降低挤压变形AM50镁合金的循环应变硬化指数和循环强度系数；在高的外加总应变幅下，固溶和时效处理可以提高挤压变形AM50镁合金的疲劳寿命，但当外加总应变幅较低时，固溶和时效处理则降低挤压变形AM50镁合金的疲劳寿命；固溶处理将抑制挤压变形AM50镁合金在疲劳变形期间发生动态应变时效.     

Pd、Ru、Ce元素对Pt-Pd-Rh合金再结晶的影响

研究了在Pt-Pd-Rh合金中Pd含量由约4%增至15%,及添加少量Ru、微量Ce后对合金再结晶温度和显微组织的影响.结果表明：Pd对合金的再结晶影响不大;少量Ru（＜3%）提高了合金的再结晶温度,微量Ce能显著提高合金再结晶温度,但Ce含量过高却使合金的再结晶温度降低.     

A high strength Mg-6Zn-1Y-1Ce alloy prepared by hot extrusion

Microstructures and tensile properties of Mg-6Zn-1Y-1Ce alloy extruded in a temperature range between 300 °C and 400 °C were investigated. The yield strength of the material increased as the extrusion temperature decreased due to grain refinement. The yield strengths and grain sizes of extruded samples met Hall-Petch equation. The microstructure of the alloy extruded at 300 °C had a bimodal grain size distribution with an average grain size of 2.7 μm and showed a yield strength of 327 MPa with an elongation of 9%. The fine-grained microstructures were attributed to the dynamic recrystallization and the pinning effect of fine strengthening particles.     

Al-5Fe-1.2Si-1Mg-0.6Cu-0.5Mn合金轧制变形行为及组织性能

为了细化Al-5%Fe基合金中粗大的脆性针状或针片状富铁相,采用电磁搅拌及固态挤压技术制备Al-5%Fe-1.2%Si-1%Mg-0.6%Cu-0.5%Mn合金轧制坯锭,研究Al-5%Fe基合金的轧制变形能力及合金的组织性能,并用热压缩实验模拟了铝铁合金在783~693K、变形速率为0.01~10s^-1条件下的热变形行为.结果表明：该合金高温变形时存在明显的稳态流变特征,流动应力对应变速率和温度敏感.板材力学性能较挤压态有大幅度提升,其室温下的抗拉强度和伸长率最高达到354.5MPa和7.6%,比挤压态分别提高了105.6%和184.6%.轧制对铝铁合金中富铁相的破碎作用十分明显.     

Effects of Extrusion Processing on Microstructure of 7075Al Alloy in the Semi-solid State

A recrystallization and partial melting(RAP) process was introduced to prepare the semi-solid 7075 aluminum alloy used for thixoforming. In order to obtain an ideal semi-solid microstructure, a series of extrusion experiments were conducted to comparatively investigate the optimum extrusion process parameters. Commercial 7075 Al alloy samples were firstly extruded with varying extrusion ratios below the recrystallization temperature followed by homogenization, then these samples were reheated to the semi-solid state and held in the range of 5 to 50 minutes. The experimental results show that varying process cause the difference in the deformation degree and microstructure for as-extruded samples, resulting in various semi-solid microstructure. It is verified that the formation of equiaxed grains in semi-solid microstructure depends on recrystallization behavior of extruded samples during partial melting. Both relative high extrusion temperature and low extrusion ratio lead to high volume fraction of recrystallized area, thus entirely equiaxed solid grains in semi-solid 7075 Al alloy samples can be obtained finally. In addition, Ostwald ripening was determined as the dominate coarsening mechanism of solid grains in semi-solid state for this 7075 Al alloy during the RAP route. The influence of predeformation on recrystallization behavior of this 7075 Al alloy was discussed in detail.     

AZ31B镁合金动态力学行为及变形机制

为了研究挤压态AZ31B镁合金在高应变速率下的力学行为及变形机制,采用分离式Hopkinson压杆和反射式拉杆装置在室温对挤压态AZ31B镁合金进行了动态压缩和拉伸试验,平均应变速率范围在500~2600s^-1之间,用光学显微镜观察了测试后试样的微观组织变化.结果发现,由于在挤压过程中形成了基面织构,沿挤压方向压缩时,拉伸孪晶｛1012｝<1120>首先启动,屈服强度对应变速率不敏感,且屈服强度较低,但在塑性变形的第二阶段,位错滑移参与变形,应变速率硬化效应显著;沿挤压方向拉伸时,压缩孪晶｛1011｝<1120>和非基面滑移是其主要的塑性变形机制,合金屈服强度较高,并表现出轻微的正应变速率效应;由于织构的形成,合金在压缩和拉伸时表现出很强的拉压不对称性,压缩屈服强度与拉伸屈服强度的比值约为0.32.     

Microstructures and mechanical properties of Mg-Ce-Zn-Zr wrought alloy

Microstructures and mechanical properties of Mg-2.0 ?-0.7 % Zn-0.7% Zr alloy were studied. The results of scanning electron microscopy show that Mg12 Ce phase mainly distributes at the grain boundaries. The fine Mg12 Ce phase can apparently elevate recrystallization temperature by preventing the grain boundary migration. No dynamic recrystallization occurs during the hot-extrusion. The mechanical properties of as extruded specimens are σb=278.5MPa, δ=12.0%, while those of the specimens annealed at 250℃ for 100 h are σb=272.6 MPa, δ=11.3%, which indicate that the alloy has good mechanical properties at room temperature.     

Mg-9Gd-3Y合金热变形行为与本构关系

为了解决Mg-9Gd-3Y合金在热塑性变形过程中的本构关系问题,对Mg-9Gd-3Y合金进行了不同变形温度（653～753K）下采用不同应变速率（0.01～10s-1）的热压缩试验,利用载荷/位移数据建立真应力/真应变曲线和本构方程.结果表明：动态再结晶在晶界处较易发生,流变曲线显示出典型的动态再结晶特征,以及应力水平与变形温度和应变速率的关系.本构方程预测出的流变应力数据与相应的试验结果较一致.     

AZ91镁合金热挤压成形工艺的研究

通过对均匀化退火后的AZ91镁合金热挤压成形工艺试验研究,分析了热挤压成形时挤压力以及组织性能的变化规律．结果表明：挤压力随挤压温度的升高、挤压比和挤压速度的减小而下降,抗拉强度随挤压温度、挤压比和挤压速度的升高而升高,同时证明了均匀化后的AZ91镁合金具有良好的挤压成形性,其制品有较好的综合力学性能,抗拉强度σ6均在310—340MPa之间,延伸率8在10％-12％之间．     

Plastic deformation behavior of ZK60 magnesium alloy with addition of neodymium

The hot deformation simulation of a ZK60 magnesiuln alloy at different temperatures from 373 to 673 K and different strain rates of 0.1, 0.01 and 0.002 s^-1 was studied by using the Gleebe-1500 simulator. The plastic deformation behavior was measured and the deformation activation energy was calculated. The microstructures of ZK60 magnesium alloy with an addition of neodymium during the deformation process were observed by using Polyvar-MET optical microscope and Tecnai G^2 20 TEM. The results show that the working hardening, the dynamic recovery and the dynamic recrystallization occur during the plastic deformation process at different temperatures and strain rates. The dynamic recrystallization starts when the temperature is over 473 K and the DRX grain size after hot deformation is only 5-10 μm. So the refined grains improve both the tensile strength and the elongation of alloys at room temperature. Neodymium is added into the alloy and a precipitate phase Mg12Nd that impedes the movement of dislocations is formed, which benefits to increasing mechanical properties of ZK60 magnesium alloy.