ON THE INDUCED MAGNETIC ANISOTROPY OF METALLIC GLASS Fe__(78)Si_(10)B_(12)

研究了金属玻璃Fe_(78)Si_(10)B_(12)的磁化惑生各向异性常数K_(um)和应变感生各向异性常数K_(us)的350℃等温退火动力学行为和随测量温度T的变化,具有正值的K_(um)以lgta的线性函数随退火时间ta变化,而正比于M_s~(4.6)(T)随T变化,具有负值的K_(us)对于退火时张力的施加和去除作可逆的弛豫变化,而正比于M_s~(7.5)(T)随T变化,用一种畸变方向有序模型对结果作了定性解释。     

金属玻璃Fe_(78)Si_(10)B_(12)的感生磁各向异性

研究了金属玻璃Fe_(78)Si_(10)B_(12)的磁化惑生各向异性常数K_(um)和应变感生各向异性常数K_(us)的350℃等温退火动力学行为和随测量温度T的变化,具有正值的K_(um)以lgta的线性函数随退火时间ta变化,而正比于M_s~(4.6)(T)随T变化,具有负值的K_(us)对于退火时张力的施加和去除作可逆的弛豫变化,而正比于M_s~(7.5)(T)随T变化,用一种畸变方向有序模型对结果作了定性解释。     

EFFECT OF ROTATING MAGNETIC FIELD ANNEALING ON INDUCED ANISOTROPY OF AMORPHOUS ALLOYS

研究了旋转磁场退火对非晶态合金Fe_4Co_(66)Ni_2T工_2Si_(10)B_(16),Fe_5Co_(70)Si_(15)B_(10)及Fe_(40)Ni_(40)B_(20)的磁各向异性的影响。用磁转矩方法测定了在不同旋转速率的磁场作用下合金中感生磁各向异性在等温退火(260—280℃)过程中的变化。实验结果指出,在旋转磁场退火过程中,原存于试样中的感生磁各向异性K_u值随退火时间单调下降,其下降曲线和磁场的旋转速率无关;而由旋转磁场退火所感生的磁各向异性,在一般实际条件下,可以忽略不计.这个实验结果可以成功地用本文提出的理论进行解释.     

旋转磁场退火对非晶态合金中感生磁各向异性的影响

研究了旋转磁场退火对非晶态合金Fe_4Co_(66)Ni_2T工_2Si_(10)B_(16),Fe_5Co_(70)Si_(15)B_(10)及Fe_(40)Ni_(40)B_(20)的磁各向异性的影响。用磁转矩方法测定了在不同旋转速率的磁场作用下合金中感生磁各向异性在等温退火(260—280℃)过程中的变化。实验结果指出,在旋转磁场退火过程中,原存于试样中的感生磁各向异性K_u值随退火时间单调下降,其下降曲线和磁场的旋转速率无关;而由旋转磁场退火所感生的磁各向异性,在一般实际条件下,可以忽略不计.这个实验结果可以成功地用本文提出的理论进行解释.     

MSSBAUER STUDY ON MAGNETIC ANISOTROPY OF AMORPHOUS ALLOY Fe_(71)Ni_(10)B_(13)Si_4C_2

本文研究了Fe_(71)Ni_(10)B_(13)Si_4C_2非晶态合金在磁场退火时的反常磁各向异性变化。结果表明,在430℃磁场热处理时优先发生了表面晶化现象,导致垂直磁各向异性的反常增大。磁矩取向的择优性取决于压应力引起的和磁场热处理感生的两种磁各向异性。     

非晶态合金Fe_(71)Ni_(10)B_(13)Si_4C_2磁各向异性的Mssbauer谱研究

本文研究了Fe_(71)Ni_(10)B_(13)Si_4C_2非晶态合金在磁场退火时的反常磁各向异性变化。结果表明,在430℃磁场热处理时优先发生了表面晶化现象,导致垂直磁各向异性的反常增大。磁矩取向的择优性取决于压应力引起的和磁场热处理感生的两种磁各向异性。     

非晶合金带的单轴各向异性SCIEI

本文给出了非晶合金带Fe_(54.4)Ni_(36.4)Cu_(0.5)Mn_(0.3)Co_(0.2)Si_(0.2)P_(8.0)室温下的铁磁共振(FMR)谱及谱线形状随θ角的变化(θ角为静磁场H_e与非晶合金带轴方向之间的夹角)。当θ=0°时FMR谱为单峰,当θ=90°时出现明显的复峰,线宽ΔH具有各向异性特性。用FMR理论分析得出非晶合金具有以带轴方向为易轴的单轴各向异性。     

7050铝合金厚板平面应变断裂韧度的研究

采用紧凑拉伸C(T)试样测试7050-T7451铝合金厚板不同厚度、不同取样方向的断裂韧度,通过宏观断口形貌、扫描电镜微观断口形貌和能谱分析等手段研究材料平面应变断裂韧度K_(ⅠC)性能。结果表明:试样满足一定厚度要求时,虽然表面存在小范围平面应力层,亦可获得有效平面应变断裂韧度结果;不同取样方向的断裂韧度性能存在显著各向异性,L-T方向断裂韧度最大,为韧窝型韧性断裂;其次是T-L方向,为韧窝排列具有方向性的脆性断裂,S-L方向断裂韧度最小,主要为沿晶脆性断裂。     

Tb_xDy_(1-x)(Fe_(0.6)Co_(0.4))_2合金的磁性和磁致伸缩性能

利用电弧熔炼法制备Tb_xDy_(1-x)(Fe_(0.6)Co_(0.4))_2合金(0.27≤x≤0.40),对合金的磁性和磁致伸缩性能进行研究。利用XRD、交流初始磁化率测试仪、超导量子干涉仪和标准应变测试仪,对样品的物相组成、居里温度、磁化曲线和磁致伸缩性能进行表征。结果表明:当x≤0.27时合金的易磁化方向为á100?方向,当x≥0.30时合金的易磁化方向变为〈 111〉方向;合金的居里温度随x的增加而增加;x=0.32附近时合金的磁晶各向异性常数K_1有极小值,室温时合金在x=0.32附近时达到各向异性补偿;当x=0.32时饱和磁致伸缩系数达到9.57×10~(-4);随Co含量的增加,合金的各向异性补偿点向Tb含量高的方向移动。Tb_(0.32)Dy_(0.68)(Fe_(0.6)Co(0.4))_2合金具有高磁致伸缩系数和低各向异性,是一种实用的磁致伸缩候选材料。     

镁基六铝酸镧粉体的制备及高温原位XRD研究

采用反向化学共沉淀-高温煅烧法制备了镁基六铝酸镧(La Mg Al_(11)O_(19))粉体。利用X射线衍射、场发射扫描电子显微镜、高温原位X射线衍射及Rietveld晶体结构精修法对粉体的物相组成、显微形貌、晶体结构及晶格热膨胀行为进行了研究。结果表明,反向化学共沉淀制备的氢氧化物前驱体经1600℃热处理后完全转变为磁铅石结构的La Mg Al_(11)O_(19),呈规则六方板片状,晶面光滑平整。采用高温原位XRD技术及Rietveld晶体结构精修系统研究了镁基六铝酸镧材料的晶格热膨胀行为。随着温度的升高,镁基六铝酸镧(La Mg Al_(11)O_(19))晶格热膨胀表现出各向异性,晶胞参数a和c随温度变化关系为:a T=5.5821+1.625×10~(-5)T+1.757×10~(-8)T~2+4.24×10~(-12)T~3,c T=21.9189+1.1952×10~(-4)T+4.587×10~(-8)T~2+5.463×10~(-11)T~3。室温~1300℃,//a平均热膨胀系数为8.42×10~(-6)℃~(-1),//c平均热膨胀系数为12.54×10~(-6)℃~(-1)。La-O键键长(或键能)的各向异性是La Mg Al_(11)O_(19)晶格热膨胀各向异性的主要原因。     

压应力对Sm-Fe-B薄膜磁致伸缩性能的影响

压应力对Sm-Fe-B磁致伸缩性能的改善有重要影响,但是其大小对磁致伸缩特性变化趋势的研究很少,而且还未见到压应力对磁各向异性影响的报道。本文利用特制夹具,使玻璃衬底在镀膜过程中受到不同应力作用,镀膜结束后,当玻璃衬底从夹具取下后,利用其恢复到原来状态,可以对稀土Sm-Fe-B薄膜产生压应力作用。通过调整夹具使衬底具有不同的预应力,可得到受到玻璃衬底不同压应力大小作用的薄膜样品。利用LK-G150激光微位移传感器与交变梯度磁强计（AGM）分别测试薄膜悬臂梁自由端偏转量与磁滞回线,以研究具有不同压应力对薄膜的磁致伸缩性能的影响,并且利用磁力显微镜（MFM）测试了薄膜样品垂直表面的磁畴分布情况。实验结果表明：受到压应力作用的薄膜易磁化轴都位于膜面内,以面内各向异性为主,磁畴结构基本分布在面内。随着压应力的增加,易磁化轴由膜面内的短轴转向膜面内的长轴,这一转变有利于器件的设计,但是磁畴在垂直膜面方向略有提高,薄膜的低场磁致伸缩性能也随着压应力的增大而有显著提高。     

Influence of Oblique Sputtering on Stripe Magnetic Domain Structure and Magnetic Anisotropy of CoFeB Thin FilmsEI北大核心CSCD

Magnetic anisotropy is one of the most important fundamental properties of magnetic thin film. The strength of magnetic anisotropy determines the ferromagnetic resonance frequency of magnetic films in the high-frequency applications. Because of the directionality of conventional static magnetic anisotropy in magnetic film, the high-frequency device usually shows an obvious directionality. When the microwave magnetic fi eld deviates from the perpendicular direction of magnetic anisotropy, the devices cannot reveal their best performance. The magnetic film with a stripe magnetic domain structure displays an in-plane rotatable magnetic anisotropy, which can be an important strategy to solve the problem of magnetic fi eld orientation dependent performance in high-frequency device. Therefore, the magnetic domain, the magnetic anisotropy, and the high-frequency behaviors for magnetic fi lms with a stripe magnetic domain structure have received extensive attention. Previously, most of the studies focused on the stripe magnetic domain structure of polycrystalline thin films. However, less attention was paid on amorphous magnetic thin films. Since the amorphous magnetic films have no long-range ordered crystal structure, no magnetocrystalline anisotropy, no grain boundary defects resistance hindering the domain wall displacement, they usually show excellent soft magnetic properties and have been widely applied in high-frequency devices. CoFeB alloy is one of the most important amorphous magnetic materials and has been extensively applied in various spintronic devices. In this work, amorphous CoFeB magnetic thin films were prepared by using a method of oblique sputtering technique at room temperature. The influences of oblique sputtering on the stripe magnetic domain structure, the in-plane static magnetic anisotropy, the in-plane rotational magnetic anisotropy, and the perpendicular magnetic anisotropy of the amorphous CoFeB films were studied by scanning probe microscope, vibrating sample magnetometer, ferromagnetic resonance. It is found that the method of oblique sputtering could effectively reduce the critical thickness for the appearance of stripe magnetic domain in amorphous CoFeB films. For a non-oblique sputtered CoFeB film, the critical thickness for the appearance of the stripe magnetic domain is above 240 nm. In contrast, after been subjected to the oblique sputtering, the critical thickness becomes below 240 nm. The different magnetic characterizations indicate that for the growth of CoFeB films with stripe magnetic domain structure, the oblique sputtering could not only enhance the strength of in-plane static magnetic anisotropy, but also improve the in-plane rotational magnetic anisotropy and the perpendicular magnetic anisotropy. All of the magnetic anisotropies are increased with the angle of oblique sputtering. The observation results of XRD and TEM prove that the prepared CoFeB thin films tend to amorphous structure. The characterization of SEM observation indicates that although the amorphous CoFeB films do not possess long-range ordered crystalline structure, they still could form a kind of columnar structure. The slanted columnar structure of CoFeB films could significantly increase the perpendicular magnetic anisotropy, thus lead to the appearance of stripe magnetic domain structure.     

In-plane anisotropy of 1545 aluminum alloy sheet

1　INTRODUCTIONThe in plane anisotropy of mechanical proper ties brings the limitation to the use of alloy sheet.At the same time, during the material processing,the difficulties of contour machining will also be in creased. For this reason, when designing high performance aluminum alloy sheets, the in planeanisotropy is an important performance parameterthat must be considered. Studies have shown thatminor Sc and Zr in the Al Mg Mn alloy can refinegrains of cast ingot, inhib…     

In-plane Uniaxial Anisotropy and Magnetization Reversal Mechanism of FeCo Films by Strip Pattern

Strip-like Fe Co films were patterned by a traditional lithograph process from intrinsically isotropic continuous Fe Co films. The strip-patterned Fe Co film shows a strong in-plane uniaxial magnetic anisotropy with easy axis along the length direction of the strip. The angular dependences of remanence ratio, switching field, and coercivity indicate that the magnetization reversal mechanism of the strip-patterned Fe Co film is coherent rotation and domain wall depinning when the applied field is near the hard axis and easy axis, respectively. The consistency of the experimental hysteresis loops of the strip-patterned Fe Co film and calculated hysteresis loops with a simple in-plane uniaxial anisotropy model indicates that the strip-patterned Fe Co film behaves as a single domain. The absence of the domain wall and the strong in-plane anisotropy field make the strip-patterned Fe Co films have much potential for high-frequency application.     

Co—Ni合金磁诱发马氏体相变的热力学分析

从应力诱发马氏体相变热力学角度出发,分析了外磁场作用下具有高磁晶各向能的Co-Ni合金磁诱发马氏体相变热力学,并建立了新的数学模型。     

Roles of interface roughness and internal stress in magnetic anisotropy of CoPt/AlN multilayer films

Magnetic anisotropy of CoPt/AlN multilayer films has been studied by systematically varying the nominal thickness of CoPt layers, t_CoPt (1–10 nm), and the annealing temperature, T_a (300–500 °C). The as-deposited films show in-plane magnetic anisotropy in the full range of t_CoPt, whereas the annealed films show perpendicular magnetic anisotropy (PMA) within small t_CoPt but change to in-plane magnetic anisotropy when t_CoPt is over a certain thickness. The critical thickness for such anisotropic transformations increases as the T_a increases. The maximum PMA obtained in this work is 1.13 × 10⁷ erg cm^?3. The interface roughness was analyzed by cross-sectional high-resolution electron microscopy and X-ray reflectivity using an abrupt interface model with a Debye exponent shape. The internal stress was analyzed by X-ray diffraction using an equal biaxial stress model. The results show that the CoPt/AlN interface roughness decreases from 0.385 nm to 0.158 nm and the internal stress increases from ?2.36 GPa (compressive) to 1.73 GPa (tensile), as the T_a increases to 500 °C. The roles of the interface roughness and the internal stress in the magnetic anisotropy of CoPt/AlN multilayer films are studied.     

Low-frequency ferromagnetic resonance in a uniaxial magnetic film

The equations of the precession dynamics of the magnetic moment have been analyzed to study the specific features of the low-frequency ferromagnetic resonance corresponding to magnetic biasing along the hard magnetic axis of a film with an in-plane uniaxial anisotropy. It has been found that the precession trajectories exhibited a complicated hopping behavior and the resonance curve was asymmetric. This behavior and the asymmetry were due to an angular bistability arising from the presence of two symmetric angular positions of equilibrium near the anisotropy field.     

Effect of fabrication parameters on the microstructure,in-plane anisotropy and magnetostriction of Fe-Ga thin films

The microstructure,in-plane anisotropy,and magnetic properties of Fe-Ga thin films were investigated by X-ray diffraction analysis,vibrating sample magnetometer,and capacitive cantilever method.The in-plane induced anisotropy is well formed by the applied magnetic field during sputtering,and the anisotropy field Hk decreases with the sputtering power increasing.The coercivity of Fe-Ga thin films decreases with increasing power when the sputtering power is less than 60 W and increases when the power is larger than 60 W.The magnetostriction of the thin films reaches 66 × 10-6 at the sputtering power of 60 W.Excellent Fe-Ga films,which exhibit good field sensitivity,low coercivity and high magnetostriction,have been fabricated at the power of 60 W,and they can be used as the materials of magnetostrictive transducers.     

Feasibility of magneto-optic flaw visualization using thin garnet films

We investigate the feasibility of using rare-earth iron garnet films grown on (111)-oriented substrates as magneto-optic indicator films for the visualization of magnetic leakage fields in non-destructive evaluation. In most cases the leakage field of the defect has a strong component in the film plane. The influence of this in-plane dc magnetic field on the image formation is investigated. It is shown that the presence of a strong in-plane magnetic field allows one to extend the dynamic range of the out-of-plane field imposed by the uniaxial anisotropy field H_A. On the other hand, an in-plane field reduces the sensitivity. The guidelines for selecting parameters of magneto-optic indicator films are given.     

纵磁退火处理和张应力对1K101非晶合金薄带磁化特性及损耗的影响

研究了纵磁退火处理和张应力对1K101非晶合金薄带磁化特性以及损耗的影响,并采用Kerr方法观测了合金的磁畴形貌。结果表明,张应力驱动淬火态1K101合金感生出宏观单轴各向异性,使带材沿应力方向趋向于易磁化,且铁损下降,这与经纵磁退火处理后的带材磁化特征高度相似。通过磁畴观测发现,在张应力作用下,淬火态非晶合金中迷宫样窄小畴的磁畴壁沿应力方向呈Z字形排列,说明沿应力方向磁化时需消耗的外磁场能减少,这对带材软磁性能的优化起到了关键作用。