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1.
热锻模长期在高温环境中承受较大机械载荷以及冷热疲劳等作用,容易发生破坏失效。通过等离子粉末堆焊在模具表面上堆焊制备出高性能表面覆层,大幅度提高了模具性能。通过对复合材料的制备方案的分析,选择镍基自熔性合金粉末,借助等离子粉末堆焊工艺制备出碳化铬增强镍基堆焊覆层。以H13钢为例,对比研究了镍基合金堆焊层以及镍基碳化铬堆焊层的组织成分、相结构及显微硬度。堆焊层的微观组织表明,堆焊层与基体冶金结合良好,堆焊层熔接线附近元素呈梯度分布。镍基堆焊层以及镍基碳化铬堆焊层组织均以γ-Ni固溶体为主,在晶界处分布有碳化物和硼化物。由于碳化铬颗粒的强化作用,镍基碳化铬堆焊层中的固溶体晶粒更加细小,同时碳化物数量更多,弥散分布在固溶体的晶界处。  相似文献   

2.
介绍了用横流式CO2激光器在X60CrMnMoVNbN2110钢表面熔覆Si3N4陶瓷的方法。用透射电镜和光学显微镜熔覆层内相组成及界面结构。结果表明,熔覆层内Si3N4或WC颗粒与粘结相Co形成包裹结构,各相结合致密,且与基材形成了冶金结合。其主要组成相为α-Si3N4,β-Si3N4,WC和Co,Si3N4在α→β相转变时,形成非周期性的反相畴结构。性能测定指出,熔覆层具有较高的硬度(1600  相似文献   

3.
激光熔覆Cu基复合涂层工艺与组织特征研究   总被引:4,自引:1,他引:3  
利用2kW的CO2气体激光器在45钢上熔覆Cu+Cr2O3粉末,获得了良好的的熔覆层。SEM观察发现,熔覆层组织中出现分层现象,由黑白两层交替组成。成分分析结果表明,黑层组织是富Fe相,而白层组织是富Cu相。以上双层组织形成过程与激光熔覆时溶池中的流动密切相关。  相似文献   

4.
李现勤  梁工英 《金属学报》1999,35(9):928-933
利用5kWCO2激光器激光熔覆A1合金表面的Ni-Cr-A1涂层,SEM与TEM分析结果表明,在激光熔覆层中的非晶组织呈空间扭曲薄片和杉叶状,它们分别存在于熔覆层颗粒间白色网状组织与颗粒中,利用差热分析(DTA)半定量测定熔覆层中的非晶含量。功能密度,扫描速度对非晶含量有较大的影响。  相似文献   

5.
为了在H13钢表面获得显微硬度呈梯度分布的铁基合金熔覆层,试验选取了三种铁基合金粉末FJ-1粉末、铁基合金粉末1号和高铬铁基合金粉末逐层进行激光熔覆,并探究了每层熔覆时的工艺参数,最终获得了由三种粉末堆积成的铁基合金梯度熔覆层,并对熔覆层的表面硬度、结合状态、组织和显微硬度等进行了分析。结果表明,三种粉末逐层熔覆后的梯度熔覆层表现出了表面平整、表面硬度较高、内部组织无明显缺陷且层间结合紧密的特征。熔覆层顶层晶粒细小,夹层和底层晶粒逐渐变大,熔覆层与H13钢结合处呈现良好的冶金结合特性。各层的显微硬度由基体逐渐向顶层升高,呈明显的梯度分布,最终得到梯度熔覆层。  相似文献   

6.
CeO2对NiCrBSi激光熔敷层组织和性能的影响田保红吴磊郑世安(洛阳工学院)杨院生(中科院金属研究所)在金属材料表面进行激光熔敷以获得特殊表面性能的研究已取得很大进展,并已用于生产,其中以镍基自熔合金应用最广[1~4]。但目前仍存在敷层与基体结合...  相似文献   

7.
目的 对比有无超声作用下熔体润湿行为,阐明超声对于熔体润湿行为的影响及作用机制,为超声辅助激光熔覆高质量成形提供参考。方法 基于高速相机拍摄研究了超声对于液滴润湿性的作用效果,进而研究了超声辅助激光熔覆过程中熔池的润湿行为,使用Canny算法提取熔池轮廓,采用体视显微镜和共聚焦显微镜观察试样宏观形貌,采用光学显微镜观察分析微观组织。结果 将超声振动施加于金属液滴,其在基板表面润湿性增强,金属液滴与基板接触面积增大39.3%。在熔覆过程中引入超声振动,熔池面积显著增大。随着超声功率比的增强,熔覆层的熔高降低,熔深减小,熔宽逐渐增大,熔覆层逐渐由弧形轮廓变为扁平。当超声功率比为80%时,熔覆层高度为无超声下的75.2%,熔覆层和基体之间的润湿性显著改善。在微观形貌上,超声能够改变晶粒生长方向,抑制枝晶外延生长。结论 超声振动作用于激光熔覆过程中,促进了熔体的润湿作用且加大了熔池流动性。熔体润湿行为的改变导致扁平熔覆层形状的形成,熔覆过程中熔池面积增大,熔池流动性增强,导致晶粒生长方向与枝晶长度的改变。  相似文献   

8.
氩弧熔覆Fe—Cr—Si—B系熔覆层的物相分析   总被引:6,自引:0,他引:6  
采用氩弧熔覆工艺在Q235基材上熔覆Fe-Cr-Si-B系列合金,获得良好的,具有较高硬度和耐磨性的熔覆层。对熔覆层的显微组织,硬度,耐磨性,物相形貌和相结构等进行分析,确定了不同条件下熔覆层中产生的物相种类。  相似文献   

9.
激光熔覆镍基WC层的耐蚀性能研究   总被引:5,自引:0,他引:5  
用5kW连续CO2激光器在40Cr钢基材表面对不同成分的镍基WC合金喷涂层进行激光重熔,研究了WC和CeO2加入量对激光熔覆层显微组织和耐蚀性能的影响,结果表明,添加适量WC和CeO2可以改善激光熔覆镍基自熔合金层的耐蚀性能。  相似文献   

10.
利用ATEM研究了铁基多元合金FeCrWNiC激光熔覆层的微观组织、亚稳相结构特征以及高温时效时的亚稳相转变机制。结果表明组织为亚共晶组织,即γ+(γ+M7C3),γ奥氏体为具有较高合金度的过饱和亚稳相,M7C3(M为Cr,Fe,W)为六方结构的Cr基亚稳合金碳化物。熔覆组织在高温时效时存在两类碳化物形成机制,即亚稳γ中析出M23C6、M2C与MC碳化物以及M7C3→M23C6与M7C3→M6C的碳化物原位转变机制。熔覆组织具有较高的显微硬度并存在显著的二次硬化特征  相似文献   

11.
吴玉梅  熊晓云  靳蓉  孙敬民  杨林  罗晓星 《金属学报》2005,10(10):1100-1103
目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。  相似文献   

12.
Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.  相似文献   

13.
The rheology feature of Sb, Bi melt and alloys was studied using coaxial cylinder high-temperature viscometer. The results showed that the curve of torsion-rotational speed for Sb melt presents a linear relation in all measured temperature ranges, whereas for the Bi melt, the curve presents obvious non-Newtonian feature within the low temperature range and at relative high shear stress. The rheology feature of Sb80Bi20 and Sb20Bi80 alloy melts was well correlated with that of Sb and Bi, respectively. It is considered that the rheology behavior of Sb melt plays a crucial role in Sb80Bi20 alloy and that of Bi melt plays a crucial role in Sb20Bi80 alloy.  相似文献   

14.
The effect of short-time aging in the temperature range between 400 and 1000 °C on the pitting corrosion behavior and mechanical property of a novel lean duplex stainless steel(LDSS) 2002 was investigated through the potentiostatic critical pitting temperature(CPT) tests and the Charpy impact tests. Both the pitting corrosion resistance and the toughness of aged specimens degraded due to the precipitation of detrimental secondary phases and the most significant reduction of CPT and impact energy emerged at 650 °C concurrently. The CPT of LDSS 2002 specimen aged at 650 °C decreased by 28 °C, and the impact energy dropped from 69 to 29 J/cm~2 compared with the solution-annealed sample. Transmission electron microscopy characterization showed that the main precipitates in LDSS 2002 were Cr_2N and M_(23)C_6 along the ferrite–austenite grain boundaries.  相似文献   

15.
《中国铸造》2014,(6):537-538
The invention provides a method of making a mold which can reduce SOx generation rate while preventing decrease in hardening rate in the case of using sulfuric acid for a hardener composition. The method has a mixture step in which fire-resistant particles, a hardener composition and a binder composition are mixed to obtain a composition for a mold. The hardener composition contains sulfuric acid. In the mixture step, sodium carbonate is added. A molar ratio of the sulfuric acid to the sodium carbonate is 0.5 or more and 4.0 or less.  相似文献   

16.
《中国铸造》2014,(6):542-546
China Foundry Week, hosted by the Foundry Institution of Chinese Mechanical Engineering Society (FICMES) each year, is a large academic event in China. It is one of the ten high-impact activities sponsored by the Chinese Mechanical Engineering Society.  相似文献   

17.
正1.Contents In order to promote the academic exchanges and technical communication of the research in the field of fluid power transmission and control,fluid control engineering specialized committee of the Chinese Society of Theoretical and Applied Mechanics will hold the 17th Conference of Hydrodynamic and Electromechanical Control Engineering on July 27-29,2014 in Tibet,Lhasa city.  相似文献   

18.
正The Transactions of Nonferrous Metals Society of China,founded in 1991 and sponsored by The Nonferrous Metals Society of China,is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology,including mineral processing,extraction metallurgy,metallic materials and heat treatments,metal working,physical metallurgy,powder metallurgy,with the emphasis  相似文献   

19.
Preface     
<正>We are pleased to present this Special Issue of Transactions of Nonferrous Metals Society of China containing selected papers from the First Asian Conference on Aluminum Alloys(ACAA-2013),held in Beijing,China,13–17 October 2013.This conference has been initiated,with approval of  相似文献   

20.
The Transactions of Nonferrous Metals Society of China, founded in 1991 and sponsored by The Nonferrous Metals Society of China, is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology, including mineral processing, extraction metallurgy, metallic materials and heat treatments, metal working, physical metallurgy, powder metallurgy, with the emphasis on fundamental science. It is the unique preeminent publication in English for scientists, engineers, under/post-graduates on the field of nonferrous metals industry. This journal is covered by many famous abstract/index systems and databases such as SCI Expanded, Ei Compendex Plus, 1NSPEC, CA, METADEX, AJ and JICST.  相似文献   

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