金属微孔网板微细电解加工技术研究

提出了采用微细圆柱群电极电解加工金属网板微孔的工艺方法.以电化学腐蚀法制备了直径(72 μm)一致的单排微细圆柱群电极,并用此群电极为工具阴极,进行了网板微孔的电解加工工艺试验,实现了金属微孔网板的稳定电解加工.     

电化学腐蚀法制备倒锥状微细电极的试验研究

以电化学腐蚀加工法为基础,提出了一种加工复杂形状微细电极的工艺方法.利用端面绝缘的方法改变阳极的局部导电性,使阳极和阴极之间的电场分布发生变化,从而得到倒锥状微细电极.通过试验成功地制备出倒锥状微细电极,并结合对比圆柱状电极进行了微孔电解加工试验,结果证明倒锥状电极在微孔电解加工中能获得更好的加工定域性.     

微细阵列群电极电解加工关键技术研究

提出了基于阴极优化的微细阵列圆柱凸台群电极电化学腐蚀加工法。根据电化学腐蚀基本原理,通过有限元方法分析计算群电极电化学腐蚀加工过程中的电极表面电场分布,以电流密度分布均匀性为目标,优化设计阴极形状,并进行阵列群电极制备。在制备出直径均匀的阵列群电极的基础上,探索用局部涂胶保护法制备大长径比的盘状阵列群电极,用于微细孔电解加工,进一步提高电解加工的定域性。     

综合改善微细电解加工精度的工艺研究

电解加工的阳极电化学溶解原理使其在微细加工领域具有巨大的发展潜力,但杂散腐蚀和流场条件恶劣制约加工精度的提高.分析了影响微细电解加工的主要因素,提出综合改善微细电解加工精度的工艺途径.理论分析和实验研究均表明:将LIGA工艺制备高质量微细阵列电极、电极侧壁绝缘、高频脉冲电流及非线性电解液加工、电极间歇回退伺服控制等方法有机结合,能有效约束电场、改善流场,提高微细电解加工的精度.     

微细硅工具电极的制备及其微细电解加工实验

提出了一种采用重掺杂单晶硅作为工具电极基体、二氧化硅/氮化硅作为绝缘层的硅工具电极用于微细电解加工。设计了利用体硅湿法腐蚀实现电极基体成形,化学气相沉积制备绝缘层的微细硅工具电极制备工艺。初步实验得到电极加工部尺寸约为100μm,绝缘层厚度为800 nm的硅工具电极。利用高速旋转的微细硅工具电极在18Cr Ni8材料上加工出了微细沟槽结构和微细通孔。实验结果验证了侧壁绝缘层对杂散腐蚀抑制作用的有效性。经过96 min的持续加工实验,电极绝缘层保持了可靠的绝缘效果。     

摩擦副表面微坑结构的微细电解加工技术研究

降低发动机的机械损失一直是研究热点,在摩擦副表面加工微坑,作为改善滑动摩擦的方法已引起了研究者的重视.提出了采用微细圆柱群电极电解加工微坑的工艺方法.以电火花反拷贝的方法制备了直径为250 μm的单排微细圆柱群电极,进行微坑的排电极电解加工工艺实验,获得了平均直径361 μm、深度7.8 μm的摩擦副表面微坑.     

微细电加工应用技术研究

微细电加工要达到工业应用的目的,需兼顾加工效率和加工精度两方面的要求.以微细孔、微细三维结构的加工为目标,进行了微细孔电火花加工、三维微细结构电火花伺服扫描加工及微细电化学加工技术的研究开发.设计出微细电极的损耗补偿进给和导向机构,开发出三维微细结构的电火花伺服扫描加工工艺,研究了采用阵列微细电极的微细电化学加工方法.微细孔电火花加工可连续加工直径小至100 μm的孔.伺服扫描电火花加工可便捷地在小于1 mm2区域内加工出三维微细结构.提出的微细电化学加工技术路线拟将微细电解加工应用于阵列微细孔和三维微细结构的加工.     

基于可重构方法设计的多功能微细电加工系统

简要介绍了可重构制造系统的概念和可重构机床的特点。基于可重构机床模块化的设计方法,设计了一套可进行微细电火花加工和微细电解加工的多功能微细电加工系统。在多功能系统中利用在线电解的方法制备微细钨电极,并用此电极进行电火花微细孔加工试验。     

微细轴的电加工技术

针对微细轴的加工问题，分析了当前普遍使用的特种加工方法。分别对线电极磨削、块电极反拷、单脉冲放电、电火花沉积、电解加工和电化学沉积等加工方法在微细轴加工方面的特点进行了归纳，并给出了具有代表性的加工实例。     

某型航空发动机燃油喷嘴旋流室的微细电解加工研究

针对某型航空发动机燃油喷嘴结构尺寸微小、材料硬度较高、切削加工困难等问题,介绍了微细电解加工的原理和实验装置,制备了微细棒状工具电极和三角形钩状成形电极,利用分层电解铣削进行粗加工快速去除工件多余材料,再利用环形扫描电解铣削进行旋流室全锥面的精加工,实现了发动机喷嘴微小尺寸旋流室的微细电解加工成形,达到加工精度和表面质量要求。研究表明,微细电解铣削加工是加工金属材料微小结构的有效可行的方法。     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

Rheology Feature of Simple Metal Melt

The rheology feature of Sb, Bi melt and alloys was studied using coaxial cylinder high-temperature viscometer. The results showed that the curve of torsion-rotational speed for Sb melt presents a linear relation in all measured temperature ranges, whereas for the Bi melt, the curve presents obvious non-Newtonian feature within the low temperature range and at relative high shear stress. The rheology feature of Sb80Bi20 and Sb20Bi80 alloy melts was well correlated with that of Sb and Bi, respectively. It is considered that the rheology behavior of Sb melt plays a crucial role in Sb80Bi20 alloy and that of Bi melt plays a crucial role in Sb20Bi80 alloy.     

Microstructures and Mechanical Properties of a Newly Developed Austenitic Heat Resistant Steel

The effect of heat treatment on the microstructures and mechanical properties of a newly developed austenitic heat resistant steel(named as T8 alloy) for ultra-supercritical applications have been studied. Results show that the main phases in the alloy after solution treatment are γ and primary MX. Subsequent aging treatment causes the precipitation of M_(23)C_6 carbides along the grain boundaries and a small number of nanoscale MX inside the grains. In addition, with increasing the aging temperature and time, the morphology of M_(23)C_6 carbides changes from semi-continuous chain to continuous network.Compared with a commercial HR3C alloy, T8 alloy has comparable tensile strength, but higher stress rupture strength. The dominant cracking mechanism of the alloy during tensile test at room temperature is transgranular, while at high temperature, intergranular cracking becomes the main cracking mode, which may be caused by the precipitation of continuous M_(23)C_6 carbides along the grain boundaries. Typical intergranular cracking is the dominant cracking mode of the alloy at all stress rupture tests.     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

The 15th Global Foundry Sourcing Conference 2014held in Qingdao China

Organized by Suppliers China Co., Ltd and co-organized by the National Technical Committee 54 on Foundry of Standardization Administration of China, the 15th Global Foundry Sourcing Conference 2014 （hereinafter referred to as FSC 2014） was successfully held on Sep. 23rd in Grand Regency Hotel, Qingdao. More than 500 delegates from home and abroad attended this conference, including over 130 purchasers from 20 countries and 380 domestic and foreign suppliers.     

Secondary Recrystallization Behaviors of Grain-Oriented 6.5 wt% Silicon Steel Sheets Produced by Rolling and Nitriding Processes

By rolling and nitriding processes, 0.23- to 0.3-mm-thick grain-oriented 6.5 wt% silicon steel sheets were produced. The core losses of grain-oriented 6.5 wt% silicon steel at frequencies ranging from 400 Hz to 20 k Hz were lower than that of the grain-oriented 3 wt% silicon steel with the same thickness by 16.6–35.8%. The secondary recrystallization behavior was investigated by scanning electron microscopy, energy-dispersive spectroscopy, and electron backscattered diffraction. The results show that the secondary recrystallization in high-silicon steel sheets develops more completely as the nitrogen content increases after nitriding, secondary recrystallized grain sizes become larger, and the sharpness of Goss texture increases. Because more {110}116 grains in the subsurface and the central layer of the sheets have a lot of 20°–45° high-energy boundaries in addition to Goss grains, {110}116 can be the main component through selective growth during secondary recrystallization when the inhibitor quantity is not enough and inhibitor intensity is weaker. The increases in nitrogen content can increase the inhibitor intensity and hinder abnormal growth of a mount of {110}116 grains and therefore enhance the sharpness of Goss texture.     

Laser Cladded TiCN Coatings on the Surface of Titanium

Laser cladded coatings of TiCN were produced on the surface of titanium. To obtain the optimal techniques, several conditions were tested by varying the laser scanning rate. The choice of shielding gas was also studied. The cladded coatings were then evaluated from the surface mechanics point of view based on their microhardness. The microstructure of some interesting samples was investigated by optical micrographs (OM). The results showed that under the condition of fixed pulse frequency and pulse width, the laser scanning rate and the shielding gas are the main factors influencing the components of coatings. TiCN coatings were decompounded and oxidized during the cladding process in the condition of no shielding gas of N2. X-ray diffraction results indicated that the composite coatings composed of TiCN, TiC, Ti2N, and TiO2 were produced using appropriate techniques. The results indicated that the best condition in terms of the surface microhardness is obtained when the scanning rate is 1.5mm / s, the pulse frequency is 15Hz, the pulse width is 3.0ms, and N2 is chosen as the shielding gas. The microhardness of the composite coatings is about 1331kg · mm - 2, which is about 4 times that of the substrate. The optical micrographs indicated that the cladding zone is made up of TiCN, TiO2, and some interdendritic Ti, but the diffusion zone mainly consists of the dendrites phase, and the cladded depth is about 80?滋m, which is more than 2 times that of the laser nitrided sample. There were no microcracks or air bubbles in the cladded sample, which was cladded using the above optimal techniques.     

Effect of Short-Time Aging on the Pitting Corrosion Behavior of a Novel Lean Duplex Stainless Steel 2002

The effect of short-time aging in the temperature range between 400 and 1000 °C on the pitting corrosion behavior and mechanical property of a novel lean duplex stainless steel(LDSS) 2002 was investigated through the potentiostatic critical pitting temperature(CPT) tests and the Charpy impact tests. Both the pitting corrosion resistance and the toughness of aged specimens degraded due to the precipitation of detrimental secondary phases and the most significant reduction of CPT and impact energy emerged at 650 °C concurrently. The CPT of LDSS 2002 specimen aged at 650 °C decreased by 28 °C, and the impact energy dropped from 69 to 29 J/cm~2 compared with the solution-annealed sample. Transmission electron microscopy characterization showed that the main precipitates in LDSS 2002 were Cr_2N and M_(23)C_6 along the ferrite–austenite grain boundaries.     

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正The Transactions of Nonferrous Metals Society of China,founded in 1991 and sponsored by The Nonferrous Metals Society of China,is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology,including mineral processing,extraction metallurgy,metallic materials and heat treatments,metal working,physical metallurgy,powder metallurgy,with the emphasis