烟道流量计量标准装置

为了解决我国烟道流量计的量值溯源问题,中国计量科学研究院建立了烟道流量计量标准装置。装置使用可溯源至标准转盘的激光多普勒测速仪作为原级标准器,采用激光多普勒流速剖面扫描和超声流量计波动修正的方式测量标准流量,经校准的8声道超声流量计为工作级标准表,具备了908~104840m3/h的测量能力,扩展不确定度为0.62%(k=2),可对最大口径为1m的流量计进行校准。装置下游测试段包括圆形管段和矩形管段,能够开展烟道流量计测量性能的研究。     

Effects of different carbon sources and C/N values on nonvolatile taste components of Pleurotus eryngii

Pleurotus eryngii, the second largest industrial cultivation mushroom in China, is usually cultivated on substrates mainly consisting of sawdust and corncob. In this study, experiments were performed to determine the effects of different carbon sources and C/N values on nonvolatile taste components of P. eryngii. The effects of different carbon sources on nonvolatile taste components levels revealed that sawdust was beneficial to high levels of crude protein, amino acids, 5′‐nucleotides and equivalent umami concentration, while corncob was beneficial to high contents of carbohydrate, polysaccharides and trehalose. At the similar C/N values, relatively higher sawdust content was beneficial to umami amino acid production, while relatively higher corncob content was beneficial to high contents of carbohydrate, polysaccharides and mannitol. Higher C/N value was beneficial to high levels of crude protein, amino acids, 5′‐nucleotides and equivalent umami concentration, while lower C/N value was beneficial to high contents of carbohydrate, polysaccharides and trehalose. These results provided information for P. eryngii fruit body industrial cultivation to obtain specific nonvolatile taste components with high levels.     

Effect of substituent carboxylic group on the self-assembly of cadmium coordination polymers: Syntheses,topological analyses and photoluminescence properties

Two coordination polymers, formulated as {[Cd(1,4-BDC)(ppene)]·CH₃CN}_n (1) and [Cd(H₂O)(1,2,4-HBTC)(ppene)_0.5]_n (2) have been synthesized through the solvothermal reactions between Cd(NO₃)₂·4H₂O and 4-pyr-poly-2-ene (ppene) in the presence of 1,4-benzenedicarboxylic acid (1,4-H₂BDC) or its derivative 1,2,4-benzenetricarboxylic acid (1,2,4-H₃BTC). These two compounds were structurally characterized by infrared spectroscopy, elemental analysis, single crystal X-ray diffraction and powder X-ray diffraction. Compound 1 exhibits a three-dimensional two-fold interpenetrating 4¹²6³-pcu network. The coordination network of 2 shows a three-dimensional (4,5)-connected framework with rare (4⁴6²)(4⁴6⁶) tcs topology. Owing to the linkage of hydrogen bonding interactions between protonated carboxylic groups, 2 further displays a three-dimensional (5,5)-connected supramolecular network with an unprecedented Schläfli symbol (4⁸6²)(4⁶6⁴). Thermal stability and photoluminescence properties of 1 and 2 were also investigated.     

车辆悬架用电磁执行器的建模与试验研究

应用电磁感应的基本原理,设计了一种新型的车辆主动悬架用电磁直线执行器,该执行器具有响应快,出力大和动行程大的特点。通过两种不同的建模手段,即有限元建模和集总元件动力学建模的电磁力仿真对比分析,两者基本吻合,表明了执行器模型的准确性。利用所建立的有限元模型,研究了执行器结构参数如气隙厚度和次级铜层厚度对电磁力的影响规律,并选取合理的参数进行执行器的样件试制。通过对加工后的样机模型进行电磁力响应的试验测试,并分别与有限元模型和集总元件动力学数学模型进行相应的比较,试验数据与仿真结果基本一致,进一步验证了模型的准确性。     

Simulation Method of Dynamic Characteristics of Turbine Flow Sensor

Computational Fluid Dynamics (CFD) simulation is one of the important methods to study the performance and in-fluencing factors of turbine flow sensors. According to the working characteristics of the turbine flow sensor, the passive simulation method based on the six degrees of freedom (6-DOF) model and dynamic mesh is proposed in this paper. The reliability of the simulation method is verified by steady-state experiments and unsteady-state experiments. The results show that the trend of meter factor with flow rate acquired from the simulation is close to the experimental results, and the deviation between the simulation result and the experiment result is low with a maximum deviation of 2.88%. In the unsteady simulation study, the impeller speed changes with the inlet velocity of the turbine flow sensor, which has a good follow-up. The passive simulation method can be used to predict the dynamic performance of the turbine flow sensor.     

固相萃取净化-气相色谱-质谱法测定染料中7种指示性多氯联苯

本文建立了以固相萃取(SPE)前处理净化、结合气相色谱-质谱(GC-MS)测定染料中7种指示性多氯联苯的分析方法。该法将染料样品经溶剂萃取后,通过固相萃取(SPE)净化、浓缩,气相色谱-质谱采用选择离子监测模式(SIM)测定,以保留时间和特征离子定性,外标法定量。     

基于QEMU的外部总线仿真技术

综合嵌入式系统通过外部总线实现各个子系统之间的通信连接。为解决综合嵌入式系统的接口测试问题,采用系统虚拟机仿真综合嵌入式系统的连接方式,通过在虚拟机中创建外部总线仿真模块,配置仿真模块的连接,从而实现虚拟机之间的通信。提出一种基于以太网通信的外部总线仿真结构,以CAN总线仿真为例,在全系统虚拟机QEMU的内部总线上配置与注册外部总线设备,为读写总线设备数据的接口建立共享内存,组织总线协议报文。实验结果表明,通过网络收发报文,可实现总线仿真节点模块之间的数据交换,从而达到仿真总线的数据通信功能。