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Lignin‐based wood adhesives are obtained that satisfy the requirements of relevant international standards for the manufacture of exterior‐grade wood particleboard. Formulations based on low molecular mass lignin and presenting an increase in the relative proportion of reactive points yield better results than the higher molecular mass lignin used in the past. These lignins allow a higher proportion of hydroxymethylation during preparation of methylolated lignins. These lignin‐based adhesives also yield acceptable results at particleboard pressing times that are sufficiently low to be of industrial significance. Lignin‐based wood adhesives, in which a nonvolatile nontoxic aldehyde (glyoxal) is substituted for formaldehyde in their preparation, are prepared and tested for application to wood panels such as particleboard. The adhesives yield good internal bond strength results for the panels, which are good enough to comfortably pass relevant international standard specifications for exterior‐grade panels. The adhesives also show sufficient reactivity to yield panels in press times comparable to that of formaldehyde‐based commercial adhesives. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 1690–1699, 2007 相似文献
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乙二醛对淀粉/低密度聚乙烯/黄麻纤维复合材料性能的影响 总被引:1,自引:0,他引:1
通过熔融共混法制备淀粉/低密度聚乙烯/黄麻纤维复合材料(S/LDPE/F).考察乙二醛的加入对复合材料拉伸性能和耐水性的影响.结果表明:乙二醛的加入有效地提高了复合材料的拉伸强度,当乙二醛的加入量为5%(质量分数)、压片反应时间为5min时,拉伸强度达到21.5 MPa,比相同条件下制备的未加乙二醛的复合材料拉伸强度(6.25 MPa)提高了244%;加入乙二醛后复合材料的耐水性也有所提高;XRD结果显示:加入乙二醛后淀粉的结晶被进一步破坏.拉伸断口扫描电镜照片表明:乙二醛的加入使黄麻和塑化后淀粉之间的界面结合得到了改善. 相似文献
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利用报废的液体推进剂硝酸-27S和乙醛制备乙二醛。比较了硝酸法和硝酸-27S氧化法对产品乙二醛收率的影响,对反应工艺条件进行了研究,确定了利用硝酸-27S作氧化剂制备乙二醛的较适宜工艺条件,并对测定乙二醛的国标法进行了改进,提出利用紫外分光光度法可快速测定其含量,实验表明硝酸-27S氧化法制锵的乙二醛收率高于硝酸氧化法。较适宜的工艺条件为:反应温度40%左右,硝酸-27S滴加时间1-1.5h,反应时间2h,n(硝酸.27S):n(乙醛)=1:1,用亚硝酸钠作催化剂,乙二醛收率可达45%以上。 相似文献
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Cross‐linked zein has been produced using glyoxal (GLY) as the cross‐linking reagent via reactive extrusion for the first time in a twin screw extruder using dilute sodium hydroxide as catalyst. Tri(ethylene glycol) was used as a plasticizer for various items. The extrudate was then ground and processed using either compression or injection molding. At the highest level of GLY (6%), tri(ethylene glycol) was used at 10% as a plasticizer to allow further processing to take place. With this formulation, samples could be obtained from the injection mold, however, the samples did not hold their molded shape due to the elasticity of the sample at the mold temperature. When lower levels of GLY were used, injection molded sample bars of similar quality to control were obtained. The physical properties of these samples were similar to control. At GLY levels of 1.75% and higher, the samples were resistant to dissolution by acetic acid. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009 相似文献
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用双氧水/乙二醛对真丝绸低温染色 总被引:1,自引:0,他引:1
本文就双氧水/乙二醛氧化还原系统,对蚕丝织物低温染色进行了研究。讨论了影响染色的若干因素,并制定了可行的染色工艺,在染色机理方面也作了初步探讨。 相似文献