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91.
Na+、K+离子交换对Co-Mo/MCM-41加氢脱硫催化剂的影响 总被引:1,自引:1,他引:0
用偏硅酸钠和正硅酸乙酯作硅源制备了MCM-41(分别记作MCM-41(S)和MCM-41(T))分子筛,并用Na2C2O4和K2C2O4对MCM-41(S)进行了碱金属离子交换改性。以质量分数0.8 %的二苯并噻吩(DBT)的十氢萘溶液为模型化合物,考察了不同MCM-41担载的Co-Mo硫化物催化剂对DBT的加氢脱硫反应性能。结果表明,MCM-41担载的Co-Mo催化剂加氢活性较低,DBT主要通过直接脱硫反应路径脱硫。其活性顺序为:Co-Mo/MCM-41(T)>Co-Mo/MCM-41(S)>Co-Mo/MCM-41(K)>Co-Mo/MCM-41(Na)。UV-Vis结果表明,部分Co与MCM-41(S)中少量Al发生相互作用,生成了CoAl2O4,是造成Co-Mo/MCM-41(S)活性降低的重要因素。而在Co-Mo/MCM-41(K)和Co-Mo/MCM-41(Na)中,除CoAl2O4物种之外,碱金属的引入还促进了Co3O4物种的形成,使其活性进一步降低。 相似文献
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93.
丝网气液分离器分离性能和压力损失分析 总被引:3,自引:0,他引:3
对丝网气液分离器的分离机理进行了详细分析,在此基础上给出了丝网气液分离器的分离效率和压降计算公式。与HG/T 21618-1998《丝网除沫器》中的公式相比,此公式可以用于任意组合的丝网结构,更具普适性,并且能定量分析各种分离机理对分离的贡献。对丝网式空气过滤器计算的结果表明,此公式具有很好的精度,可以用于工程设计。 相似文献
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The objective of this study was to compare methane production and characteristics of digested material in anaerobic digestion concepts according to the Animal By-Products Regulation (ABP-Regulation) of the EC (hygienisation of biowaste for 1 hour at 70 degrees C, particle size < 12 mm) and Finnish national regulations (treatment temperature 55 degrees C, feeding interval 24 h, hydraulic retention time (HRT) 20 d, particle size < 40 mm) and with small variations in treatment methods for treating manure and biowaste. Moreover, the survival of three different salmonella bacteria in these processes was studied. Hygienisation of biowaste prior to digestion at 35 degrees C enhanced methane production by 14-18% compared to similar treatment without hygienisation. The differences in treatment temperature, HRT and hygienisation of biowaste prior to digestion did not significantly affect the characteristics of digested material. The concepts according to the ABP-Regulation and Finnish national regulations were effective in destroying salmonella bacteria to an undetectable level. 相似文献
96.
设计并实现了一种基于FPGA的四进制连续相位调制器(PCM)。该调制器的基带调制模块通过查表法实现,复杂度较低。仿真结果验证了设计的正确性。 相似文献
97.
文章采用一种新颖方法对商用IP进行可靠性提升、完善,同时进行容错结构设计,建立了拥有自主知识产权的专用加固型标准单元库,构建了面向空间应用的SoC设计方法与流程,形成了面向空间电子系统的系统集成设计平台,用该技术实现了面向卫星等空间应用的32位嵌入式RISC处理器SoC芯片,获得了一次投片成功。 相似文献
98.
99.
Jean-Fran?ois Blais Nathalie Meunier Guy Mercier Patrick Drogui Rajeshwar Dayal Tyagi 《Canadian Metallurgical Quarterly》2004,130(5):516-525
This research is related to a preindustrial pilot scale study of the performance of the simultaneous sewage sludge digestion and metal leaching (SSDML) process for decontamination and stabilization of sewage sludge. Ten batch tests were carried out in two 4?m3 bioreactors under various conditions of operation. Results indicated that the addition of 1.0 to 1.5?g?S0/L, which is the equivalent of approximately 30 to 50?kg?S0 per tons dry sludge, is sufficient to obtain conditions of acidity (pH<2.5) and oxido-reduction potential greater than 500 mV necessary for an effective solubilization of toxic metals. The final average of metal solubilization in the output sludge during the SSDML process varied in the following ranges: 25–78% Cd, 9–32% Cr, 48–100% Cu, 77–99% Mn, 15–53% Ni, 12–47% Pb, and 66–100% Zn. The N, P, and K contents were also preserved in the decontaminated sludge. Moreover, the use of low concentrations of elemental sulfur makes it possible to obtain decontaminated sludge with a low total sulfur content (1.4–1.5% S) compatible with agricultural use. The suspended solids removal calculated for the SSDML process was slightly lower, (2.5±0.4)% volatile suspended solids per day, than those reached using standard aerobic digestion. Finally, the SSDML process was found to be effective in removing bad odors and in the destruction (99–100%) of indicator bacteria. 相似文献
100.
The vapour phase compositions of a series of pack powder mixtures containing elemental Al and Hf or W powders as depositing sources and CrCl3·6H2O or AlF3or CrF3as activators were analysed in an attempt to further develop the pack cementation process to codeposit Al and Hf or W to form diffusion coatings on nickel base superalloys. The results suggested that Al could be codeposited with Hf, but not with W, from the vapour phase. Compared with both AlF3and CrF3, CrCl3·6H2O has been shown to be a more suitable activator for codepositing Al with Hf. The optimum coating temperature was identified to be in the range of 1050°C to 1150°C. Based on the thermochemical analysis, a series of coating deposition studies were undertaken, which confirmed that codeposition of Al and Hf could be achieved at a deposition temperature of 1100°C in the CrCl3·6H2O activated packs containing elemental Al and Hf powders. The coating obtained had a multilayer structure consisting of a Ni7Hf6Al16top layer and a NiAl layer underneath, followed by a diffusion zone, which revealed that the coating was formed by the outward Ni diffusion. It is suggested that the compositions suitable for codeposition of Al and Hf could be effectively identified by comparing the vapour pressures of HfCl4and HfCl3with that of AlCl in the packs activated by chloride salts. It has also been experimentally demonstrated that, although W could not be deposited from the vapour phase, a high volume of fine W particles can be entrapped into the outer NiAl coating layer formed by the outward Ni diffusion using a modified pack configuration. This leads to the formation of a composite coating layer with W particles evenly distributed in a matrix of NiAl. It is suggested that this modified pack process could be similarly applied to develop nickel aluminide coatings containing other refractory metals that may not be codeposited with Al from the vapour phase. 相似文献