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991.
992.
研究了以醋酸钴和醋酸锰为催化剂、氢溴酸为促进剂,在169~192 ℃下对甲基苯甲酸(p-TA)的液相氧化反应动力学.采用幂函数动力学模型对实验数据进行了拟合.结果表明,对甲基苯甲酸液相氧化反应是串联反应,甲基苯甲酸和中间产物对羧基苯甲醛的反应级数均为1.拟合得到的活化能数据表明对甲基苯甲酸氧化为整个反应的控制步骤.利用该动力学模型能够成功预测186 ℃下液相组分随时间的变化趋势.实验表明,当金属离子的配比满足[Co2 ]/[Mn2 ]为3∶1时,催化剂具有最高的活性. 相似文献
993.
994.
Preparation and characterization of porous carbon beads and their application in dispersing small metal crystallites 总被引:2,自引:0,他引:2
Porous carbon beads were prepared by the pyrolysis of poly(vinylidene chloride) beads that were synthesized by suspension polymerization. After prolysis treatment at 180–300 °C under argon stream, the polymeric beads were further carbonized at 1000 °C for 3 h under argon stream to acquire porous carbon beads, of which the specific surface area was about 1000 m2/g, and pore size was mainly in the width range of 0.8–1.2 nm. The carbon structure and surface chemical composition characterized by X-ray diffraction and X-ray photoelectron spectroscopy, depended on the preparation temperature and the relations between them were examined. The characterization of the carbon beads by scanning electron microscopy, atomic force microscopy presented the morphological structure of the carbon beads surface and a global view of pores. The dispersion of nickel crystallites on the carbon beads surface was characterized by electron microprobe analysis. This study reveals that uniform surface morphological structure leads to the fine dispersion of metal crystallites. 相似文献
995.
This paper focuses on the design of a low order robust stabilizer for the tracking/disturbance rejection problem based on the internal model principle in the time-varying setting and its application to the hydraulic pressure tracking with varying frequency. The problem of this kind known as output regulation generally consists of two major parts: internal model unit construction and stabilizer design. While the construction of the time-varying internal model unit is non-trivial by itself and a very recent research outcome enables its synthesis for a class of linear time-varying systems, the effective stabilization of the augmented system (internal model unit and plant) for practical applications remains a challenge. This is due to the need to stabilize the high order time-varying augmented system using a low order stabilizer in a robust fashion and with desirable transient performance. While directly applying the stabilization approaches for a general LTV system will result in a high order stabilizer, a new method is proposed in this paper that overcomes this bottleneck by taking advantage of the unique structure of the internal model based control system. Instead of using a dynamic stabilizer with high order, this approach uses a sequence of time-varying gains that are directly injected into the internal model unit. A critical issue addressed is how to avoid the non-convex optimization associated with the time-varying gain synthesis and then convert the stabilizer design into a series of Linear Matrix Inequalities (LMIs). The proposed control approach is then demonstrated on an electrohydraulic system. 相似文献
996.
A bridge crane is a complicated nonlinear underactuated mechatronic system, for which high-speed positioning and anti-swing control is the kernel objective. Existing methods for varying cable length cranes require either linearizations or approximations, when performing analysis, and they usually assume small load swing; moreover, the ranges of the tracking errors cannot be guaranteed during the overall process. Motivated by these facts, we present a new tracking scheme for cranes with load horizontal transportation and lowering control, which achieves simultaneous load swing suppression and elimination. To the best of our knowledge, the proposed method yields the first feedback closed-loop control result not needing linearization or approximation operations to the original nonlinear crane dynamics with cable length variation, while relaxing the common assumption imposed on load swing associated with existing methods. It can also guarantee that the tracking errors are always within a priori set bounds and converge to zero rapidly. Lyapunov-like analysis is implemented to support the theoretical derivations. We carry out hardware experiments to illustrate the superior control performance of the new method. 相似文献
997.
In the present paper, we investigate the output-controllability and optimal output control problems of a state-dependent switched Boolean control network. By using the semi-tensor product, the algebraic form of the system is obtained. Then, output-controllability problems of the system are discussed and some necessary and sufficient conditions are given. Next, the Mayer-type optimal output control issue is considered and an algorithm is provided to find out the control sequence. At last, an example is given to show the effectiveness of the main results. 相似文献
998.
With a combined compact difference scheme for the spatial discretization and the Crank–Nicolson scheme for the temporal discretization, respectively, a high-order alternating direction implicit method (ADI) is proposed for solving unsteady two dimensional convection–diffusion equations. The method is sixth-order accurate in space and second-order accurate in time. The resulting matrix at each ADI computation step corresponds to a triple-tridiagonal system which can be effectively solved with a considerable saving in computing time. In practice, Richardson extrapolation is exploited to increase the temporal accuracy. The unconditional stability is proved by means of Fourier analysis for two dimensional convection–diffusion problems with periodic boundary conditions. Numerical experiments are conducted to demonstrate the efficiency of the proposed method. Moreover, the present method preserves the higher order accuracy for convection-dominated problems. 相似文献
999.
本文采用气相色谱法分析乳氟禾草灵的含量,选用OV-17固定液,Gas-ChromQ为担体制备色谱柱,以苯二甲酸二正戊酯为内标物。方法的标准偏差为0.31,变异系数为0.34%,乳氟禾草灵的回收率在99.21-100.70%之间。 相似文献
1000.
由成都建筑材料工业设计研究院有限公司(简称成都院)和中国建材装备有限公司组成联合体总承包的UCC 10 000 t/d熟料水泥生产线,成都院负责提供合同范围内所有的工程设计、核心技术及核心设备、现场管理、人员培训、生产线达标考核,并具体负责实施和完成所有的土建及安装工程。在总承包工程建设的过程管理中,成都院以设计为灵魂,贯彻了"工艺流程顺畅,总图布局合理,系统配置先进可靠,合理节省投资"的设计理念;成都院克服了要求高、工期短、气候条件恶劣、国外施工人员管理难度大、功效低等重重困难,按时、保质保量、安全地完成了土建、安装、调试和试车任务;2007年4月26日,该生产线一次性通过业主的达标考核。我们的经验是:(1)有专业设计院全面介入的工程总承包是项目顺利进行的可靠保证;(2)参与建设的相关单位要相互信任、相互配合、目标一致;(3)工程建设管理科学化、人性化很重要。该项目的成功建设,使成都院总包工程建设的过程管理更加正规化、合理化和科学化。 相似文献