铜及铜合金中铜量分析方法综述

现行标准ＧＢ５２３１－ＧＢ５２３５－８５中共有８８个合金牌号要求测定铜量，其含铜量从５３％到９９．９７％以上。本文就ＩＳＯ、ＧＢ和主要铜材生产企业分析规程中铜量测定方法，结合本人的实践经验进行综述。     

克拉玛依原油中各组分的乳化性质

用沉淀法和色谱分离法将克拉玛依原油分离成沥青质，极性物和抽余油三组分，红外光谱分析表明，沥青质和极性物中存在一些含氧官能团的羧酸类或酚类以及含氮化合物，而抽余油则主要为烃类物质，因而沥青质和极性物的界面活性大于抽余油，沥青质具有较强的油包水（W／O）乳化能力，是造成克拉玛依原油W／O乳化的主要组分，极性物具有较强的水包油（O／W）乳化能力，是造成克拉玛依原油O／W乳化的主要组分，抽余油的乳化能力很弱。     

HG-ICP-MS同时测定复杂样品中的痕量AS,Se,Hg

HG-ICP-MS方法中利用HNO3作为样品溶液的酸介质,用实验室自制的二级气液分离器代替易消耗的膜分离器,在优化的实验条件下实现了As,Se,Hg的同时测定,分别获得了0.022,0.016,0.009ng/ml的检测限;并且避免了Cl对测定的质谱干扰.试验研究了样品酸度,NaBH4浓度,载气流速和引入方式等因素对测定灵敏度和稳定性的影响,以及二级气液分离器中的气液分离行为.回收率试验的结果表明,HG-ICP-MS同时测定As,Se,Hg的主要干扰来自于成氢化物元素之间,以及Fe,Cu等过渡金属离子.样品溶液中Vc-硫脲的加入可以很好地掩蔽这些离子的干扰,利用HG-ICP-MS方法测定人发,灌木叶和大米粉标样中痕量的As,Se,Hg,结果与标准参考值相符.     

Impacts of green roofs and rain water use on the water balance and groundwater levels in urban areas

Ohne Zusammenfassung

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Impacts of green roofs and rain water use on the water balance and groundwater levels in urban areas

     

崇礼东坪黄金公司缓倾斜薄矿体采空区综合治理

在采空区调查的基础上,以FLAC工程力学分析软件为手段,应用“诱导崩落和封闭采空区综合治理”理论,进行缓倾斜薄矿体采空区综合治理研究.该项研究与实践为缓薄矿体采空区综合治理提供了可供借鉴的经验,并为矿山创造了可观的经济效益.     

黄河三角洲河口地区土地利用及生态环境景观分析

通过人机交互解译1996年和2004年TM影像得到2期土地利用数据,求得到土地利用转移矩阵和各种生态环境景观指数。通过分析两期土地利用及景观结构指数之间的差异性,指出由自然和人为原因引起的生态环境的变化:研究区总面积有所减少,盐碱地改良后用于了鱼虾养殖,部分未利用地和水域盐碱化,区域景观类型丰富且均匀,局部破碎严重。     

Two closely related adenovirus genome types with kidney or respiratory tract tropism differ in their binding to epithelial cells of various origins

The host cell interactions of the genome types Ad11p and Ad11a of human adenovirus serotype 11, displaying kidney or respiratory tropism, were compared using FACS analysis. Kinetic experiments indicated that the virus binding stated immediately and reached a plateau after 30 min. The binding of biotinylated virions to seven continuous cell lines. A549, A498, J82, HeLa, CHO, MDCK, and human diploid fibroblasts (HEDF), was quantitated by FACS analysis. The binding capacities of the two viruses to all human cell lines but A549 cells appeared to differ. Ad11p virions manifested high affinities, whereas Ad11a virions presented low affinities. Neither of the two viruses bound to CHO or MDCK cells. Reciprocal competition experiments showed that the Ad11a virions could be weakly blocked by the Ad11p virions, whereas the Ad11p virions could not be competed at all by the Ad11a virions. The binding of the Ad11p virions to cells could be blocked by the rfiber antiserum of Ad11p, but not by the corresponding antiserum against Ad11a or Ad35p. A comparison of the cytopathogenicity of the seven cell lines infected by Ad11p and Ad11a demonstrated that the efficiency of the initial event of an adenovirus infection directly affects the outcome of the viral infection. The Ad11a in the A498, J82, HeLa, or HEDF cells that presented lower affinity and receptor concentration showed 100 times less infectivity than that in A549 cells displaying high affinity and receptor concentration. These results indicate that the cell susceptibility to Ad11p and Ad11a infection strongly depends on both the number of fiber receptors on the host cells and the receptor affinity for ligands on the fiber knob. Our findings also suggest that the receptors for Ad11p and Ad11a on the surface of different cell types may be different or on different sites.     

新型高性能脉冲峰值保持电路

本文介绍了两种新型跨导型脉冲峰值保持器，分别用于多丝正比室（ＭＷＰＣ）和复合晶体闪烁探测器（Ｐｈｏｓｗｉｃｈ）输出脉冲信号的形状和幅度分析。电路的跨导放大级采用跨导型集成运算放大器，使电路结构简单化，且性能优良可靠，能响应输入脉冲最小上升时间分别为５０ｎｓ（Ｐｈｏｓｗｉｃｈ）和５００ｎｓ（ＭＷＰＣ）的信号，在４０ｄＢ的动态范围内，两电路的积分非线性均好于０．１％，特别适用于空间γ射线观测。     

A ctivation measurement of neutron distribution in intermediate energy heavy ion target area

The distribution of neutrons produced by the reaction of 50MeV/u ^12C-ion on a thick Cu target are studied.The neutrons are measured with threshold activation detectors.Al.F,C,Al and In activation samples were used to measure neutrons with energy greater than 7,11,20,50MeV and thermal neutrons,respectively,The fluence rate,energy and angular distributions of neutrons,total neutron yield of 12C-ion and the emission rate in the forward direction of neutrons over 11 and 20MeV were obtained.     

高可用性舰船网络系统研究

随着舰船信息系统网络化应用的不断增加,信息系统对舰船网络的依赖性也在不断增强,这对网络持续提供服务的高可用能力提出了更高的要求。鉴于目前舰船网络系统的可用性不能满足舰船信息业务对数据中断恢复时间所提出的要求,将最新的商用高可用性IRF2技术引入舰船网络系统,提出了一种新的舰船网络系统方案。该方案采用双交换机堆叠及跨交换机链路聚合的方式实现网络的网关冗余和路径冗余,简化了网络的逻辑结构,提高了整网的故障恢复时间。通过搭建的原型系统对方案的重要参数进行了测试,结果表明：相比于目前的舰船网络,该方案提升了网络效率,并将故障倒换时间从秒级缩短到了50ms级。