The structure of noncrystalline, chemically vapour-deposited boron fibres was investigated by computer modelling the experimentally obtained X-ray diffraction patterns. The diffraction patterns from the models were computed using the Debye scattering equation. The modelling was done utilizing the minimum nearest-neighbour distance, the density of the model, and the broadening and relative intensity of the various peaks as boundary conditions. The results suggest that the fibres consist of a continuous network of randomly oriented regions of local atomic order, about 2 nm in diameter, containing boron atoms arranged in icosahedra. Approximately half of these regions have a tetragonal structure and the remaining half a distorted rhombohedral structure. The model also indicates the presence of many partial icosahedra and loose atoms not associated with any icosahedra. The partial icosahedra and loose atoms indicated in the present model are in agreement with the relaxing sub-units which have been suggested to explain the anelastic behaviour of fibre boron and the loosely bound boron atoms which have been postulated to explain the strengthening mechanism in boron fibres during thermal treatment. 相似文献
Summary Monomeric Bis-(4-hydroxybutyl) terephthalate has been synthesized and characterized. Titanium iso-propoxide has been found to be a superior catalyst for transesterification compared to metal acetates. Further polycondensation of Bis (HBT) yields poly (1,4-butylene terephthalate). The effect of various titanium derived catalysts on the polycondensation of Bis (HBT) has been studied. The catalytic efficiency of these derivatives is ascribed to their relative hydrolytic stability and the degree of interaction between the carbonyl oxygen and the metal. 相似文献
This paper describes unusual applications of ultrasound that are based upon recent advances in transduction efficiency in
air and gaseous media. Piezoelectric transducer devices – capable of generating extremely high intensity ultrasound in ambient
air up to 5 MHz – have been successfully developed and tested. This is in addition to the obvious uses for gas analysis, remote
sensing, liquid level, gap, and thickness measurement, and proximity analysis. These new generation transducers make it possible
to analyze solids and liquids not only non-destructively, but also without physically contacting the test sample. Among various
applications to the non-destructive characterization (NDC) of industrial materials, we also describe the feasibility of a
forensic application. This concerns the detection of objects such as knives, guns, contraband drugs, dead bodies, etc., hidden
inside false compartments or walls.
Received: 15 October 1997 / Accepted: 24 October 1997 相似文献
Changes in techno-functional properties of buffalo milk were evaluated due to variation in calcium content. Decalcification resulted in significant variation in ζ-potential, casein size, colour and ηapp. However, calcium addition only influenced ζ-potential of milk. In case of acid gelation, the time and temperature required for coagulation decreased significantly for both calcium-depleted and -added milks. However, during chymosin gelation, only 20%–30% of calcium-depleted milk coagulated with an increased clotting time. Furthermore, calcium addition increased firmness, consistency and cohesiveness of both chymosin and acid-induced gelation. 相似文献
Silicon - In this study, an innovative one part, solution free concept applied for the development of hybrid inorganic–organic geopolymeric precursors having Si-O-Al networks at the precursor... 相似文献
The proposed system portrays the application space examination of a diverse cryptosystem processor with dynamic reconfiguration abilities. It is appropriate to a variety of signal processing application domains namely telecommunications, image processing, video coding and cryptographic processing. To differentiate between application spaces of the processor, the performance is correlated with cutting edge devices, taking ability to program, energy efficiency and computational potential as the important factors. In general the conventional method of computation is processed by means of Virtual Secure Circuit (VSC) on Advanced Encryption Standard (AES) and performance of the device Field Programmable Gate Array (FPGA) after implementation is analyzed in terms of delay and throughput. In the conventional method area overhead and power consumption are less where as the architecture lags in performance and throughput. It has been overcome through the fully parallel pipelined Architecture of the VSC on AES which outperforms the existing method in terms of performance and throughput. The energy efficiency and performance are considerably more important than processor that are used for general purpose, while still preserving a Convenient approach of programming that mainly bank on software oriented languages. The exploit of VSC based AES is to formulate the cryptographic processor held against Side Channel Attacks like attacks based on power supply and electromagnetic signals. Then the experimental result shows the promising outcomes when compared to previous methods.
Persistent scatterer interferometry (PSI) is a major advancement in radar interferometry for detecting and monitoring land deformation. PSI is the most advanced class of differential interferometric synthetic aperture radar (DInSAR) techniques. The technique conquers the main drawbacks of the conventional DInSAR technique by identifying radar targets having stable backscattering characteristics in time. These targets are termed as persistent scatterers (PSs). The higher the number of PSs for a study area the higher the accuracy of the results will be, which is most common for deformation analysis in urban areas. However, for non-urban or highly de-correlated areas, PSs density collapses significantly, which needs to increase for optimal results. For this purpose, partially coherent/distributed scatterers (DSs) are being exploited in addition to the PSs. The field surface of this study is one of the copper-rich mining belts in India, which consists of two major underground metal mines. Scatterer characterziation of the field surface under study suggests that most of the scatterers are DSs and very few scatterers under the influence of the mining zone are PSs. In addition to this, a preliminary investigation of deformation characteristics of the field surface under study reveals that the spatial extent of deformation is small/localized along with slow and non-linear deformation. Keeping in view scatterer and deformation characteristics of the field surface under study, in this research paper, a Quasi-Persistent Scatterer based PSI approach has been applied using high-resolution TerraSAR-X interferometric data stack (10 images) to generate deformation time series and deformation velocity. Furthermore, results obtained from the applied PSI approach and ground-based observations (using GNSS) have shown good agreement with each other, in the order of ?5.20?mm/year (LOS) and ?5.38?mm/year (subsiding), respectively. 相似文献