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991.
Jun Yang Jianbao Li Hong Lin Xiaozhan Yang Xuguang Tong Gangfeng Guo 《Journal of Applied Electrochemistry》2006,36(8):945-950
In this paper, we describe the preparation of a porous nanosheet-stacked NiCo2O4 composite electrode using a novel electrophoretic deposition (EPD) calcination method. The effects of the deposition time and voltage, and of the calcination temperature have been investigated. The microstructure of the deposited films in the electrodes before and after calcination has also been investigated. The electrocatalytic properties of the electrodes have been investigated using cyclic voltammetry and polarization curves. The electrode films produced using this new technique have a porous structure composed of stacked hexagonal NiCo2O4 nanosheets. The resulting electrodes exhibit good electrocatalytic properties for water electrolysis. 相似文献
992.
993.
Comparison of Three‐Dimensional Korean Male Anthropometric Data with Modeling Data Generated by Digital Human Models 下载免费PDF全文
The purpose of this study was first to extract the anthropometric data of typical Korean male adults, based on the three‐dimensional anthropometric data measured through the Size Korea project. The data were then analyzed to identify the differences in the anthropometric characteristics between typical Koreans and 3D Korean mannequinmannequins generated by digital human models. Revision equations were then suggested to improve the inaccuracy of digital human models. Typical Korean adults subject to the 3D body scan data were selected by factor analysis with respect to the 5th, 50th, and 95th percentiles. Comparisons of anthropometric differences included the differences of the height and length variables in the vertical direction and the breadth, depth, and circumference variables in the horizontal direction. These comparisons demonstrated the differences in the anthropometric characteristics between typical Koreans and Korean mannequins based on differences in body shape and proportions between Korean and Western populations. Typical Koreans have shorter legs and longer torso than those of such mannequins generated from their own modeling algorithms, and the body shape of Koreans is more of an inverted triangular shape compared to the models. Although 3D digital human models are required to be modified to appropriately reflect the Asian body shape, modification of the modeling algoritms is not available to the public. The revision equations that convert the Korean modeling data of RAMSIS and Human in CATIA into typical Korean anthropometric data were instead suggested by regression analysis. It is expected that the proposed revision equations will help the designer evaluate design alternatives and improve the suitability of ergonomic evaluation for Korean customers. © 2012 Wiley Periodicals, Inc. 相似文献
994.
995.
Fractionation of the MeOH extract of Homaxinella sp., a marine sponge, led to the isolation of a sodium salt of a new brominated FA (1), two new MG (2 and 4), and a new lysoPC (6). The geometry of the double bonds in 1 and 2 was defined by comparison of the NMR chemical shifts of the allylic carbons, nuclear Overhauser effect spectroscopy correlations
of the allylic protons, and coupling constants of the vinylic protons with those reported. Evidence mainly from NMR and MS
analyses established the planar structures of the compounds. Compounds 1, 2, 4, and 6 were evaluated for cytotoxicity against a panel of five human solid tumor cell lines. Only compound 1 showed moderate activity. 相似文献
996.
997.
Guofeng Zhao Minchang Yu Chuan Xu Hong Tang 《通讯和计算机》2014,(1):59-65
Generating web traffic is of great importance to analyze performance of new designed network, test new equipment, and verify new protocols, etc.. However, most existing traffic generation systems tend to simulate the overall characteristics of network traffic, while neglecting of the behavior of the individual users. Nevertheless, in principle, the emerged characteristics of overall traffic originate from the aggregation of individual users' access behavior. In this paper, we propose an innovative web traffic generating method based on user browsing behavior. Our method simulates the real users' accessing behavior, and visits the real web servers. Then, we design and develop a web traffic generating system. Because our system accesses the real websites, it can produce almost the real network traffic. The test results show that the traffic generated by our system has characteristics of burstiness and self-similarity, which are widely found and characterized in many real networks. In addition, our system can better reflect real user's web browsing behavior. 相似文献
998.
Dong-Wan Kim Do-Kyun Kwon Kug Sun Hong Deug Joong Kim 《Journal of the American Ceramic Society》2003,86(5):795-799
Samples of 1/6Ba5 Nb4 O15 ·5/6BaNb2 O6 along with the pure end members, Ba5 Nb4 O15 and BaNb2 O6 , were sintered under low oxygen partial pressure. The degradation mechanisms of dielectric loss in this reducing atmosphere have been studied. We found that the degradation occurred primarily due to the formation of oxygen vacancies caused by the reduction of Nb5+ . This was determined by measuring the electrical conductivity, and through X-ray photoelectron spectroscopy. More importantly, the dielectric loss of 1/6Ba5 Nb4 O15 ·5/6BaNb2 O6 samples with higher temperature stability was further decreased on sintering in a reducing atmosphere. This observation has been explained by considering the increased porosity and formation of a reduced second phase, Ba0.65 NbO3 . 相似文献
999.
This article deals with the selection of quaternary ammonium groups for synthesis of water‐soluble, photosensitive phenolic resins, containing acrylate and different quaternary ammonium salt groups (AQSPRs), via ring‐opening reactions of epoxy phenolic resin (EPR) with acrylic acid and with different tertiary amine‐protonic acid salts. Conversion of epoxy groups, solubility, photosensitive properties, and thermal decomposition of the different AQSPRs were compared. Modification of AQSPR with methanol solution of KOH to form phenolic resin containing both quaternary ammonium hydroxide groups and acrylate groups (AQHPR) was also studied. Characterization by IR spectrum, DSC, and thermal gravimetric analysis was carried out. The results showed that in the synthesis of AQSPRs containing different quaternary ammonium salt groups, the efficiency of ring‐opening reaction of epoxy phenolic resin with tertiary amine salt in terms of conversion of epoxy groups decreases in the following order: for the tertiary amine, N,N‐dimethyl benzylamine (DMBA) > triethylamine (TEA) > trimethylamine (TMA) > N,N‐dimethyl aniline (DMA) > triethanolamine (TENA) > tri(n‐butylamine) (TBA); for the protonic acid, HCl > HBr > HCOOH > HI > NaHSO3 > Cl3CCOOH > HClO4 > HBF4. All the AQSPRs except that from HClO4 can be dissolved in water, methanol, DMF, or DMSO. The gel content formed during UV exposure decreases in the following order of acids used in forming quaternary ammonium salt groups: HCl > HCOOH > NaHSO3 > Cl3CCOOH; or decreases in the following order of tertiary amines or hydrohalic acids used in forming the quaternary ammonium groups: TMA. > TEA > DBMA; HCl > HBr > HI. During thermal decomposition of EPR with about half epoxy groups of EPR ring‐opened with tertiary amine salt at 160°C for 0.5 h, water‐insoluble product was formed. The insoluble content and the % decrease of epoxy groups or halide ions increase in the following order: TMA < TEA < DMBA; HCl < HBr < HI. The % decrease of epoxy groups for the insoluble residue is nearly equal to the % decrease of halide ions. A crosslinking reaction mechanism occurred in the thermal decomposition was thus proposed. During the modification of AQSPR with KOH, conversion of quaternary ammonium chloride groups can reach above 90%. The decomposition temperature of the quaternary ammonium groups was lowered from 204 to 120°C after modification of AQSPR with KOH. The photosensitive properties of the resin after modification became lower. It is better to react DMBA · HCl with EPR so as to obtain a product with higher conversion of epoxy groups, good water solubility, moderate photosensitivity, lower decomposition temperature, and better postcuring. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 91: 2914–2922, 2004 相似文献
1000.
The sintering behavior and dielectric properties of Bi3 NbO7 ceramics prepared by the high-energy ball milling (HEM) method and conventional mixed oxides method with V2 O5 addition were investigated. All the samples were sintered between 840° and 960°C. For the ceramics prepared by the mixed oxides method, the pure tetragonal Bi3 NbO7 phase formed without any cubic phase. With changing sintering temperature, the dielectric constant ɛr lies between 79 and 92, while the Q × f values are between 300 and 640 GHz. The samples sintered at 870°C have the best microwave dielectric properties with ɛr =79, Q × f =640 GHz, and the temperature coefficients of resonant frequency τf between 0 and −20 ppm/°C. For the ceramics prepared by the HEM, a pure cubic phase was obtained. The ɛr changes between 78 and 80 and Q × f were between 200 and 290 GHz. 相似文献