参考信号频率自调整的数字相敏检波器算法的研究

本文提出了一种不需要外接同频参考信号的数字相敏检波器算法。该算法首先提取计算机产生的参考信号与被测信号频率的差值，然后根据该差值调整参考信号的频率直到满足要求。本文还讨论了数字相敏检波器的幅频特性，仿真试验表明理论分析与实际结果是一致的。该算法可以用于同频参考信号不能获得时正弦信号的幅度和相位测量。     

实现多层混合刻蚀薄膜大面积均匀的方法浅探

采用多层光刻工艺结合氩离子铣的混合刻蚀方法，刻蚀高Ｔｃ超导ＹＢａＣｕＯ／ＺｒＯ２（１００）薄膜图形，取得了较好的结果。在进行氩离子镜的工艺步骤中，使用普通氩离子铣设备（离子束斑极不均匀），但采取了一定的措施─－使被刻样品在刻蚀台座上可移动，模糊地实现了薄膜的相对＂大面积＂（直径φ≥２０ｍｍ）均匀刻蚀─－可同时刻蚀２～３片６ｍｍ×１０ｍｍ薄膜，并且被刻蚀部分表面起伏约在１０ｎｍ左右。图形样品的最小线条达２μｍ，其Ｔｃ、Ｊｃ人与刻蚀前薄膜的Ｔｃ、Ｊｃ相当，即：ＴＣ为８５～９０Ｋ，Ｊｃ～１０６Ａ／ｃｍ２（在７７Ｋ下）。     

Numerical simulation of two-phase turbulent flow in hydraulic and hydropower engineering

In connection with the specific features of high velocity aerated flow generated by hydraulic engineering structures, the mathematical model is developed for high turbulence air-water two-phase flow with the use of twin flow theoretical model in this paper. Furthermore the numerical method is proposed to treat bubbled flows. In addition, on the basis of air-water stratified twin flow model, the new calculation methods and free surface tracking technique are proposed to describe complicated movements of the free surface. Finally, the proposed model is used to calculate artificial aerated flows. The computed results coincide quite well with experimental results. This means that the proposed method can provide solid basis for practical engineering design.     

Stabilization of bioethanol recovery with silicone rubber‐coated ethanol‐permselective silicalite membranes by controlling the pH of acidic feed solution

In order to produce highly concentrated bioethanol by pervaporation using an ethanol‐permselective silicalite membrane, techniques to suppress adsorption of succinic acid, which is a chief by‐product of ethanol fermentation and causes the deterioration in pervaporation performance, onto the silicalite crystals was investigated. The amount adsorbed increased as the pH of the aqueous succinic acid solution decreased. The pervaporation performance also decreased with decreasing pH when the ternary mixtures of ethanol/water/succinic acid were separated. Using silicalite membranes individually coated with two types of silicone rubber, pervaporation performance was significantly improved in the pH range of 5 to 7, when compared with that of non‐coated silicalite membranes in ternary mixtures of ethanol/water/succinic acid. Moreover, when using a silicalite membrane double‐coated with the two types of silicone rubber, pervaporation performance was stabilized at lower pH values. In the separation of bioethanol by pervaporation using the double‐coated silicalite membrane, removal of accumulated substances having an ultraviolet absorption maximum at approximately 260 nm from the fermentation broth proved to be vital for efficient pervaporation. Copyright © 2005 Society of Chemical Industry     

辽河减压渣油中金属铁的赋存与分布特征

考察了辽河减渣在吸附分离、酸性溶液萃取和沥青质轻度降解过程中金属铁的分布和转移情况。结果表明，辽河减渣中有近90％的铁富集在胶质和沥青质中，部分铁以侧链较短的环烷酸盐或酚盐形式存在，部分铁连接在沥青质分子的侧链上，或是被包裹在沥青质大分子中。     

开发井低渗透储层中长期产能预测

研究表明，某些低渗透储层具有启动压力梯度影响，即实际生产压差只有大于某个数值时，储层流体才能流动。针对此问题，从低速非达西渗流理论入手，给出了考虑启动压力影响的低速非达西储层的产能预测方法，并在F160-126等开发评价井上进行了应用，达到了准确评价低渗透非达西储层中长期产能、指导开发井生产的目的。     

入侵检测系统技术现状及其发展趋势

阐述了入侵检测系统（IDS）的起源、发展和分类，介绍了它的结构和标准化工作，对入侵检测系统存在的问题及发展趋势作了概述。     

40000m~3/h空分设备主换热器的设计及制造

通过对进口 4 0 0 0 0m3 /h空分设备主换热器进行结构分析及对比模拟计算 ,用国产传热翅片进行设计、采用真空钎焊工艺制造的主换热器 ,经并网运行 ,设计指标优于原空分设备 ,为今后成套大型空分设备板翅式换热器国产化设计、制造创造了条件。     

秦岭造山带（陕西部分）中新生代陆内造山及与矿产关系

印支运动后的秦岭造山带受古亚洲构造域、环太平洋构造域和特题斯三大构造域联合作用，发生了强烈的陆内造山，奠定了该区条块相间构造岩片系统的基本构造格架，控制了本区斑岩型钼矿和众多热液型多金属矿产的最终成矿作用和矿带展布。     

Electrospinning of hydroxyapatite fibrous mats

Polyvinyl alcohol (PVA) with an average molecular weight between 40,500 and 155,000 g/mol was electrospun with a calcium phosphate based sol. The sol was prepared by reacting triethyl phosphite and calcium nitrate and was directly added to an aqueous solution of PVA. This mixture was electrospun at a voltage of 20 kV. The results indicate that the sol was distributed uniformly in the PVA fibers, whose diameter was on the order of 2 μm. This electrospun structure was calcined at 600 °C for 6 h to obtain a residual inorganic, fibrous network, with fiber diameters between 200 and 800 nm. The fibrous structure consists predominantly of hydroxyapatite with an average crystal size of almost 10 to 30 nm. A variety of structures including non-woven mats of solid or micro-porous hydroxyapatite fibers and highly porous scaffolds could be obtained by varying the polymer molecular weight and the sol volume fraction. These structures can have many potential uses in the repair and treatment of bone defects, drug delivery and tissue engineering.