WC/Cu复合材料制备及其高温性能

用机械合金化法结合冷变形，制备了WC／Cu复合材料，研究了冷变形后复合材料的组织特征和高温退火时韵性能变化。结果表明：烧结后的材料经冷变形，组织呈显著纤维状，WC颗粒弥散分布，密度明显提高，达到理论密度的99．2％；复合材料经600～900℃高温退火，强度和硬度略有下降，塑性则有大幅提高；900℃退火时未发生明显的再结晶，界面结合良好；所制备的WC／Cu复合材料有优良的综合性能。     

一种基于空间到达角的卫星电子侦察信号分选方法

在建立简化的卫星电子侦察空间模型的基础上，提出了一种利用空间到达角分选卫星电子侦察信号的新方法。通过仿真实验验证了这种方法的可行性。该方法可用于密集信号的预处理。     

Study on the inhibiting behavior of AMT on bronze in 5% citric acid solution

The corrosion behavior of bronze in the presence of 2-amino-5-mercapto-1,3,4-thiadiazole (AMT) has been investigated in 5% citric acid by electrochemical measurements such as potentiodynamic polarization method and electrochemical impedance spectroscopy (EIS). It has been revealed that AMT is a good inhibitor for bronze. Both cathodic process and anodic process on bronze treated with AMT were different from that on the bronze without AMT treatment. Fourier transform infrared (FTIR) analysis was carried out to characterize the protective film, which revealed that the composition of the protective film was polymeric Cu(I)-inhibitor complex. AMT acted as bidentate ligand through the aminic nitrogen atom and the closed ring nitrogen in the complex.     

基于模式理论光栅椭偏参数反演的数值模拟

将一种广泛用于求解系统优化问题的方法——正单纯形法，求解光栅的椭偏方程。首先，利用求解光栅的傅立叶模式理论对TE和TM波的复反射系数进行求解。然后计算出其相应的椭偏参数(△，Ψ)，并在该值的基础上加入不同偏差的随机高斯噪声，将加入噪声后的值(△m，Ψm)作为模拟测量值。最后使用优化算法进行反演。通过对几种常用面形光栅椭偏参数的数值模拟，一方面表明傅立叶模式理论计算光栅的椭偏参数不仅精度高。而且速度快；另一方面表明利用正单纯形法得到的光栅参数值很接近于正演时假设的参数值，从而从理论上证明了利用椭偏法测量光栅各种光学参数的可行性。     

Preparation, patterning and luminescent properties of nanocrystalline Gd2O3:A (A=Eu, Dy, Sm, Er) phosphor films via Pechini sol–gel soft lithography

Nanocrystalline Gd₂O₃:A (A=Eu³⁺, Dy³⁺, Sm³⁺, Er³⁺) phosphor films and their patterning were fabricated by a Pechini sol–gel process combined with a soft lithography. X-ray diffraction (XRD), atomic force microscopy (AFM), scanning electron microscopy (SEM) and optical microscopy, UV/vis transmission and photoluminescence (PL) spectra as well as lifetimes were used to characterize the resulting films. The results of XRD indicated that the films began to crystallize at 500 °C and that the crystallinity increased with the elevation of annealing temperatures. Uniform and crack free non-patterned phosphor films were obtained by optimizing the composition of the coating sol, which mainly consisted of grains with an average size of 70 nm and a thickness of 550 nm. Using micro-molding in capillaries technique, we obtained homogeneous and defects-free patterned gel and crystalline phosphor films with different stripe widths (5, 10, 20 and 50 μm). Significant shrinkage (50%) was observed in the patterned films during the heat treatment process. The doped rare earth ions (A) showed their characteristic emission in crystalline Gd₂O₃ phosphor films due to an efficient energy transfer from Gd₂O₃ host to them. Both the lifetimes and PL intensity of the rare earth ions increased with increasing the annealing temperature from 500 to 900 °C, and the optimum concentrations for Eu³⁺, Dy³⁺, Sm³⁺, Er³⁺ were determined to be 5, 0.25, 1 and 1.5 mol% of Gd³⁺ in Gd₂O₃ films, respectively.     

基于Gabor展开的水下目标激光探测的信号检测与识别

针对水下目标激光探测的信号检测与识别的问题 ,通过对回波信号的Gabor展开进行分析 ,建立了局部窗口多重相关的峰值检测方法 ,以及利用系数矩阵的迹和特征值描述目标的反射性能 ,实现了对目标的分类识别。实验表明 ,上述方法对目标的有效检测率达 93 0 % ,分类识别有效率达 83 2 %。     

宝力格油田保护油层钻井液技术

钻井液作为与油层首先接触的外来流体极易对油层造成损害,做好钻井液保护油层工作在整个油层保护系统工程中非常重要.针对华北油田宝力格油田的储层物性,室内从岩心的敏感性评价入手,开展了钻井液保护油层技术的研究.通过对油层封堵技术的研究,研制出了适合于该油田储层特征的油层保护剂,结合现场钻井液施工的特点,制定了便于现场操作的保护油层施工措施.该技术自2002年开始,在二连地区宝力格油田共实施162口井.采取油层保护措施的井,完善井为86%,说明该钻井液技术在宝力格油田应用效果较好.     

油井封堵注水泥一次不留管柱堵水工具

吉林油田开发到中后期,油井出水现象日趋复杂,以往的注水泥堵水技术均不能满足现状的要求。鉴于此,研制出油井封堵注水泥一次不留管柱堵水工具,并形成了水泥堵水新工艺。该工具的核心为封堵注水泥装置,由打压坐封总成、胶塞座丢手总成、注水泥器本体总成和单流定压器总成等4部分组成,具有打压坐封、注水泥、投胶塞和丢手等一次性功能。经过现场6口井的施工,无一口井发生卡井事故,施工有效率100%,成功率100%。     

铁路远程网络维护的有效方法--呼叫回拨

本文阐述了网络远程维护人员进行网络维护时比较有用的三种有效方法的原理及其设置 ,较好地解决了故障排除的时间和网络维护成本的矛盾。     

葛洲坝二江电厂监控系统升级改造的实施与探讨

葛洲坝二江电厂计算机监控系统投产于1995年,运行时间已久,无论从硬件还是软件方面已不能满足目前的生产要求。升级后的新系统在各个方面均有了很大程度的改进,它的应用使得葛洲坝二江电厂的自动化控制程度有了很大的提高,为厂站“无人值班(少人值守)”的现代化管理以及三峡—葛洲坝梯级电站的联合调度提供了有力的保障。