Ce3+离子对掺Er3+碲酸盐玻璃光谱性质的影响

研究了Ce3 + 对掺Er碲酸盐玻璃荧光光谱性质的影响 ,比较了不同的Ce3 + 掺杂浓度下Er3 + 离子荧光发光强度的变化 ,分析了Ce3 + 离子对Er3 + 离子作用的原理 ,应用经典方程计算了Er3 + 离子 4I1 1 / 2 能级的荧光寿命及其变化     

CdSe量子点的制备与荧光特性研究

主要讨论了CdSe量子点的制备及荧光特性。CdSe量子点由化学方法制备，通过选择不同的反应时间得到不同尺度的量子点样品。用荧光方法研究了量子点样品在石英衬底和有机溶剂中的荧光特性。实验表明，这些量子点都有良好的荧光特性。还用无限深球方势阱模型分析了量子点样品的电子态，并根据荧光参数估算了量子点的尺度．各样品荧光峰具有一致的半峰宽，表明CdSe量子点的成核过程在反应开始时同时完成。     

工业层析洗梯液回收套用的一种方法

以生产甲胺基阿维菌素苯甲酸盐精品的工艺——工业层析产生的洗梯液回收套用的过程为例，说明利用二元恒沸物的组成随压力的变化而变化的规律，对生产洗梯液进行有效、简洁、合理分离及套用的方法。     

预应力锚固技术在龙滩水电站高边坡工程中的应用

龙滩水电站进水口高边坡最大坡高达420m，为保证高边坡的稳定，采用预应力锚索技术。预应力锚索的加固作用非常明显，不仅为边坡的稳定提供了经济、有效的手段，而且为按期截流创造了条件。     

基于RBF网络和IMM的机动目标跟踪方法

文中提出了一种应用RBF神经网络对标准IMM算法中的卡尔曼滤波结果进行校正的方法。网络输人为预测误差、卡尔曼增益以及测量值与估计值之差．网络输出反映了由于目标机动所带来的滤波误差．将网络输出结果和直接由卡尔曼滤波求解得到的结果相加．可以得到更为准确的滤波值。同时．在网络的学习算法中．在网络权值矩阵的修正公式中增加了反映滤波残差的调整项．若卡尔曼滤波的残差较大，网络调整权值的幅度也相应增大。仿真结果表明．在目标发生机动转弯处．校正后的IMM算法的跟踪误差要明显小于标准IMM算法的跟踪误差．跟踪精度较高。     

级进模两步法冲裁模设计要点

从寻求发挥多工步冲裁优越性的角度出发,通过试验测试,证明了以第1工步为半冲裁、第2工步为推料的两步法冲裁,能消除自动化冲压加工中的废料上行和废料堵塞,降低冲裁工艺噪声。提出了实现两步法冲裁级进模的结构,包括两工位两工步及三工位两工步级进冲裁模的4种具体结构,并给出了其设计要点。     

漫步潮汕小故宫

潮汕民间流行一种说法：“朝州厝，皇宫起”只有身临其境，见识了潮汕的世家望族兴建的豪宅庄园，才知此话不含糊。     

基于瞬态熔融理论的新型螺杆研究

通过对挤出机固体输送段物料融解过程的分析，提出了通过在螺槽中垫高固体床，将熔化的熔融物挤进螺槽内侧的熔池中，而在螺槽内侧的熔池保持高度不变，从而使物料和熔融物相对分离，以提高熔化速率以及减少熔融物降解的新型螺杆模型。     

MICROWAVE-ASSISTED EXTRACTION OF CAPSAICINOIDS FROM CAPSICUM FRUIT

The applicability of microwave irradiation to assist the extraction of capsaicinoids from capsicum fruit was investigated. The procedure involved irradiation of 2 g samples in a closed-vessel followed by gas chromatography of capsaicinoid derivatives. The optimum conditions for extraction were determined to be acetone at 30% power for 7 min irrespective of ground or whole tissue.
The yield of the compounds extracted was significantly greater (P < 0.05) using microwave-assisted extraction (MAE) compared to traditional reflux and shaken flask methods. A single extraction step was efficient in recovering approximately 95% of the total capsaicinoid fraction in 15 min compared with 2 h for the reflux and 24 h for the shaken flask methods. Due to the considerable savings in time and energy as well as reliability, this technique is suitable for fast extraction of capsaicinoids from large samples.     

Effect of the graft yield of maleic anhydride on the rheological behaviors,mechanical properties,thermal properties,and free volumes of maleic anhydride grafted high‐density polyethylene

The rheological behavior, thermal properties, and molecular mobility of a series of maleic anhydride (MA) grafted high‐density polyethylenes were characterized and evaluated. The rheological behavior was studied with a Haake minilaboratory. The viscosity of the samples in their melt state decreased with an increase in the graft yield, and this could be attributed to the higher molecular mobility for samples with a higher degree of grafting. The thermal properties were investigated with dynamic mechanical analysis and differential scanning calorimetry. Positron annihilation lifetime measurements were used to study the effect of the degree of grafting on the chemical environment and the atomic‐scale free‐volume properties. It was found that the grafted MA group played a significant chemical inhibition role in positronium formation when the graft yield was low. The results also indicated that the higher the degree of grafting was, the broader the free‐volume distribution was. The relationship between the microstructure and rheological behavior is discussed. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2008