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51.
Miguel Morales Joan Josep Roa José Manuel Pérez-Falcón Alberto Moure Jesús Tartaj Mercè Segarra 《Journal of the European Ceramic Society》2012,32(16):4287-4293
La0.85Sr0.15Ga0.8Mg0.2O3?δ pellets obtained by the polymeric organic complex solution method, isostatic pressing and sintering at 1350 °C have been electrical and mechanically studied. Electrical measurements evidenced reasonable ionic conductivities (0.01 S cm?1 at 800 °C), which were comparable to those reported for the La1?xSrxGa1?yMgyO3?δ prepared by other synthesis methods. On the other hand, the mechanical properties (elastic modulus, E and hardness, H) have been determined at micro/nanometric scale using the instrumented indentation technique. While E did not vary significantly with the increasing indentation depth (h), H values strongly decreased with the indentation depth up to 500 nm. For h > 500 nm, both mechanical properties remained almost constant, thus obtaining E = 271 ± 6 GPa and H = 13.2 ± 0.4 GPa. Finally, the residual imprints and fracture mechanisms have been observed by atomic force microscopy (AFM). 相似文献
52.
Stability of the antimicrobial activity of acetogenins from avocado seed,under common food processing conditions,against Clostridium sporogenes vegetative cell growth and endospore germination 下载免费PDF全文
Adriana Pacheco Dariana Graciela Rodríguez‐Sánchez Raúl Villarreal‐Lara Jesús Manuel Navarro‐Silva Carolina Senés‐Guerrero Carmen Hernández‐Brenes 《International Journal of Food Science & Technology》2017,52(11):2311-2323
Anticlostridial activity of acetogenins from avocado seed was further characterised, and their stability and effectiveness under food processing conditions, and in a model food system, studied for the first time. Isolated AcO‐avocadenyne (1) and AcO‐avocadene (2) showed anticlostridial potential, particularly the latter molecule. Enriched acetogenins extracts, obtained at laboratory scale (EAE) and semi‐commercially (Avosafe®), presented similar MIC values (3.9–9.8 ppm) and a bacteriostatic effect. Extracts bioactivity showed resistance to heat (≤120 °C), high hydrostatic pressure (HHP; 300–600 MPa, 3–6 min, 25 °C) and salt (≤3% w/v). In addition, the extract was most stable at pH ≥ 7.0 and potency against endospores increased after HHP treatment and exposure to pH 9.5, suggesting a positive effect on solubility or structure of particular acetogenins. In a model food system processed by HHP, acetogenins were retained; however, initial quantities gradually declined by 63% and 32% at 25 and 4 °C, respectively, at the end of the storage period (42 days). Most stable molecules (persediene (4) > persenones > AcO‐avocadene (2)) possess a keto or trans‐enone group at C‐4 in the aliphatic chain, which could support hydrogen donation to surrounding carbon atoms and confer antioxidant activity. Active endospores were completely inhibited by 5000 ppm Avosafe® in the model food system (37 °C, 72 h) and lower concentrations (500–1000 ppm) resulted in 1–2 log reduction of a 3 log inoculum target. Efficacy information generated in the present work is considered crucial to improve scientific knowledge on spore inhibition properties of avocado acetogenins. 相似文献
53.
María‐Jesús Oliveras‐López Marzia Innocenti Francisco Martín Bermudo Herminia López‐García de la Serrana Nadia Mulinacci 《European Journal of Lipid Science and Technology》2012,114(9):999-1006
In this approach we studied the glycaemia levels in 20 healthy young volunteers (26 ± 2 years), before and after a 30‐day intake of 50 mL of extra virgin olive oil (EVOO). We selected an oil rich in phenolic compounds (523 mg/L) with a high content of secoiridoidic derivatives (over 94.5%). The findings from our study reveal a significant decrease of glycaemia from 89.6 ± 6.8 to 82.7 ± 10.3 mg/dL (p<0.05), related to a long term daily intake of the study EVOO, as the only added fat. A significant increment of the HDL cholesterol, from 68.7 ± 11.5 to 75.2 ± 4.9 mg/dL, was also highlighted. Total cholesterol, LDL, VLDL, triglycerides, and blood pressure did not show significant variation after the 30‐day consumption of this EVOO. So far, few articles have described the influence of EVOO consumption, on plasma glucose levels in humans. This effect is observed in a group of healthy young humans. Moreover, we confirm that the level of free hydroxytyrosol (OH‐Tyr) in plasma increased up to fourfold (p<0.05) after the 30‐day intake of this EVOO. In addition, the excretion in urine of the main metabolite of OH‐Tyr, homovanillic acid (HVA), significantly increased. 相似文献
54.
Abstract A detailed study of image and Fourier transform formation by GRIN lenses is presented. It is shown how, within paraxial approximation, GRIN lenses exhibit similar behaviour to those of conventional lenses. 相似文献
55.
56.
Ahmad Amani Jordi Muela Eugenio Schillaci Jesús Castro 《American Institute of Chemical Engineers》2022,68(5):e17565
Volume of fluid (VOF) method with its Piecewise Linear Interface Calculation (PLIC) reconstruction algorithm is one of the most popular approaches in numerical simulation of interfacial flows with a wide range of applications in different areas. In an effort to evaluate the similarity of the PLIC-generated planes in comparison with the exact interface, a point-cloud, based on the polygon centers of PLIC planes is extracted, which later is used to form a triangular grid that represents the estimated interface. The main objective of this article is to evaluate the interface geometrical properties based on the extracted triangular grid of the interface. The methods presented in this article, characterized by a higher spatially convergence ratio, are compared with the commonly used methods. The proposed methods are tested for two 3-dimensional general test cases, where an evident improvement is seen in calculation accuracy and spatial convergence of the errors of interface normal vector and curvature. 相似文献
57.
Jesús Enrique Sosa-Márquez Lorena Zamarrón-Montes Sion Federico Olive-Méndez Francisco Espinosa-Magaña 《Journal of the American Ceramic Society》2022,105(9):5956-5965
Pure and Mn-doped lithium tantalate nanofibers, with Mn concentrations of 1%, 2.5%, and 5%, were synthesized by the electrospinning method. The morphology, microstructure, and crystal structure of as-spun and annealed composite nanofibers were characterized by scanning electron microscopy, X-ray diffraction, and transmission electron microscopy. Raman spectroscopy has shown to be a powerful tool to detect either local variations or changes of the whole structure. Position and width of one Raman line can be used as markers of a structural change. Some vibrational modes are especially associated with the site of Li or Ta ions and so, they can be affected by the introduction of dopant ions. Any damages or local changes in the microstructure can be detected by a line broadening. With the use of Raman spectroscopy, the sites where Mn ions enter the doped structures were established by recording the shift and broadening of peaks in Mn-doped structures with respect to pure lithium tantalate. Thus it was proven that Mn ions enter the Li sites for low Mn concentration and, on the other hand, for higher concentrations, the dopant substitutes Li and Ta sites. First-principles calculations were performed within the density functional theory, including lattice-dynamic calculations of the phonon modes at the zone center (Γ point), for the pure structure, to find the irreducible representation of the modes. 相似文献
58.
Measurement of research activity still remains a controversial question. The use of the impact factor from the Institute for
Scientific Information (ISI) is quite widespread nowadays to carry out evaluations of all kinds; however, the calculation
formula employed by ISI in order to construct its impact factors biases the results in favour of knowledge fields which are
better represented in the sample, cite more in average and whose citations are concentrated in the early years of the articles.
In the present work, we put forward a theoretical proposal regarding how aggregated normalization should be carried out with
these biases, which allows comparing scientific production between fields, institutions and/or authors in a neutral manner.
The technical complexity of such work, together with data limitations, lead us to propose some adjustments on the impact factor
proposed by ISI which — although they do not completely solve the problem — reduce it and allow glimpsing the path towards
more neutral evaluations. The proposal is empirically applied to three analysis levels: single journals, knowledge fields
and the set of journals from the Journal Citation Report. 相似文献
59.
60.
Nelly Abigail Rodríguez Efrain Almanza María de Jesús Pérez Carlos Rodrigo Mu?iz Scott Packer Russell Steel 《Frontiers of Materials Science in China》2010,4(4):415-419
This study evaluates the degree of sensitization (DOS) of 304 stainless steel joined by friction stir welding (FSW). Single-loop
electrochemical potentiokinetic reactivation tests were performed using a 0.5 mol/L H2SO4 + 0.01 mol/L KSCN solution. Sensitization was promoted by exposition of the stainless steel at temperatures between 400°C
and 850°C. The microstructure was characterized using optical microscopy to identify the weld zone and the base metal. The
samples treated at 550°C showed the most severe intergranular corrosion. The DOS was lower in the weld zone than in the base
metal after heat treatments. This reduction in the DOS for the weld zone indicates that FSW is a beneficial process in joining
stainless steel. 相似文献