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61.
铁素体钢在低温条件下存在明显的韧脆转变现象。为防止脆断事故的发生,需要确定铁素体钢制压力容器的最低使用温度。针对ASME中的A^D四条冲击豁免曲线,对应地选取了4种材料,基于材料实际的屈服强度和参考温度,按照ASME中豁免曲线的计算方法,计算得到4种材料的最低设计金属温度曲线,并与对应的A^D曲线对比,定量地分析ASME中豁免曲线的保守性。结果表明,ASME中的豁免曲线相对于材料自身的最低设计金属温度曲线保守性较大;韧性相近的材料被划分到不同的豁免曲线,使得韧性富裕量差异较大,对于某些材料,其断裂韧性被低估。 相似文献
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目的研究蛋类礼盒包装结构的缓冲性能。方法以蛋类尺寸为基础,建立可发性聚乙烯(expandable polyethylene. EPE)缓冲单元结构和组合结构,进行静态仿真分析和实验验证,比较结构在形状、叠合层数、组合形式等参数变化时的载荷与位移。结果结构层数变化相同时,单元结构的极限载荷从143N增加到236 N,组合结构的极限载荷从224 N增加到476 N,均呈近线性增长。结论蛋类礼盒包装中,组合结构的承载能力优于单元结构,通过单元结构的组合,可满足不同蛋类的包装要求。 相似文献
64.
使用分析纯物质模拟微晶玻璃熔体,分别采用柱体旋转法和拉曼光谱技术研究了La2O3含量对SiO2-CaO-Al2O3-MgO熔体黏度和结构的影响规律。结果表明:熔体黏度和黏流活化能随着La2O3含量的增加而降低;拉曼光谱表明La2O3能破坏硅酸盐结构(Qn),随着La2O3含量的增加,Q1、Q2的百分含量增加,Q3的百分含量减小,Q0的百分含量基本不变,表明熔体中非桥氧数量增加,熔体聚合度降低。La2O3在熔体中起网络修饰体的作用。 相似文献
65.
A. Amala Jeya Ranchani V. Parthasarathy Chechia Hu Yi-Feng Lin 《Chemical Engineering Communications》2020,207(6):871-886
AbstractAn eco-friendly catalyst system was synthesized using three step reaction. The Cu nanoparticles bridged aminoclay catalyst was analyzed using various analytical techniques. The structure of the catalyst was confirmed by FTIR and XRD. The synthesized catalyst system was used for the reduction of p-nitrophenol (NP), Cr(VI), and fluorescein (Flur) dye individually, as well as in their mixture forms. The kapp value was computed to access the efficiency of the catalyst. The results indicated that the kapp value of the individual system is higher than that of the mixture systems due to the absence of the complex formation reaction. The catalytic performance of the catalyst was also tested for the Schiff base (SB) formation between poly(ethyleneglycol) (PEG) and aniline (ANI) in an oxygen atmosphere. The 1H-NMR spectroscopy result indicates that the present catalyst system produced 86% yield. 相似文献
66.
Guojun Hu 《Polymer-Plastics Technology and Engineering》2020,59(13):1407-1416
ABSTRACT Polymeric foams have received increasing attention in both academic and industrial communities. Using of nanoparticles as heterogeneous nucleation agent has been verified as one of the most valid means to enhance cell nucleation and improve cell morphology. However, few researches have been conducted to investigate the effect of the nanoparticles’ spatial orientation on their nucleation efficiency. In this work, to study the influence of the orientation of nanoparticles on their performance in improving morphology of polymeric foam, thermoplastic polyurethane (TPU) composite fibers with different nanoparticles (carbon nanotubes, graphene and SiO2) were prepared by using different traction speeds. The different traction speeds lead to different orientation state of the nanoparticles which then resulted different nucleation effect. It was found that carbon nanotubes (CNTs) were easily oriented and aligned along the fiber length direction under the high traction speed, while graphene and SiO2 nanoparticles did not show orientation under the traction speed in this study. As a result, the foam of TPU/CNTs composite fibers from high traction speed exhibited a much smaller cell size and higher cell density compared to the foams of the fibers from low traction speeds, while TPU/graphene, and TPU/SiO2 composite fibers with different traction speeds showed almost similar cell size and size density after foaming, indicating that the orientated nanoparticles possessed higher heterogeneous nucleation efficiency. To our best knowledge, this work, for the first time, demonstrated the high nucleation effect of the aligned nanoparticles, which hopefully open a new path for improving the cell morphology of polymeric foam materials. 相似文献
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Rong Zhang Hailong Hu Hai Chen Siqi Li Cheng Ying Shuai Huang Qingting Liu Xudong Fu Shengfei Hu Ching-Ping Wong 《应用聚合物科学杂志》2020,137(39):49186
Recently, thermal interface materials (TIMs) are in great demands for modern electronics. For mechanically mixed polymer composite TIMs, the thermal conductivity and the mechanical properties are generally lower than expected values due to the sharply increased viscosity and poor filler dispersion. This work shows that addition of a small amount of polyester-based hyperbranched polymer (HBP) avoided the trade-off in mechanically mixed ABS/hexagonal boron nitride (h-BN) composites. After adding 0.5 wt% HBP, the maximum h-BN content in the composites increased from 50 to 60 wt%. The out-of-plane, in-plane thermal conductivity, and tensile strength of ABS/h-BN with 50 wt% h-BN were 0.408, 0.517 W/mK, and 18 MPa, respectively, and were increased to 0.729, 0.847 W/mK, and 32 MPa by adding 0.5 wt% HBP, while 0.972, 1.12 W/mK, and 29.5 MPa were achieved for ABS/h-BN/HBP with 60 wt% h-BN. The morphological and rheological results proved that these enhancements are due to the improved h-BN dispersion by decreasing viscosity of composites during mixing. Theoretical modeling based on the modified effective medium theory confirmed such results and showed that the interfacial thermal resistance also decreased slightly. Thus, this work demonstrates a facile and scalable method for simultaneously improving the thermal conductivity and mechanical properties of thermoplastic-based TIMs. 相似文献