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Novel organic hybrid silver thiostannates [Hen]4[Ln(en)4]2[Ag6Sn6S20]·3en (Ln = Er, 1; Tm, 2; Yb, 3) were prepared by the reactions of Ln2O3, Ag, Sn and S in ethylenediamine (en) under solvothermal conditions. Six SnS4 tetrahedra and six AgS3 triangles are connected into the heterometallic sulfide cluster [Ag6Sn6S20]10 − via edge-sharing. In the [Ag6Sn6S20]10 − cluster, a hexanuclear Ag6S6 core is enclosed by two Sn3S10 fragments. The Ag6S6 core is the first As–S cluster stabilized by inorganic SnS4 ligands. In 1–3, all Ln3 + ions are in 8-fold coordination environments that involved four bidentate en ligands, forming bicapped trigonal prisms. Compounds 1–3 show well-defined absorption edges with band gaps in the range of 2.18–2.47 eV. 相似文献
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在分析水电厂水调信息体系结构和应用需求的基础上,探讨采用现代信息技术构建基于交互式Web、自报/查询短消息、自动收发邮件及自动应答语音等的水调信息发布系统,从而实现多途径水调信息的发布、查询和管理,以解决水电厂单一模式的水调信息发布方式,提升水调信息多途径传递方式,以及信息传递的实时性和可靠性. 相似文献
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介绍了一种数字化阻抗测试方法,它采用锁相同步采样、数字化矢量电压电流比法及校准技术测试元器件或线路阻抗。同时介绍了相应实验电路原理,并结合线路接口,进行了通信电缆的线路阻抗测试实验。 相似文献
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为实现医用药瓶溶液杂质检测,提出一种基于二维Otsu阈值分割法的改进算法,并在Matlab环境中进行仿真。仿真结果表明:相对于传统的二维Otsu法,本文提出的改进方法提高了算法的抗噪性,减少了错误划分,加强了图像的分割效果,且容易实现。 相似文献
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《Expert systems with applications》2014,41(1):105-125
Information systems (IS) facilitate organisations to increase responsiveness and reduce the costs of their supply chain. This paper seeks to make a contribution through exploring and visualising knowledge mapping from the perspective of IS investment evaluation. The evaluation of IS is regarded as a challenging and complex process, which becomes even more difficult with the increased complexity of IS. The intricacy of IS evaluation, however, is due to numerous interrelated factors (e.g. costs, benefits and risks) that have human or organisational dimensions. With this in mind, there appears to be an increasing need to assess investment decision-making processes, to better understand the often far-reaching implications associated with technology adoption and interrelated knowledge components (KC). Through the identification and extrapolation of key learning issues from the literature and empirical findings, organisations can better improve their business processes and thereby their effectiveness and efficiency, while preventing others from making costly oversights that may not necessarily be only financial. In seeking to enlighten the often obscure evaluation of IS investments, this paper attempts to inductively emphasise the dissemination of knowledge and learning through the application of a fuzzy Expert System (ES) based knowledge mapping technique (i.e. Fuzzy Cognitive Map [FCM]). The rationale for exploring knowledge and IS investment evaluation is that a knowledge map will materialise for others to exploit during their specific technology evaluation. This is realised through conceptualising the explicit and tacit investment drivers. Among the several findings drawn from this research, the key resulting knowledge mapping through FCM demonstrated the complex, multifaceted and emergent behaviour of causal relationships within the knowledge area. The principal relationships and knowledge within IS investment evaluation are illustrated as being determined by a blend of managerial and user perspectives. 相似文献
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