Co-precipitation of nano Mg–Y/ZrO2 ternary oxide eutectic system: Effects of calcination temperature

In the family of inorganic nanomaterials, zirconia is a highly promising functional ceramic with a high refractive index, hardness, and dielectric constant, as well as excellent chemical inertness and thermal stability. These properties are enhanced in nano-zirconia ceramics, because nanopowders have a small particle size, good morphology, and uniform and dispersive distribution. In this study, a co-precipitation process was proposed to synthesise highly dispersed MgO–Y₂O₃ co-stabilized ZrO₂ nanopowders. The effects of different calcination temperatures on the crystallisation degree and particle dispersion of zirconia nanopowders were characterised by X-ray diffraction (XRD), thermogravimetry-differential scanning calorimetry (TG-DSC), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), nitrogen adsorption using the Brunauer–Emmett–Teller (BET) theory, transmission electron microscopy (TEM), and field emission scanning electron microscopy (FESEM). The optimum synthesis conditions were obtained as follows: 6 h of high-energy planetary grinding and calcination at 800 °C in an electric furnace. Under these optimum conditions, the average particle size of the prepared powder was 28.7 nm. This process enriches the literature on the controllable preparation of Mg–Y/ZrO₂ nanopowders obtained by the co-precipitation method.     

基于YCbCr肤色模型改进算法及区域特征的人脸检测研究

针对当前人脸检测的研究现状与难题,采用改进的YCbCr椭圆聚类肤色模型进行肤色区域提取,根据肤色在YCb’Cr’空间的分布,对于亮度小于80的非肤色像素点会误判为肤色点,则缩小椭圆聚类;对于亮度大于230的肤色像素点会误判为非肤色点,则扩大椭圆聚类,有效避免了在高亮度区域和亮度较低的区域中的肤色点误判问题。接着利用人脸的几何特征,对二值化图中的目标区域进行比例、大小结构的分析,排除不可能的人脸区域,并基于肤色和位置进行区域优化,将处理后的结果作为候选人脸区域输出。     

高纯天然石膏水热法制备硫酸钙晶须研究

以高纯天然石膏为原料，加压水热法制备高品质硫酸钙晶须。采用常规分析方法、XRD和扫描电镜等手段分析和表征石膏原料和硫酸钙晶须产品。结果表明，制备硫酸钙晶须的最优条件为：料浆质量分数为6.0%，转晶剂氯化镁加入量为石膏质量的0.05%，硫酸加入量为水体积的1.0%，反应时间为4.0 h，快速过滤干燥即得硫酸钙晶须产品。分析结果表明：硫酸钙晶须长度最大为280.4 μm，最小为19.59 μm，平均长度为80 μm；硫酸钙晶须直径最大为5.86 μm，最小为0.20 μm，平均直径为2.67 μm；通过统计分析可知，长径比范围为10～80。     

甲烷高温燃烧催化剂研究进展

催化燃烧具有环保、高效、节能等诸多优点.综述了甲烷高温催化燃烧的研究现状,对甲烷燃烧催化剂材料的研究进展做了较详细的介绍,并阐述了甲烷高温催化燃烧反应器的研究进展.     

Immobilization of mushroom polyphenol oxidase on poly(allyl glycidyl ether-co-ethylene glycol dimethacrylate) macroporous beaded copolymers

Functional, macroporous, beaded copolymers containing epoxy groups were synthesized for immobilization of polyphenol oxidase (PPO) from edible mushroom (Agaricus bisporus). The effect of incorporation of two different sets of monomers such as glycidyl methacrylate (GMA) and allyl glycidyl ether (AGE) and the effect of cross-linking agent ethylene glycol dimethacrylate (EGDM) with varying cross-link densities on binding and expression of mushroom PPO activity were studied. The effect of porogen viz. cyclohexanol and hexanol on PPO immobilization was studied. AGE copolymers with hexanol as a porogen were found to give higher binding and expression of PPO activity than GE polymers. Cross-linking of amino groups of enzyme with 5% glutaraldehyde for 6 h gave a stable binding of PPO on AGE-75(Hex) polymer with storage half-life of approximately 25 days. Under optimum conditions, AGE-75(Hex) polymer gave 70.3% of activity yield while percent retention of PPO activity was found to be 83.5%. Immobilized PPO showed a broader pH, higher temperature and excellent storage stability.     

泥磷回收制磷危险性分析与防治

泥磷回收制磷属于化学危险品生产,由于黄磷本身的易燃特性和生产中其他因素的诱导,极容易发生泄漏引发火灾和灼伤。介绍了泥磷的产生和泥磷回收制磷的工艺特点。应用系统安全工程的原理和方法,辨识了泥磷回收制磷生产的潜在危险性;辨识了泥磷回收制磷生产过程中的物质危险性、装置危险性和工艺危险性。运用预先危险性分析法（PHA）对泥磷回收制磷的主要危险、有害因素进行分类和分级。根据对主要危险、有害因素分类和分级的结果,提出技术措施和管理措施来提高企业安全生产管理水平和预防生产性事故的发生。     

广告代言人民事责任相关基本问题探析

广告代言人代言虚假广告的事件层出不穷,对消费者和同行竞争者的危害非常巨大,甚至影响到社会公平和市场秩序。但是,在现行法律体制下却难以追究虚假广告代言人的民事责任,因此有必要对广告代言人民事责任的性质、广告代言人承担民事责任的必要性及理论基础等相关基本问题进行研究,为我国广告代言制度提供立法参考。     

企业构建汇率风险防范体系之我见——以国际工程承包企业为例

我国国际工程承包企业面临日益增大的汇率风险。国际工程承包企业要构建有效的汇率风险防范体系,应有效组合制度与技术两方面因素,以外汇集中管理系统和汇率风险监测系统为制度平台。只有在构建制度平台的基础上,采取适当的技术措施,企业才能有效应对国际工程承包市场的日常汇率风险。     

经济全球化背景下我国外宣翻译面临的挑战

指出在经济全球化背景下外宣翻译工作的重要性,就我国目前外宣翻译工作所面临的挑战,包括:国外媒体对我国太多的负面报道、外宣翻译中存在着严重的误译、汉语中的外来词在回译时不能到位、外宣翻译时忽视中西文化的差异、外宣翻译中大量自制的"中式英语"、外宣翻译人员的综合素质有待提高等因素的制约和影响进行了示例性分析,旨在提高外宣翻译质量。     

基于物流数据仓库和决策树算法的客户信用度分析

根据物流企业与客户之间的互动关系,通过物流数据仓库决策树分析,得到各类影响因素的层次,为物流企业与客户今后的交易往来提供辅助决策信息,进行客户信用等级的评价,以此制定相应的赊销政策,控制客户信用风险。