碘掺杂聚苯胺催化合成丁醛乙二醇缩醛

制备了碘掺杂聚苯胺催化剂,采用正交实验探讨了合成丁醛乙二醇缩醛的影响因素。结果表明,在n (丁醛)：n(乙二醇)=1：1．5,催化剂的用量为反应物料总质量的0．60%,带水剂环己烷的用量为8 mL,反应时间为1．0 h条件下,丁醛乙二醇缩醛的收率可达71．6%。     

数字视音频传输中的光纤通道网络技术

随着数字技术的发展，数字视音频数据量迅速增加，这就需要一种新的视音频网络技术来提高数字视音频文件传输的速度，数字视音频的光纤通道网络技术解决了这个难题。主要介绍数字视音频的光纤通道网络技术的性能、优势以及网络环境建设。     

光学材料的激光微加工研究进展与应用前景

综述了国内外在光学材料激光微加工方面的研究成果和应用状况，并展望了其发展前景。     

壳聚糖和粉煤灰对间甲酚的吸附处理

用壳聚糖和粉煤灰对含间甲酚的废水进行吸附处理,考察了壳聚糖的用量、振荡时间、振荡速度以及粉煤灰与壳聚糖的混合比对处理效果的影响.结果表明:在常温下,对于初始质量浓度为56 mg/L的间甲酚,当壳聚糖用量为3 g/L,以170 r/min的转速吸附振荡0.5 h,去除率可达到88%以上;在上述条件下,加入质量比4:1的粉煤灰与壳聚糖混合物5g/L时,间甲酚的去除率可达到91%.     

Fabrication and characterization of TiO2/short MWNTs with enhanced photocatalytic activity

TiO₂/short MWNTs nanocomposites were prepared by the sol–gel method using butyl titanate and short MWNTs as starting materials in the solvent of isopropyl alcohol. Their photocatalytic activity in the degradation of X-3B was studied. The effects of mass ratio of short MWNTs to butyl titanate, and heat-treatment temperature on the photoactivity of TiO₂/short MWNTs nanocomposites were discussed. For comparison purpose, other photocatalysts were also employed in the photodegradation experiment. Thermogravimetric–differential thermal analysis (TG–DTA), scanning electron microscopy (SEM), X-ray diffraction (XRD) and UV–Vis absorption spectra were utilized to characterize the prepared photocatalysts. The results showed that the TiO₂/short MWNTs nanocomposites synthesized with 1% mass ratio of short MWNTs to butyl titanate had the best photoactivity.     

HDPE/CB-GP复合材料体系电性质的研究

当HDPE含量46％（质量分数，以下同）、其它添加剂（如抗氧剂、阻燃剂、交联剂和润滑剂等辅助填料）的含量11％，两种导电填料石墨（GP）和碳黑（CB）的总含量为43％时，研究结果表明石墨含量的变化对HDPE/CB-GP复合材料室温电阻率、阴C强度和后NTC强度有显著的影响．HDPE/CB-GP复合材料中GP的含量〈8．6％时，样品的室温电阻率〈30Ω·m，PTC强度〉7、后NTC强度〈1．3；电阻率．温度曲线经过17次冷热循环后重现性好，复合材料具有实际应用价值；GP在复合材料中为层片状结构。     

LD3320的嵌入式语音识别系统的应用

语音交互系统是比较人性化的人机操作界面,它需要语音识别系统的支持。LD3320就是这样一款语音识别芯片。介绍了该芯片的工作原理及应用,给出了LD3320与微处理器的硬件接口电路及软件程序。随着高档MCU的不断出现,以MCU为核心的嵌入式语音交互系统会有非常好的应用前景。     

Optimal Performance in Tracking Stochastic Signal Under Disturbance Rejection

The analysis method of optimal tracking performance is proposed for multiple‐input multiple‐output (MIMO) linear time‐invariant (LTI) systems under disturbance rejection. An H₂ criterion of the error signal between the output of the plant and the reference signal is used as a measure for the tracking performance. Spectral factorization is applied to obtain the optimal solution of the system tracking error. The explicit expressions are derived for this minimal tracking error with respect to random reference signals under disturbance rejection. It is shown that the nonminimum phase zeros, the zero direction, the unstable poles, the pole direction of a given plant, statistical characteristics of the reference input signal, and disturbance signal have a negative effect on a feedback system's ability to reduce the system error with disturbance rejection. The results show that the optimal tracking performance will further be damaged because of disturbance rejection. Some typical examples are given to illustrate the theoretical results.     

糠酸甲酯的合成

以糠醛为起始原料,通过康尼查罗反应、酰氯化和酯化反应合成了糠酸甲酯,实验结果表明:酯化反应时间2.5h,糠酸甲酯收率可达85.0%。     

铜(Ⅱ)、钴(Ⅱ)与组氨酸配合物的稳定性研究

用分光光度法测定了Cu(Ⅱ)、Co(Ⅱ)与组氨酸(His)形成配合物的紫外吸收光谱、平衡常数及配位数,探讨了pH值对配位反应的影响.结果表明,pH值越大,配合物越不稳定.在模拟生理条件下,Co(Ⅱ)配合物的稳定性比Cu(Ⅱ)配合物更好.