Sealing behaviour of glass-based composites for oxygen transport membranes

In this study, seven different filler materials in different proportions were added to a Ba-Ca-Si glass matrix “H” to investigate new sealant with higher thermal expansion coefficient (CTE) value and good sealing performance for application in oxygen transport membrane (OTM). SrTi_0.75Fe_0.25O_3-δ (STF25) was used as an OTM, and the sealing partners were ferritic steel Aluchrom and pre-oxidized Aluchrom. Compatibility tests were carried out to investigate the feasibility of the composites. Higher CTE values were found in dilatometer tests on composite samples by adding 40 wt% Ag (HAg40) and 30 wt% Ni-Cr (HNC30). Gas-tightness measurements of sandwiched samples produced appropriate helium leakage rates in the range of 10^?6 mbar·l·s^?1. Sealing behaviour of sealants HAg40 and HNC30 were investigated by joining STF25 and as-delivered/pre-oxidized Aluchrom together. Scanning electron microscopy (SEM) on cross-sections of the joints revealed a homogeneous microstructure and good adherence of the glass sealants to support metals and STF25.     

Grain orientation evolution and multi-scale interfaces enhanced thermoelectric properties of textured Sr0.9La0.1TiO3 based ceramics

Sr_0.9La_0.1TiO₃ based textured ceramics (SLTT-S3T) with a texture fraction of 0.81 are successfully fabricated by the reactive template grain growth method, in which Sr_0.9La_0.1TiO₃/20 wt%Ti was used as matrix and 10 wt% plate-like Sr₃Ti₂O₇ template seeds were used as templates. The phase transition, microstructure evolution, and the anisotropic thermoelectric properties of SLTT-S3T ceramics were investigated. The results show that the ceramics are mainly composed of Sr_0.9La_0.1TiO₃ and rutile TiO₂ phases. Grains grow with a preferred orientation along (h00). A maximum ZT of 0.26 at 1073 K was achieved in the direction perpendicular to the tape casting direction. The low lattice thermal conductivity of 1.9 W/(m K) at 1073 K was obtained decreased by 34%, 40%, and 38% compared with non-textured, SrTiO₃ and Sr_0.9La_0.1TiO₃ ceramics prepared by the same process, can be attributed to the enhanced phonon scattering by the complex multi-scale boundaries and interfaces. This work provides a strategy of microstructural design for thermoelectric oxides to decrease intrinsic lattice thermal conductivity and further regulate thermoelectric properties via texture engineering.     

Recovery of Sb(V) using a functional-ligand-containing porous hollow-fiber membrane prepared by radiation-induced graft polymerization

A ligand-containing porous membrane was prepared by radiation-induced graft polymerization of an epoxy-group-containing monomer of glycidyl methacrylate onto a polyethylene porous hollow-fiber membrane and by subsequent conversion of the epoxy group to an N-methylglucamino (NMG) group at a density of 0.78 mmol/g of the membrane. Sb(V) solution was permeated through the NMG-ligand-containing porous hollow-fiber membrane. Optimum pH for Sb(V) recovery was 3.0. Breakthrough curves of Sb (V) overlapped irrespective of residence times of Sb (V) in the membrane, due to negligible diffusional mass-transfer resistance. Maximum amount of Sb (V) adsorbed was 130 mg/g-membrane, which was equivalent to 1.3 binding molar ratio. Repeated usage of the membrane for adsorption and elution was possible.     

致密砂岩储集层裂缝综合录井识别技术研究

四川盆地油气勘探结果表明，盆地油气储集层普遍为致密砂岩非常规储集层，有效性主要取决于孔、洞、缝发育程度，因此在油气钻井中如何识别致密储集层的孔、洞、缝并确定其所在井段尤其重要。针对综合录井仪的0．1m钻时及相关参数的资料采集技术要求，通过对大量录井数据资料的统计和演算，建立起储集层裂缝发育程度及裂缝发育位置的3种储集层裂缝识别模型，即直接识别模型、地层可钻性（A值）识别模型、钻时回归（RWSR）值识别模型。系统阐述了致密砂岩储集层裂缝综合录井识别技术方法原理，详细介绍了致密砂岩储集层裂缝识别的3个模型在实际生产中的应用情况。该技术方法的研究在国内尚属首次，为油气勘探中储集层评价提供了一个新的方法和手段，可最大限度地发挥现代录井技术在油气勘探开发过程中的作用。     

塔河油田三叠系水平井地质导向技术研究

针对塔河油田三叠系碎屑岩油气藏油层薄、储集层非均质性较强、泥质和低渗致密夹层纵横向变化大的地质特点，在分析、研究不同区块多口水平井资料的基础上，探讨了水平井不同地质情况下斜井段及目的层砂顶的预测和判别技术，以实例阐述了井眼轨迹调整方法，首次形成了一套适合于该地区碎屑岩非均质薄层油气藏水平井录井地质导向技术，在塔河油田水平井钻探开发中取得了显著的成效。     

复杂场景实时目标检测方法

针对含有非平稳背景的复杂场景,提出一种基于空间混合高斯模型的实时目标检测方法.该方法以混合高斯模型作为颜色分布的统计框架,并在空间邻域中利用背景与前景隶属度之间的竞争确定像素的归属,提高了检测准确率;同时通过基于偏差均值的匹配判断和低权重模型的移除提升了混合高斯统计框架的性能,以实时地对运动目标进行准确的检测.实验结果表明,文中方法对非平稳背景有很好的适应能力,在检测准确率和运行效率上均优于其他检测方法.     

定量配料实践教学的远程监控系统设计

针对定量配料加工过程粉尘大、噪声大不适合长期监看加工,定量配料实践教学的远程监控系统设计采用了远程计算机MCGS组态软件来监控多台皮带秤配料加工过程。网络控制网关解析MCGS组态软件通过RS485发出的命令,分别监控各台皮带秤稳定工作。网络控制网关采用的是嵌入式ARMLPC2136芯片开发,LPC2136微处理器是高性能、低功耗、高集成度并具有工业级温度范围和性能的微处理器。     

双目视觉系统在风洞伞摆角测量中的研究与应用

伞系统是飞行器的重要组成部分,其摆角参数是系统安全性的重要指标之一;针对目前风洞试验中伞摆角难以测量的问题,提出了一种基于双目视觉系统的试验方法,该系统主要由两部CCD相机、图像采集卡和控制计算机组成,通过立体视觉标定和数字图像处理技术解算出空间特征标记的三维坐标,根据坐标的空间几何关系计算出伞摆角参数;试验结果表明该方法应用成功,能够同时获取伞运动过程中投影在正交平面上的竖直和水平摆角,且具有系统组成简单、通用性强的优点,有较高的应用价值。     

便携式数控系统ARM监控平台的设计

在数控系统中,通常需要利用串口或者CAN总线进行数据监控,针对满足其数据采集与发送及存储的技术要求,提出一种便携式的数控系统监控平台设计方法;基于Freescale的ARM芯片MCIMX357与Linux操作系统,利用外围接口电路,实现大容量数据存储、串口多模式通信、CAN总线数据监控,同时附加人机友好界面,利用配套电源管理方案实现低功耗便携功能;通过测试表明设计合理可靠,功耗为3.5W,串口通信频率为115200bps,CAN通信速度为500K,同时该设计成果成功应用于我单位某型数控系统中。     

基于K-means聚类的通航协同空域规划算法设计和实现

随着通航产业的不断发展,通航协同空域的合理划设是其高效、安全运营的关键,但目前以人为认知和经验划设的协同空域在使用效率和便利性上并不能满足当前通航产业链快速发展的需求。针对这个问题,文章运用K-means算法对海量历史ADS-B监视数据进行聚类分析,计算得出使用率高、通用航空器数量密集的空域范围,可为低空运行中心空域规划提供辅助决策。