Flow stress and softening behavior of wrought magnesium alloy AZ31B at elevated temperature

1　INTRODUCTIONThewroughtmagnesiumalloyshaveexcellentspecificstrengthandstiffness ,machinability ,dampcapacity ,dimensionalstability ,lowmeltingcostsandare ,hence ,veryattractiveinsuchapplicationsasau tomobile ,aviation ,electronicandcommunicationin dustry[16 ] .Investigationsontheflowstressandsofteningbehaviorofmagnesiumalloysathigherformingtem peratureandstrainratehavebeenanimportantsub jectinwroughtmagnesiumalloysforming[710 ] .InthispapertheflowstressandsofteningbehaviorofAZ31Bdeform…     

高流速高分辨辉光放电质谱法测定粉末高温合金中26种微量和痕量元素

准确测定粉末高温合金中微量及痕量元素,对粉末高温合金的生产、应用具有重要意义。将样品在放电电流40～45 mA,放电电压1 100～1 200 V,氩气流速400～450 mL/min下进行辉光放电激发,选择合适的同位素和分辨率以消除质谱干扰,使用基体匹配的内控标准样品和标准物质校准各待测元素的相对灵敏度因子(RSF),实现了高流速高分辨辉光放电质谱法(GDMS)对粉末高温合金中硼、钠、镁等26种微量及痕量元素的测定。采用实验方法对粉末高温合金内控样品中26种微量及痕量元素进行测定,各待测元素的测定值与参考值基本一致,测定结果的RSD(n=6)在0.9%～15.4%之间。采用实验方法对粉末高温合金样品进行测定,测定结果分别与电感耦合等离子体原子发射光谱法(ICP-AES)测定硼、铁和锆,高频感应燃烧红外吸收法测定硫,原子荧光光谱法测定硒,高分辨电感耦合等离子体质谱法(HR-ICP-MS)测定其余元素(钠、镁、硅、磷、钙、钒、锰、铜、镓、砷、银、锡、锑、碲、镧、铈、铪、钽、铊、铅和铋)的结果保持一致,测定结果的RSD(n=6)在0.2%～26.6%之间。     

镁合金激光焊接技术的研究现状与应用

镁在自然界中是大量存在的,我国的镁资源非常丰富,镁及其合金均具有许多优点,如重量轻、比强度和比刚度高、消震性能好、优良的机械加工性能和抛光性能、无毒性、无磁性、高热导率以及可回收利用等,已在汽车、精密仪器、电子、体育器械、核电、国防以及航空航天等许多领域得到了广泛的应用,具有广阔的应用前景.主要论述了镁合金激光焊接技术的现有水平与发展趋势以及镁合金激光焊接技术的应用领域及应用前景.     

Influence of initial textures on dynamic recrystallization and textures in AZ31 magnesium alloys

1　INTRODUCTIONMagnesiumisthelightestmetallicstructurema terialwithhighspecificstrengthandthereforeiswidelyusedinautomotive ,electronicsandaerospaceindustries[1,2 ] .However ,magnesiumoftenshowsinsufficientplasticityatroomtemperatureduetoitsHCPstructurewithlessindependentsystemsofbasalslip .Toenhanceformabilityofmagnesium ,ahigherdeformingtemperatureisusuallyusedwithtwopur poses .Thefirstistoactivatenewslipsystemsbesidesbasalslip ,sothatmorethanfiveindependentslipsystemscanbeprovided ,be…     

原位反应自发渗透法TiC／AZ91D镁基复合材料及AZ91D镁合金的拉伸变形与断裂行为

利用原位反应自发渗透技术合成了47．5％碳化钛TiC（体积分数，下同）增强AZ91D镁基复合材料，对比研究了该复合材料与铸态镁合金AZ91D基体的室温与高温拉伸变形行为，观察了拉伸断口微观组织形貌，并分析了这两种材料的断裂特征。结果表明，TiC／Mg复合材料具有良好的高温力学性能，在拉伸变形速率为0．001s^-1以及温度为723K，时其拉伸强度可达91．1MPa，而此时相同变形条件下的铸态AZ91D镁合金拉伸断裂强度只有41．1MPa，增幅达120％。而在室温下，镁基复合材料的拉伸断裂强度仅高出基体铸态镁合金23．4％。镁基复合材料的断裂应变较低，高低温时均表现为脆性断裂；而镁合金则由室温下的脆性断裂向高温下的韧性断裂过渡。     

Ni3Al中B和Mg的非平衡晶界共偏聚

在1023－1373K的初始温度和0.05-268.91K/s的冷速范围内，用Auger剖层分析确定含B和Mg的Ni3Al合金中B和Mg的非平衡晶界共偏聚行为，按照溶质－空位复合体迁移机制所导出的描述非平衡晶界偏聚的扩散速率方程解析表达式，很好地模拟了本实验结果，并确定了Ni3Al-B-Mg合金中B及B－空位复合体，Mg及Mg-空位复合体的扩散系数及复合体激活能。     

触变成形镁合金的热处理研究

介绍了触变成形镁合金的热处理研究现状以及合金元素在热处理过程中的作用,热处理过程中的析出相形态、数量以及在基体中的分布与合金的力学性能有着密切的联系.     

冷却强度及变形程度对挤压AZ31镁合金组织性能的影响

选择AZ31镁合金为原材料,在400℃下挤压散热片型材,就冷却强度及变形程度对制品的性能(抗拉强度和导电率)及组织结构的影响进行研究。结果显示:挤压温度为400℃,制品经水冷却,变形程度大的型材具有更高的抗拉强度和导电率。     

Effects of sodium tungstate on characteristics of microarc oxidation coatings formed on magnesium alloy in silicate-KOH electrolyte

Oxide coatings on AM60B magnesium alloy were prepared using the microarc oxidation（MAO） technique in silicate-KOH electrolyte with addition of 0-6.0 g/L Na2WO4. The MAO processes in base electrolyte with different concentrations of Na2WO4 were studied. The microstructure, compositions and mechanical tribological characteristics of the oxide coatings were also investigated by SEM, XRD, XPS, microhardness analysis and ball-on-disc friction testing, respectively. It is found that the addition of Na2WO4 into the base electrolyte has direct effect on the characteristics of voltage-time curves and breakdown voltage in MAO process. The number of micropores at top of the coating surface is increased by the addition of Na2WO4. The fraction of forsterite Mg2SiO4 in the oxide coating increases with increasing concentration of Na2WO4 in base electrolytes. Furthermore, the microhardness and wear resistance of oxide coatings are enhanced as well.