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71.
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The high melting point of poly(1,4‐cyclohexanedicarboxylic anhydride) [poly(CHDA)] is a disadvantage, in that it is intractable in the melting process of a drug delivery system. This report relates to diols introduced into the polyanhydride main chain to decrease its melting point. Various poly(ester anhydride)s containing ethylene glycol, 1,3‐propanediol, 1,4‐butanediol, or 1,6‐hexandiol [poly(CHDA–XDO)] were synthesized by the esterification reaction and melt polycondensation. FTIR, DSC, WAXD, and intrinsic viscosity of polymers were recorded and hydrolytic degradation, as well as in vitro drug delivery, was conducted. The results show that the samples are stable in an anhydrous environment at room temperature and degrade in water following a surface erosion mechanism. The degradation period of poly(CHDA–XDO) ranged from 130 to 320 h as a result of the different diols and amounts of XDO introduced. The in vitro drug delivery gave 130–350 h of stable delivery along with the typical surface erosion mechanism. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 2509–2514, 2002 相似文献
74.
Recent studies of self-condensation and co-condensation of melamine-formaldehyde resins; cure at low temperatures 总被引:1,自引:0,他引:1
Self-condensation: recent research on the chemical pathways by which alcoholated melamine-formaldehyde (MF) resins react with themselves and on the product structures is summarized. Model compound studies suggest that
bridges are less stable than widely thought unless they are in hexahydro-1,3,5-triazine ring structures. In acyclic structures they are probably less stable than
bridges. Co-condensation: studies of how the composition of MF resins influences the rates of reaction with poly(ol) co-reactant show that MF resins that contain very low levels of
and/or
functionality are quite reactive. Reactivities of a variety of poly(ester) and acrylic coreactants were studied. By combining reactive MF resins with reactive co-reactants one can formulate high solids enamels that cure by co-condensation in 30 min at 50 to 65 °C with 0.5 parts per hundred (phr) of p-toluenesulfonic acid (p-TSA) catalyst. Cure at 25 °C appears feasible with higher catalyst levels. 相似文献
75.
A rapid test to measure performance,emission and wear of a diesel engine fueled with palm oil diesel
H. Masjuki A. M. Zaki S. M. Sapuan 《Journal of the American Oil Chemists' Society》1993,70(10):1021-1025
Results of performance, emission and tribological evaluations of palm oil methyl ester and its blends with conventional diesel
in an automobile diesel engine test bed are presented. Polymerization and carbon deposits on the fuel injector were monitored.
CO, CO2, O2, combustion efficiency and temperature of exhaust gases were also measured. Palm oil methyl ester and its blends have great
potential as alternative diesel fuel. Performance and exhaust gas emission for palm oil methyl ester and its blends with conventional
diesel are comparable with those of conventional diesel fuel. Palm oil methyl ester does not pose a severe environmental problem
and will not deteriorate engine and bearing components. 相似文献
76.
M.?NaczkEmail author R.?B.?Pegg R.?Zadernowski F.?Shahidi 《Journal of the American Oil Chemists' Society》2005,82(4):255-260
Possible use of canola hulls as a source of natural anti-oxidants was explored. Cyclone canola hulls were extracted with methanol
(30 to 80%, vol/vol) and acetone (30 to 80%, vol/vol). The free radical-scavenging activity of phenolic extracts so prepared
was evaluated using the 2,2′-azinobis-(3-ethylbenzothiazoline-6-sulfonate) (ABTS) radical ion (ABTSo−), 1,1-diphenyl-2-picrylhydrazyl (DPPH) radical, and chemiluminescence assays. The total content of phenolics in prepared
extracts from canola hulls ranged from 15 to 136 mg sinapic acid equivalents per gram of extract. Higher levels of condensed
tannins were detected in the acetone extracts than in the corresponding methanolic counterparts. Seventy and 80% (vol/vol)
acetone extracts displayed markedly stronger antioxidant activity than any of the other extracts investigated. Statistically
significant linear correlations were found between TEAC (Trolox equivalent antioxidant capacity) values (expressed in mM of
Trolox equivalents per gram of extract) and total pehnolics, TEAC and total condensed tannins (i.e., determined using the
modified vanillin and pronthocyanidin assays), as well as TEAC and protein precipitation activity of phenolic extracts (i.e.,
measured using the dye-labeled assay). The antioxidant activities of extracts as determined by the ABTSo− radical ion assay correlated highly with those of the chemiluminescence and DPPH radical assays. 相似文献
77.
酚醛环氧乙烯酯树脂研究 总被引:2,自引:0,他引:2
梁辉 《玻璃钢/复合材料》2002,(2):41-43
本文以酚醛环氧树脂F-51与甲基丙烯酸合成出酚醛环氧乙烯酯树脂,并对此树脂的耐热性、耐化学溶剂性能进行了研究. 相似文献
78.
以环己酮为原料合成十二烷二酸二甲酯粗品,含量测定采用气相色谱法:内标物选用癸二酸二甲酯,色谱柱选用大口径毛细柱FFAP(25m×0.53mm×1.0um)。结果表明:本方法具有简单、快速、准确、可靠。 相似文献
79.
80.