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991.
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994.
尿素包合法分离橡胶籽油中的多价不饱和脂肪酸 总被引:8,自引:0,他引:8
用尿素包合法从橡胶籽油混合脂肪酸中分离多价不饱和脂肪酸 ,用正交设计实验法对分离工艺进行研究 ,其最佳分离条件是 :原料配比为m(混合脂肪酸 )∶m(尿素 )∶m(乙醇 ) =1 0 0∶1 5∶1 8,回流时间 12 0min。经一次尿素包合法分离即可得到多价不饱和脂肪酸质量分数大于90 %的产品 ,实验收率大于 35 % 相似文献
995.
996.
KeShun Liu Frank Orthoefer Edward A. Brown 《Journal of the American Oil Chemists' Society》1995,72(2):189-192
Ten soybean genotypes grown in 1992 with seed size ranging from 7.6 to 30.3 g/100 seeds and maturity group V or VI were selected
and tested for oil and protein content and for fatty acid composition. In these germplasm, protein varied from 39.5 to 50.2%,
oil, 16.3 to 21.6%, and protein plus oil, 59.7 to 67.5%. Percentages of individual fatty acids relative to total fatty acids
varied as follows: palmitic, 11.0 to 12.8; stearic, 3.2 to 4.7; oleic, 17.6 to 24.2; linoleic, 51.1 to 56.3 and linolenic,
6.9 to 10.0. Seed size showed no significant correlations with individual saturated fatty acids, protein or oil content. However,
significant correlations were found between seed size and individual unsaturated fatty acids: positive with oleic, and negative
with linoleic and linolenic. Oil and protein content were negatively correlated with each other. Among the major fatty acids,
only the unsaturated were significantly correlated with each other: negative between oleic and linoleic or linolenic, and
positive between linoleic and linolenic. A subsequent study with soybeans grown in 1993 generally confirmed these findings.
Variation in relative percentages of unsaturated fatty acids andr values for most pairs of relationships were even higher than those obtained from the 1992 crop.
Presented at the 85th AOCS Annual Meeting and Expo, Atlanta, Georgia, May 8–12, 1994. 相似文献
997.
摘要:为解决常规聚合物无法满足超高温深井酸化压裂的技术要求,本文分别以丙烯酰胺(AM) 甲基丙烯酰氧乙基三甲基氯化铵(DMC)、AM DMC SMA(十八烷基甲基丙烯酸酯)为原料,通过自由基聚合制备出两种耐酸聚合物SY-1和SY-2,并对其结构进行表征及性能测试。结果表明:SY-2红外谱图中720 cm-1为—(CH2)n—的弯曲振动吸收峰,单体成功接枝到聚丙烯酰胺分子链上;热重分析表明,SY-1升温至600℃失重比为98%,SY-2失重比86%,热稳定性得到改善;质量分数为20%盐酸中,SY-2质量分数0.8%:180℃,170s-1流变性能测试,SY-2剪切终点黏度56mPa?s,90℃、120℃、150℃剪切1h,黏度为83.6mPa?s、43.5mPa?s、27.8mPa?s,剪切稳定性分别为85.66%、74.45%、52.01%; 180℃、3MPa条件下,静态酸岩反应速率为8.94?10-5(g/cm2?s),较常规SY-1反应速率1.69?10-4(g/cm2?s)减小一个量级。且与缓蚀剂、铁离子稳定剂配伍性良好,克服高温酸化压裂技术的应用瓶颈。 相似文献
998.
David W. L. Ma Catherine J. Field M. T. Clandinin 《Journal of the American Oil Chemists' Society》2002,79(8):755-758
CLA refers to a group of geometrical and positional isomers of linoleic acid. CLA has been shown to have potentially beneficial
effects on cancer, atherosclerosis, and body metabolism in animals. Mixtures containing equal amounts of these isomers are
commonly used in many research studies because of their greater availability and lower cost relative to pure isomers. This
has hindered progress in elucidating the biological properties of specific isomers and their relevance in animal and human
biology. A method was developed that offers a compromise between cost and utility to make available enriched mixtures of either
the Δ9c,11t- or Δ10t,12c-18:2 isomers for use in a wide range of experimental applications. A countercurrent approach was developed to separate the
Δ9c,11t- and Δ10t,12c-18:2 isomers from an equal mixture of these two isomers by urea complexation. After three successive rounds of complexation
using an equal amount of CLA and urea, a fraction enriched in Δ9c,11t-18:2 containing 42.5 and 17.4% of Δ9c,11t-and Δ10t,12c-18:2, respectively, was recovered. After a single round of complexation using 2.5 g urea/g CLA, a fraction enriched in Δ10t,12c-18:2 was recovered containing 29.7 and 69.1% of Δ9c,11t- and Δ10t,12c-18:2, respectively. 相似文献
999.
系统地研究了用空气——乙炔火焰原子吸收光谱分析法测定高纯石英粉中钙的最佳条件,建立了14%的乙醇作为增感剂,在2%盐酸介质中,0.4% LaCl3溶液作为释放剂,用塞曼火焰原子吸收法测定的可行性方案,探讨了共存元素对钙的干扰及其消除。方法操作简便快速,干扰少,方法相对标准偏差小于3%,适用于日常分析石英粉中的杂质。 相似文献
1000.
Number of blends were prepared by intergrinding clinker, gypsum, fly ash, calcined clay, microsilica and limestone in laboratory ball mill in varying percentages, and their physical properties such as fineness, consistency, setting time and compressive strength have been determined. The durability tests on selected compositions were also conducted by exposing the mortar cubes separately in 5% Na2SO4 and 5% NaCl solutions till the age of 90 and 180 days. The performance was observed by compressive strength development criteria after various length of exposure. Results have been discussed and found that the durability of blended cement is higher than the ordinary Portland cement. 相似文献