Catalytic wet air oxidation of butyric acid solutions using carbon-supported iridium catalysts

Aqueous solutions of butyric acid were treated by catalytic wet air oxidation using carbon-supported iridium catalysts in a stirred reactor. Under the operating conditions of 6.9 bar of oxygen partial pressure and 200 °C of temperature, conversions up to 52.9% after 2 h were obtained depending on the type of catalyst used. The effects of butyric acid initial concentration, loading of catalyst, oxygen partial pressure and temperature were investigated and the empirical rate law for acid conversion is presented. Oxidation intermediates such as propionic and acetic acid were identified. The heterogeneous catalyzed free-radical oxidation of butyric acid is discussed.     

非线性半导体SiC微粉及其半导体漆（带）特性试验方法的研究

本文介绍了非线性半导体 SiC 微粉及其半导体漆(带)伏安特性的测量方法,以及用微机程序计算其非线性特征参数的方法,从而为研究新型防晕结构提供了科学有效的手段。     

A Method of Measuring Current–Voltage Characteristics Based on the Hammerstein–Chebyshev Model

A method of measuring the current–voltage characteristics of nonlinear components is proposed, which involves applying a sinusoidal voltage to the object being measured, finding the Fourier spectrum to read out the output current, and a calculation using the spectrum of the coefficients of the expansion of the measured characteristic in Chebyshev polynomials. The properties of the Hammerstein–Chebyshev model are considered, a block diagram of a measuring instrument is presented, and recommendations are made for minimizing the systematic errors due to approximating their characteristics by Chebyshev polynomials.     

皇甫川流域水沙特性分析及其治理对策

作者对皇甫川流域从径流泥沙来源、水沙特性、水沙变化趋势等方面进行了较为深入地分析和研究，据此提出皇甫川流域近期治理方略是：以沟道坝系建设为切入点；积极推进林草植被建设；对砒砂岩地区实行大面积封禁治理。流域近期至2010年，治理的重点建议放在十里长川、沙圪堵至皇甫区间和沙圪堵以上的纳林川左岸。     

熔敷金属扩散氢逸出特性研究

采用酒精法测量扩散氢 ,研究了焊条熔敷金属扩散氢含量以及在测氢过程中扩散氢逸出量与逸出时间的关系 (逸出特性 )。研究结果表明 ,熔敷金属扩散氢逸出特性受扩散氢含量、焊道数、熔敷金属化学成分和表面状态等多种因素的影响。熔敷金属扩散氢 (HDo)可以分为快速逸出扩散氢 (HDq)和慢速逸出扩散氢(HDs)两部分     

东荣三矿冻结段井壁破坏原因简析

介绍了东荣三矿主井、副井、东风井三个井筒冻结段井壁的施工及破坏情况,并针对破坏的原因进行了分析,同时对冻结段的井壁结构型式提出了建议。     

基于高速摄像的ESPI全场动态特性测量

采用高速摄像与ESPI技术相结合,将运动中的被测物位移随时间变化的状态以序列图像的形式实时记录,并运用图像处理技术,成功地实现了ESPI动态测量。测量了悬臂梁的自由振动过程,获得了悬臂梁的振动周期、振动频率和阻尼系数等动态特性,实验结果与理论计算值相吻合。     

消失模铸造模成型机的特点及应用

介绍了消失模铸造工艺对成型机的特殊要求,高性能成型机在大规模工业化消失模生产中的重要性,重点阐述了德国Teubert公司TVY130/90消失模成型机的特点及应用,并对成型机的国产化研究与开发提出了建议。     

平面药包抛掷爆破的漏斗特征解析

根据惠州港通用码头陆域平面药包抛掷爆破的实爆堆积测量分析成果 ,结合药包设计的主要参数 ,对平面药包产生的爆破漏斗的范围与形态、不同药包部位的残方比与抛掷率、药包的长抗比与圆柱体药包的应力波形演变关系予以解析 ,供硐室爆破的理论研究、模拟试验和总结条形药包特性时参考     

广西某矿区托帕石的宝石学特征

广西某矿区的脉石矿物——黄玉分三个世代,其中第三世代的黄玉晶体无色透明,重量大于0.9克拉,瑕疵不明显,密度(3.50)、硬度(7.8430)和折射率(1.6330)等特征均达宝石级,经系统研究测试,可以命名为托帕石(Topaz)。