锆钡镧铝氟化物玻璃的分相研究

本文综述了氟化物玻璃中的分相研究。在前人研究基础上应用透射电镜，X射线能谱，电子能量损失谱及X射线衍射，差热分析等研究了锆钡镧铝氟化物玻璃中的液-液分相，发现此种现象普遍存在于该类玻璃之中。对玻璃成分与分相形貌及微观结构之间的关系、对析出晶相种类及分相与析晶的相互影响进行了研究。提出欲降低氟化物玻璃的光损耗，分相与析晶一样是不容忽视的因素。     

流场拟合法在缩微环境中的研究

流场拟合法是由何继善院士提出的物理探测技术。以流场拟合法为理论基础研制的管涌渗漏检测仪在堤坝检测及抗洪抢险中发挥了重要作用，本文提出了一种在缩微环境中模拟管涌渗漏，对流场拟合法进行模拟测试并获得了明显的结果。为管涌仪器的性能检测、校验、标定提供了便捷的测试方法，并为该仪器在生产过程中统一性能和企业标准的制订提供了理论依据。     

射频放大器互调失真检测和载波抵消的研究

采用高功率射频信号内部互调失真的包络特性检测与比较技术,对射频功率带外信号进行检测和估计。设计用于高功率射频放大器前馈技术线性化的一个带外信号检测器。探讨如何进行射频载波抵消以及检测放大器互调失真信号。     

红外警戒系统作战环境的计算机仿真

文中论述了红外警戒系统视景仿真研究的主要内容，给出了仿真软件流程。探讨了满足红外警戒系统全方位、多目标视景生成的实时性方法。     

Near‐Infrared Light‐Emitting Diodes (LEDs) Based on Poly(phenylene)/Yb‐tris(β‐Diketonate) Complexes

Near‐infrared‐emitting electroluminescent (EL) devices using blue‐light‐emitting polymers blended with the Yb complexes Yb(DBM)₃phen (DBM = dibenzoylmethane), Yb(DNM)₃phen (DNM = dinaphthoylmethane), and Yb(TPP)L(OEt) (L(OEt) = [(C₅H₅)Co{P(O)Et₂}₃]^–) have been studied. EL devices composed of Yb(DNM)₃phen blended with PPP‐OR11 showed enhanced near‐IR output at 977 nm when compared to those fabricated with Yb(DBM)₃phen/PPP‐OR11 blends. The maximum near‐IR external efficiencies of the devices with Yb(DBM)₃phen and Yb(DNM)₃phen are, respectively, 7 × 10^–5 (at 6 V and at 0.81 mA mm^–2) and 4 × 10^–4 (at 7 V, and 0.74 mA mm^–2). The optimal blend composition for EL device performance consisted of PPP‐OR11 blended with 10–20 mol‐% Yb(DNM)₃phen. A device fabricated using Yb‐(TPP)L(OEt)/PPP‐OR11 showed significantly enhanced near‐IR output efficiency, and future efforts will focus on devices fabricated using porphyrin‐based materials.     

红外半导体激光光镊的实验研究

激光光镊技术是一项在许多科学领域有广阔应用前景的技术。本文详细给出构建一台红外半导体激光光镊的设计思想及实例。由于采用了独特的对大功率多模红外激光选模整形和双透镜陷阱操纵技术等性能价格最优化选择 ,该系统易于构建 ,陷阱操作方便 ,其构建价格仅一般光镊的几十分之一 ,非常适合光镊技术的推广和一般实验室构建     

激光窃听技术的研究

介绍了激光窃听的基本原理，归纳了该技术的特点．并提出了激光窃听的实现方案。     

Characterization of temporal response, spectral responsivity and its spatial uniformity in photoconductive diamond detectors

Three photoconductive diamond detectors with highly oriented diamond (HOD) films fabricated by the same process were characterized with respect to temporal response, spectral responsivity and its spatial uniformity over the wavelength range from 190 to 250 nm. Temporal measurements showed a drift in the baseline, suggesting the presence of deep level carrier traps. The responsivity of specimen No. 2 was more than twice those of the other two specimens, but it showed an unpredictable current fluctuation. It was found that the spatial uniformities of all the specimens were too low for radiometric purposes. A prominent peak, thought to be due to photoemission, was found in the responsivity spatial distribution of specimen No. 3 under a negative applied voltage.     

Motor oil classification by base stock and viscosity based on near infrared (NIR) spectroscopy data

In this paper we have tried to build effective model for classification of motor oils by base stock and viscosity class. Three (3) sets of near infrared (NIR) spectra (1125, 1010, and 1050 spectra) were used for classification of motor oils into 3 or 4 classes according to their base stock (synthetic, semi-synthetic, and mineral), kinematic viscosity at low temperature (SAE 0W, 5W, 10W, and 15W) and kinematic viscosity at high temperature (SAE 20, 30, 40, and 50). The abilities of three (3) different classification methods: regularized discriminant analysis (RDA), soft independent modelling of class analogy (SIMCA), and multilayer perceptron (MLP) - were also compared. In all cases NIR spectroscopy was found to be quite effective for motor oil classification. MLP classification technique was found to be the most effective one.     

Preparation,structural elucidation,molecular weight determination,and molecular recognition of first‐ and second‐tier dendrimer molecules

1,3,5‐Triglyceratetriazine [first tier (G₁)] and tri(1,3,5‐triglycerate) triazine [second tier (G₂)] dendrimers were prepared with 1,3,5‐trichlorotriazine and sodium glycerate in a 1 : 3 mass ratio in an ethanolic medium.G₁ and G₂ were amorphous, white, solid substances. Their structures were elucidated with IR, ¹H‐NMR, and ¹³C‐NMR, and their thermal stability was studied with thermogravimetric analysis. The activation energy was calculated with the Freeman–Carroll model. Densities, viscosities, and surface tensions for 0.01–0.08 mol/kg aqueous solutions increased at 0.01 mol/kg for sodium glycerate, 1,3,5‐trichlorotriazine, 1,3,5‐triazine triglycerate chloride, G₁, and G₂. These values were measured at 298.15 K. The apparent molal volume, reduced viscosity, and inherent viscosity were calculated from the densities and viscosities, respectively. The data were regressed for the limiting densities, limiting apparent molal volumes, intrinsic viscosities, limiting inherent viscosities, and limiting surface tensions for solute–solvent interactions. The positive limiting apparent molal volume values were noted in the order of G₂ > 1,3,5‐triazine triglycerate chloride > G₁ > 1,3,5‐trichlorotriazine > sodium glycerate, with weaker hydrophilic intermolecular interactions of G₂. The higher intrinsic viscosity and limiting inherent viscosity values for G₂ implied stronger G₂–H₂O hydrophilic interactions, and the higher limiting apparent molal volume of G₂ indicated slightly higher dynamic conformational changes in comparison with G₁, with stronger structural activities. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008