硬件中断引入方法及中断深度性能测试

讨论了Windows操作系统下硬件中断产生的方法,使用硬件DIO输出卡对设计的中断服务程序作了多种时序下试验,做了Windows系统下中断服务工作时的干扰试验,在中断线程和工作线程内部提出了多种试验方法,深入研究了Windows系统下的内核级调度执行相关代码段所需的时间,测试了多种时钟的精确度,设计了工程实用的中断服务程序。     

基于用户QoE的流媒体系统性能测评模型设计

影响流媒体用户服务质量体验QoE(Quality of Experience)的因素有很多,如何对用户QoE进行量化判别是一个复杂的问题。为此,以媒体传输指标MDI为基础,研究了用于测量流媒体用户QoE的基本指标,并提出了相关测量数据的获取方法。以流媒体用户的实际体验质量为依据,提出了一种有效的流媒体系统性能评价模型,该模型为流媒体系统的性能分析和优化调整提供了理论基础,具有广泛的应用价值。     

虚拟机软件结合LoadRunner的一种测试方案探讨

基于虚拟化技术进行软件自动化测试是测试主流技术发展的一个方向。介绍了虚拟机软件VMware结合测试工具软件LoadRunner的一种软件测试方案,详细介绍了测试方法、测试环境、测试用例以及数据处理方法。通过对同一B/S系统在真实环境和虚拟环境中进行对比性能测试,并基于实测数据加以分析,论证了该方案的优越性,得出了能否应用的结论。     

防静电橡胶条配方的研制

通过采用不同品种、不同用量的炭黑及不同品种的软化剂对导电橡胶制品导电性能的影响试验，确立了防静电橡胶条的较佳生产配方。     

新型破乳-助排剂的研制及其在吉林油田的应用

储层压裂改造是低渗透油气藏增产的重要技术,压裂后使地层中的滤液及时返排能够降低油气流动阻力,增加油气井产量,压裂液的压后返排率的高低直接影响压裂增产效果。目前采用添加破乳剂和助排剂的方法提高返排率。为了降低成本、减少伤害,本文通过对压裂液体系中的破乳剂、助排剂进行优化,筛选出新型破乳-助排剂。采用新型破乳-助排剂,达到一剂两效的作用。现场应用情况表明该技术效果良好。本文分析了破乳剂和助排剂的作用机理,以及新型破乳-助排剂的性能。     

Toughening of vinylester–urethane hybrid resins through functionalized polymers

Liquid nitrile rubber, hyperbranched polyester, and core/shell rubber particles of various functionality, namely, vinyl, carboxyl, and epoxy, were added up to 20 wt % to a bisphenol‐A‐based vinylester–urethane hybrid (VEUH) resin to improve its toughness. The toughness was characterized by the fracture toughness (K_c) and energy (G_c) determined on compact tensile (CT) specimens at ambient temperature. Toughness improvement in VEUH was mostly achieved when the modifiers reacted with the secondary hydroxyl groups of the bismethacryloxy vinyl ester resin and with the isocyanate of the polyisocyanate compound, instead of participating in the free‐radical crosslinking via styrene copolymerization. Thus, incorporation of carboxyl‐terminated liquid nitrile rubber (CTBN) yielded the highest toughness upgrade with at least a 20 wt % modifier content. It was, however, accompanied by a reduction in both the stiffness and glass transition temperature (T_g) of the VEUH resin. Albeit functionalized (epoxy and vinyl, respectively) hyperbranched polymers were less efficient toughness modifiers than was CTBN, they showed no adverse effect on the stiffness and T_g. Use of core/shell modifiers did not result in toughness improvement. The above changes in the toughness response were traced to the morphology assessed by dynamic mechanical thermal analysis (DMTA) and fractographic inspection of the fracture surface of broken CT specimens. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 672–680, 2002; DOI 10.1002/app.10392     

Mechanical properties and crosslink density of rare earth‐modified high‐abrasion furnace‐filled powdered natural rubber

High‐abrasion furnace‐filled powdered natural rubber [P(NR/HAF)] has more advantages than traditional HAF‐filled bale NR (NR/HAF) because of its better environmental performance and easier processing quality, but its lower mechanical properties are disadvantageous. To improve the mechanical properties, rare earth‐modified HAF‐filled powdered NR [P(NR/HAF‐Ln)] (Ln = Sm,La,Pr) was prepared by means of coacervation–coprecipitation, using rare earth‐modified HAF as separant and filler. The effect on mechanical properties of P(NR/HAF‐Ln) vulcanizate exerted by the emulsifier/HAF ratio, powdering temperature, Ln/HAF ratio and type of Ln, and HAF content were studied. The results indicated that when optimum formulation, the mechanical properties of P(NR/HAF‐Ln) vulcanizate were better than P(NR/HAF) vulcanizate. In addition, the relationship of the apparent crosslink density and HAF content of P(NR/HAF‐Ln), P(NR/HAF), NR/HAF vulcanizates was also investigated, along with their SEM microphotographs of tensile fracture surface, which indicated that the excellent mechanical properties of P(NR/HAF‐Ln) vulcanizate was attributed to correct amount of Ln that could increase crosslink density and reinforce the interface structure of NR matrix/HAF‐Ln particle. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 1755–1762, 2006     

用稳态法测量轮胎橡胶复合材料的导热系数

利用稳态法测试了4种轮胎橡胶复合材料的导热系数，在测试温度范围内，实验结果与温度线性相关。对误差进行了分析，并用校核实验验证了实验装置的准确性和精确性。     

High-pressure fluidized bed coating utilizing supercritical carbon dioxide

Various particles with sizes between 100 and 200 μm were encapsulated with waxes commonly used in technical coating applications. For this, a homogeneous mixture of molten paraffin and supercritical carbon dioxide was prepared in an autoclave and injected into the high-pressure fluidized bed through a nozzle from the bottom. Due to the different conditions in the mixing autoclave and the fluidized bed, the paraffin precipitated in the vicinity of the nozzle and adhered to the solid particles. A complete, thin, uniform, and solvent-free coating was produced. The use of two paraffins with different alkane compositions resulted in dissimilar spreads on glass beads due to their different glass transition temperatures. A smaller pressure drop across the nozzle led to more uniform and even coatings. Glass beads, ceramic spheres, potassium chloride, and lactose showed similar coating results, whereas different morphologies were observed with a plastic material, characterized by a rougher surface and a lower surface energy. The high quality of the coating was confirmed by standard dissolution tests with coated potassium chloride crystals and lactose agglomerates.     

氧化还原引发降解天然橡胶与丙烯酸酯共聚的研究

研究了降解天然橡胶胶乳与丙烯酸甲酯、丙烯酸丁酯的聚合，以过氧化苯甲酰—N，N—三甲基苯胺(BP0—DMA)为氧化还原引发剂，考察了不同反应温度、引发剂配比、乳化剂用量及加料方式对单体转化率和接枝率的影响；用红外光谱对共聚物进行了表征。结果表明，采用乳化还原引发剂可使聚合反应低温快速进行，过量还原剂起阻聚作用，采用复合乳化剂可提高聚合反应速度和乳液稳定性，补加料可提高接技率。