填料萃取塔的操作性能及设计计算

系统地介绍了填料抽提塔的两相流动及传质特性，设计计算，对填料塔的设计和操作有一定指导意义。     

Design and characterisation of a close-concentric annular reactor for kinetic studies at high temperatures

A novel annular reactor for kinetic studies at high temperature and flow conditions has been designed to keep eccentricity tolerances below 10%. In a previous work, we have shown that it is very important to keep such low eccentricity values in order to collect reliable kinetic data from this type of reactors. As proposed in this study, a modified reactor with the use of a spacer could guarantee an annular duct with low levels of eccentricity. Manufacturing tolerances or deformation effects giving rise to eccentricity can be significantly minimised when using this apparatus. The reactor has been both experimentally and theoretically characterised. Carbon monoxide oxidation was used as a model reaction under mass-transfer limited conditions revealing an eccentricity of ∼5%. With such small eccentricity levels, a concentric annular form can be assumed in the reactor analysis. Simple 1D or 2D models can therefore be inexpensively used in the evaluation of the kinetic data. Also, prior to the design of the annular reactor, a numerical investigation was carried out to clarify the effects of eccentricity, physical properties of the carrier gas and the annular aspect ratio on mass-transfer limitations. Contrary to expectations, a considerable increase in the fuel mass-diffusivity by carrier gas substitution did not change the mass-transfer rates for cases when eccentricity and aspect ratios were high.     

多功能智能流量计研制

本文详细论述了利用单片微计算机构成的多功能、多用途流量计量与自动控制系统的研制设计，给出了系统硬件原理框图与软件结构框图。该仪器适用范围较广，具有广阔的应用前景。     

Improvement of oxygen mass transfer estimation from oxygen concentration measurements in bubble column reactors

An original procedure has been established for estimating the overall volumetric mass transfer coefficient using the oxygen concentration curves resulting from the usual gassing-in and gassing-out method. This procedure was applied to experimental data obtained in a small scale bubble column using both tap water and a coalescence-inhibiting liquid mixture that represents the coalescence behavior of biological media. It is based on the analysis of the characteristics times of the system, including those of the hydrodynamics of the two phases, the sensor dynamics and the system inertia when the gas composition is modified. A numerical procedure was developed to estimate the characteristic time of the system inertia t_i, using the assumption that this inertia is nearly independent of superficial gas velocity U_G. The calculations confirmed that the optimized t_i value was nearly independent of U_G and of the coalescence behavior of the liquid phase. Additionally, the resulting K_La_L values for tap water were closer to the correlation of Shah et al. [1982. Design parameters estimations for bubble column reactors. A.I.Ch.E. Journal 28, 353-379] than those of other conventional models. Finally, the original procedure was also reported to reduce significantly the square sum deviation between the predicted and the measured oxygen response curves.     

一种新型均速管流量计在高炉煤气测量中的应用

高炉煤气具有管径大、流速低、粉尘大、易堵塞等特点，其流量用常规装置测量效果不尽理想。近来，一种新型均速管流量计——威力巴流量计采用独特的结构设计，在高炉煤气流量测量中取得了不少进展。本文对威力巴流量计的基本原理和应用于高炉煤气测量的突出优点进行了分析，并给出了安装使用时的一些建议。     

The Effect of Ozone Gas-Liquid Contacting Conditions in a Static Mixer on Microorganism Reduction

The effect of gas-liquid contacting conditions in a static mixer on ozone transfer efficiency and reduction of Bacillus subtilis spores was studied in an experimental ozone contactor. An empirical mathematical model was developed that related the transfer efficiency in the experimental system to the superficial liquid velocity in the mixer, the gas-liquid flow rate ratio and the height of the down-stream bubble column. Spore reduction was determined primarily by the dissolved ozone concentration-time (C_avgt_m) product in the reactive flow segment and was independent of the gas-liquid contacting conditions in the static mixer. In an integrated ozone contacting system, the static mixer should be designed to maximize ozone mass transfer while the reactive flow segment should be designed for efficient microorganism reduction.     

Integration of solvent extraction and liquid membrane separation: An efficient tool for recovery of bio-active substances from botanicals

An integrated process based on simultaneous solid-liquid extraction and liquid membrane separation is proposed for recovery and isolation of valuable species from botanicals. This integration provides complete exhausting of the solid material even in the case of very low solubility of the specified solute in the extracting solvent. Selectivity of the liquid membrane ensures a preferential transport of the desired solute from the native extract into the strip solution, while the other co-extracted species remain predominantly in the native extract.     

Oxygen transport rate on Rhodococcus erythropolis cultures: Effect on growth and BDS capability

The influence of oxygen transport rate on Rhodococcus erythropolis cultures has been studied in a stirred tank bioreactor under different transport and uptake conditions. Oxygen uptake rate has been measured by applying a modified dynamic method and a kinetic model is proposed, obtaining the kinetic parameter values: specific maintenance and yield coefficients. The volumetric mass transfer coefficients under inert conditions, k_La, and during the bioprocess, K_La, have been determined. The values obtained are different and a biological enhancement factor E, has been considered. These parameters have been predicted by the theoretical model and good agreement with experimental data under the conditions studied has been found. The oxygen limitation has been expressed by a modified dimensionless Damköhler number, Da, the relationship between transport and biological reaction rates. This number decreases with increasing stirrer speed; that is, when mass transport resistance decreases. The efficiency of oxygen utilization can be determined by a film effectiveness factor, η. The effectiveness factor was found to be a strong function of Damköhler number and decrease with increasing Da. Furthermore, oxygen concentration into culture depends on the mass transfer and consumption rates. The theoretical model proposed is able to reasonably predict the evolution of dissolved oxygen concentration with time of cultivation.     

流量测量准确性的现场验证及其解决方案

流量计示值准确性的现场验证是交工验收的重要内容。介绍了现场校验法，质量平衡法，热量平衡法，设备能力法等流量测量系统的校验方法以及一些技巧。     

大规模定制下的质量控制系统框架设计

大规模定制为生产带来了变革和影响。针对新的生产方式的要求，根据推动大规模定制的过程方法和技术来分析他们对于质量控制产生的影响和要求，给出了大规模定制条件下的质量控制系统的建议，并给出了一个简要的系统模型。