YG1900超高强度钢性能指标离散机理分析及工艺改进

6t真空感应+6 t真空自耗双真空工艺冶炼+锻造成材工艺生产的Φ200 mm YG1900超高强度钢,在性能检测时发现性能指标有离散现象。本文对性能指标离散的试样显微组织进行扫描电镜及电子探针分析,结果表明:由于W、Mo偏析使组织中碳化物偏聚是导致性能指标离散的原因。将真空自耗冶炼熔速由4～5 kg/min降低到3～4 kg/min,锻造钢锭均质化温度由1 200～1 220℃提高到1 230～1 250℃,锻造生产总锻比由24～30增加到50～56,通过工艺改进后改善了YG1900超高强度钢性能指标离散问题。     

Influence of expandable graphite on fire resistance and water resistance of flame-retardant coatings

Expandable graphite (EG) coating and ammonium polyphosphate-pentaerythritol-melamine (APP-PER-MEL) coating were prepared. Thermal degradation and char formation of the coatings were investigated by differential thermal analysis (DTA), thermogravimetry (TG), X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The results have shown that the anti-oxidation and fire-resistant properties of expandable graphite coating containing EG with size of 74 μm are better than those of APP-PER-MEL coating. The static immersion test was applied to study water resistance of the coatings, and the fire protection test and mechanical test were used to analyse heat insulation and mechanical properties of coatings before and after water immersion. The fire-resistant and mechanical properties of APP-PER-MEL coating were severely damaged by water immersion, whereas EG coating containing 8.5% EG with size of 74 μm could retain the good fire resistance even after 500 h water immersion.     

Al-4%Cu多晶合金中锯齿形屈服现象的初步时序分析

对Al-4％Cu合金试样拉伸实验的锯齿形应力曲线进行了系统的统计分析，研究了锯齿应力跌幅、跌落时间以及再加载时间等特征物理量随应变、试样厚度和加载应变率的时序演化规律．结果表明，跌落时间对应变不敏感；1和2mm厚试样的平均应力跌幅和平均再加载时间均随应变线性增加，3mm厚试样的统计结果比较复杂．展示了PLC效应中自组织临界性存在的证据，并通过与经典沙堆模型的对比，结合动态应变时效原理和位错理论，解释了PLC变形带形成的非线性机制．     

链霉亲和素-蛋白A融合蛋白基因在大肠杆菌中的表达

将合链霉亲和亲-蛋白A（Streptavidin－proteinA）融合蛋白基因的表达质粒pTSAPA导入大肠杆菌BL21（DE3），成功地表达了该融合蛋白，经SIJS－PAGE及免疫印迹等方法证实该蛋白既具有IgG的结合活性，又具生物素结合活性。     

Effect of preparation conditions on the properties of a coal-derived activated carbon honeycomb monolith

Activated carbon honeycomb (ACH) monoliths were prepared by extruding of a mixture of bituminous coal and organic additives and subsequent carbonization and steam activation. Preparation parameters that were varied were carbonization temperature and activation time. The carbonization conditions were 500, 650 and 800 °C for 1 h and the steam activation conditions were 850 °C for 2, 4 and 6 h. The monoliths at various states were characterized by SEM, XRD, nitrogen adsorption and compression test. It was found that carbonization temperature has significant effects on pore size distribution and mechanical strength of ACH monoliths. The ACH monoliths prepared from high carbonization temperatures exhibited lower values of the BET surface area and total pore volume and higher value of the mechanical strength than those of the ACH monoliths prepared from low carbonization temperatures. This was attributed to the effect of high temperature carbonization that results in the formation of relatively less defective structures.     

AM与HEMA共聚制备水凝胶接触镜材料及其溶胀性能

采用丙烯酰胺(AM)与甲基丙烯酸β-羟乙酯(HEMA)进行本体共聚制备水凝胶接触镜材料,研究了水凝胶的溶胀性能及其温度和pH值敏感性。结果表明,引发剂过氧化苯甲酰(BPO)用量为反应单体总质量的0.3%、反应温度80℃,产物溶胀之后为无色透明的玻璃状水凝胶;共聚物水凝胶具有较好的pH值敏感性,水凝胶在酸性溶液中溶胀,在碱性溶液中收缩:含有AM的水凝胶,其pH值敏感性较大:随AM的含量增大,共聚物水凝胶的溶胀速度和饱和含水量增大,随温度升高,水凝胶的饱和含水量下降,共聚物水凝胶中AM的含量对其温度敏感性无显著影响:SEM照片显示,AM与HEMA共聚物存在均匀的纤维状结构,并且共聚物中AM的含量越大,这种纤维状结构越大、越明显。     

复合材料纤维缠绕成型CAD/CAM相关技术研究

纤维缠绕成型是制造高强度复合材料制品的一种重要的工艺方法，将CAD／CAM方法应用其中可以大大提高生产效率，降低设计成本。本文提出了纤维缠绕CAD／CAM系统的总体方案，并对其中缠绕数学模型、线型优化、丝嘴轨迹生成等量要组成部分进行了分析与研究，为CAD／CAM系统的开发奠定了理论基础。     

Automatic optical phase identification of micro-drill bits based on improved ASM and bag of shape segment in PCB production

This paper addresses the problem of automatic optical phase identification of micro-drill bits for micro-drilling tool inspection in printed circuit board production. To overcome the limitations of conventional active shape model (ASM) on shape modeling of micro-drill bits, six key landmarks are defined for the initialization and optimization of ASM, and a novel method based on projection profiles is also proposed for these key landmarks detection. In addition, to involve the local shape feature, a bag of shape segment (BoSS) model is developed. Based on the improved ASM and BoSS, a new shape representation of micro-drill bits is proposed for phase identification. Experimental results show that the proposed method outperforms the conventional ASM and can improve the phase identification accuracy of micro-drill bits.     

平面线弹性问题的等几何形状优化方法

介绍具有等几何分析功能的GeoPDEs平台的数据结构和分析流程,针对二维平面形状优化问题,以控制顶点为设计变量,在推导出等几何分析的灵敏度计算公式后,提出基于GeoPDEs平台的灵敏度分析的高效实现方法,并采用移动渐近线法(Method of Moving Asymptotes,MMA)算法进行等几何形状优化.形状优化实例表明该方法收敛速度快,优化结果较理想.     

水煤浆在燃油热水锅炉内的燃烧试验

主要介绍了７ＭＷ燃油热水锅炉改烧水煤浆的改造设计，水煤浆炉前系统的调试，锅炉改造后的调试和水煤浆燃烧试验的结果。