基于加权法的砾类土含水率检测

砾类土在工程建设中有着广泛的应用,其含水率是一项非常重要的指标,但现有测试方法耗时较长。以砂砾石料的砾类土为试验对象,基于加权法思想,将饱和面干含水率替代法和虚拟比重法进行结合,开展砾类土含水率快速检测方法的研究,并对现有的饱和面干含水率测定操作进行一定的改进和优化。采用多种数学方法(绝对误差、均方偏差平方和,相关曲线的相关系数和F显著性检验分析法)对加权法和烘干法的结果进行对比分析。通过试验统计数据分析,证实加权法与烘干法的测定结果基本一致。该分析结果为现场土料含水率快速测定提供了一种新的思路和手段。     

沿海地区紫菜中总砷含量及砷形态分析

建立高效液相色谱-氢化物发生-原子荧光光谱(HPLC-HG-AFS)联用法分析紫菜中4种砷的形态。在优化仪器参数的基础上,采用正交试验法分析样品前处理中的酸浓度、萃取温度和超声时间对砷提取量的影响。当硝酸浓度0.15 mol/L、萃取温度80℃、超声时间1 h时,萃取效果最佳。对低、中、高3个水平进行方法验证,砷形态的回收率为84.0%~113.6%,精密度为1.3%~4.6%,结果显示,沿海地区的紫菜产品中总砷含量高,但有毒砷占比小。方法快速高效,可用于测定紫菜中砷形态的含量。     

乙烯、丙烯中微量水含量的分析

采用便携式微量水分析仪和库仑法微量水分析仪测定了乙烯、丙烯试样中的微量水含量,对试样的传输系统、进样量的控制、液体试样的气化和水标准气体的制备方法进行了改进,优化了测试条件。以低吸附惰性管线和小死体积单进单出的不锈钢减压器为试样传输系统,缩短了测试时间。采用液态烃闪蒸气化取样进样器气化液体试样并准确控制试样的进样量,可避免液体试样渐次气化对水含量测定结果的影响及对采样钢瓶大小的限制。采用渗透管发生器制备水标准气体,可验证分析结果的准确度。采用库仑法微量水分析仪测定水含量时,试样流量选择600 m L/min较适宜,开封保存15 d之内的卡尔·费休试剂对测定结果无影响。采用便携式微量水分析仪测定水含量时,选择试样流量在400~800 m L/min之间较适宜。两种仪器的测量结果相近,稳定性好,准确度高,回收率在102%~107%之间,相对偏差小于10%。     

Preparation and characterisation of films from xylose‐glycosylated peanut protein isolate powder

This work aimed at producing and characterising xylose‐glycosylated peanut protein isolate (PPI‐X) films by dissolving PPI‐X powder in water at ambient temperature and further plasticising with glycerol. The effect of powder dissolution temperature (20–100 °C) and glycerol concentration (15.0–45.0%, w/w) on mechanical properties and integrity of these films was quantified. The results showed that the powder dissolution temperature had no significant effect on the mechanical and water resistance properties of PPI‐X films within the temperature range tested. With increasing concentration of glycerol, the tensile strength and water resistance of PPI‐X films decreased and elongation increased. The films produced by dissolving the PPI‐X powder at 20 °C and plasticising with 25.0% glycerol had comparable mechanical properties and better water resistance compared to some other plant protein films plasticising with glycerol. The results suggested that PPI‐X films could potentially be used as biodegradable packaging materials.     

九里山矿中低压综合煤层注水应用与效果分析

为了降低九里山矿综采工作面煤尘质量浓度和瓦斯涌出量,根据九里山矿煤层特性,结合16051工作面的现场实际情况,在充分利用瓦斯抽采钻孔的基础上,探索出回风巷长孔低压渗透注水工艺,结合工作面短孔中压注水工艺,建立中、低压综合注水模式,并进行了分区域对比试验,考察了各区域的煤层含水率、煤尘质量浓度和瓦斯浓度。现场应用效果表明:中、低压综合注水效果较好,煤层含水率提高了2.94倍,煤尘质量浓度降低了80%以上,工作面瓦斯均匀释放,回风巷瓦斯浓度下降了30%以上,达到了较好的注水效果。     

浅谈氯碱氢的一种深度脱水工艺

概述了氢的主要工业生产方法和实际应用,详细介绍了氯碱氢三级脱水工艺过程,并运用在线分析手段,准确显示了干燥过程中的氯碱氢水分含量变化规律。     

广州市郊填埋场附近蔬菜重金属检测与讨论

蔬菜是人们餐桌上必不可少的食物,重金属在受污染的自然环境中又无处不在,而蔬菜中的重金属含量尤其令人担忧。本文使用原子吸收分光光度法(石墨炉)和原子荧光分光光度法检测了广州市郊某垃圾填埋场附近所种植蔬菜中重金属含量。结果:抽样由2013年10月至2014年9月共持续一年,共抽样检测12次,按平均每个月一次的频率,检测结果并未发现有蔬菜超出国家规定的限量值。     

电信运营商信息安全管控架构及集中策略研究

本文对运营商信息安全集中管控架构演进和信息安全管控策略面临的问题进行了深入分析，提出了信息安全集中管控架构的演进方向建议及对信息安全监控策略工作优化的若干意见。     

Influence of spherical porous aggregate content on microstructures and properties of gas-permeable mullite-corundum refractories

In this study, six gas-permeable mullite-corundum refractories with 45–95 wt% spherical porous mullite aggregates were prepared. The influence of the spherical porous aggregate content (SPAC) on the microstructure, gas permeability, and mechanical properties was analysed by XRD, SEM, EDS and image analysis method, etc. It's found that the SPAC affected the pore characteristics and mechanical properties through changing the packing and sintering behaviours of the aggregate and matrix in the refractories. When the SPAC was 45–65 wt%, the refractories had higher strengths as well as two gas-permeable channels in the aggregate and matrix respectively. Whereas, when the SPAC increased to 75–95 wt%, the refractories had lower strength as well as one gas-permeable channel in the matrix. The optimized product contained 65 wt% spherical porous aggregate and combined a high gas permeability of 4.9 × 10⁻¹² m², a high compressive strength of 18.5 MPa, a good thermal shock resistance and well-distributed gas-permeable channels.