离子型稀土矿山淋洗及尾水富集试验研究

对浸矿后离子型稀土原地浸矿场采用清水进行淋洗，在184天的清水淋洗过程中，尾水氨氮值从最开始的507mg/L，降低至140mg/L，淋洗尾水pH4.52~3.10。淋洗尾水采用两级反渗透膜分离，既回收有价资源稀土，又能使出水氨氮达标。结果表明，产水氨氮浓度稳定低于15mg/L，对稀土的截留率高于98.25%，浓水中稀土离子平均浓度313.4mg/L，可进一步回收稀土资源。     

双酚芴环氧树脂体系热性能和粘接性能研究

环氧树脂是一种性能优异的热固性树脂，在结构胶粘剂和纤维增强复合材料领域应用广泛。但是常见的环氧树脂体系耐热性普遍较差，近年来，航空航天领域对材料的热性能提出了更高的要求，常规的环氧树脂体系已经无法满足耐高温需求。针对该问题，我们设计了一种耐热性较高的双酚芴型环氧树脂体系，并对其热性能和粘接性能进行了研究。在本文中，首先采用流变学方法和DSC研究了其工艺性能，使用DMA和TGA法分析了环氧树脂体系的耐热性能，并通过单搭接剪切试验测试了该环氧体系的粘接性能。结果表明，双酚芴型环氧树脂体系可在180℃固化，固化后的玻璃化转变温度达到190℃，失重5%时的温度为392℃，150℃时的剪切强度为5.8 MPa，展现了优异的耐热性能和粘接性能。     

基于电信号特征分析的电机故障诊断技术

介绍了电机故障诊断技术平台的组成,分析了电机常见故障下电信号的特征。利用宜昌和景洪工厂两台电机进行了实际对比测试,宜昌工厂电机定子电流特征频率在49.2Hz时表现出峰值-36.08dB,在50.8Hz时表现峰值则为-37.23dB,表明电机存在转子断条故障;景洪工厂电机在转子特征频率为113.51Hz时,出现峰值-58.47dB,表明电机存在静态偏心故障。经电机现场抽芯检查,验证了电机故障快速诊断平台给出的电机健康状态评估结果,证实了基于电信号特征分析的电机故障诊断技术的准确性。     

空中分布式作战概念及关键技术分析

空中分布式作战是美军为应对“反介入/区域拒止”挑战提出的重要作战概念，具备分布式、智能化、高动态、大规模等特点，是未来美军空中作战平台在体系支持下作战样式的发展趋势。首先，按照提出时间梳理了美军空中分布式作战概念及典型研究项目，分析了空中分布式作战内涵、特点、工作机理以及发展趋势；然后，结合空中作战平台典型构型，提出了全域作战体系支撑下的空中分布式作战样式设想；最后，设计了空中分布式作战体系技术框架，并讨论了相应的关键技术。     

Direct ink writing of vancomycin-loaded polycaprolactone/ polyethylene oxide/ hydroxyapatite 3D scaffolds

Novel inks were formulated by dissolving polycaprolactone (PCL), a hydrophobic polymer, in organic solvent systems; polyethylene oxide (PEO) was incorporated to extend the range of hydrophilicity of the system. Hydroxyapatite (HAp) with a weight ratio of 55–85% was added to the polymer-based solution to mimic the material composition of natural bone tissue. The direct ink writing (DIW) technique was applied to extrude the formulated inks to fabricate the predesigned tissue scaffold structures; the influence of HAp concentration was investigated. The results indicate that in comparison to other inks containing HAp (55%, 75%, and 85%w/w), the ink containing 65% w/w HAp had faster ink recovery behavior; the fabricated scaffold had a rougher surface as well as better mechanical properties and wettability. It is noted that the 65% w/w HAp concentration is similar to the inorganic composition of natural bone tissue. The elastic modulus values of PCL/PEO/HAp scaffolds were in the range of 4–12 MPa; the values were dependent on the HAp concentration. Furthermore, vancomycin as a model drug was successfully encapsulated in the PCL/PEO/HAp composite scaffold for drug release applications. This paper presents novel drug-loaded PCL/PEO/HAp inks for 3D scaffold fabrication using the DIW printing technique for potential bone scaffold applications.     

Simultaneous fractionation of multiple classes of polyphenols from honeybush tea using solid-phase extraction

The structural diversity of polyphenols and the inherent limitations of current extraction techniques pose a challenge to extract polyphenols using a simple and green method. Hence, in this study, a method was developed to simultaneously fractionate multiple classes of polyphenols by only varying ethanol-water solutions. Honeybush tea, which is rich in polyphenols, was selected as a model for this study. Solvent extraction followed by solid-phase extraction (SPE) was developed to obtain a polyphenol-rich fraction from six honeybush samples. Based on a gradient elution programme (10%, 30%, 50%, 70% and 90% (v/v) ethanol-water solution) of SPE, the Strata X cartridge showed a better recovery of most targeted polyphenols under 0.9 mL of the drying volume and 1 mL min⁻¹ of the dispensing speed. The elution programme for fractionating most polyphenols was as follows: single elution with 50% ethanol, followed by twice elution with 70% ethanol. The antioxidant capacity was used to analyse the differences among the polyphenol-rich fractions from six honeybush samples. Principal component analysis (PCA) revealed that unfermented C. genistoides (GG) has the greatest antioxidant capacity among the honeybush species studied. Additionally, mangiferin, isomangiferin and vicenin-2 were the main contributors to the antioxidant capacity in six honeybush fractions according to the correlation study.