冷低压分离器油相系统铵盐垢下腐蚀风险的模拟预测

为探究某加氢装置高压换热器管束腐蚀泄漏原因，利用Aspen Plus工艺模拟软件计算了冷低压分离器油相（简称冷低分油）中水质量分数分别为1%,2%,3%时，冷低分油系统的露点温度、氯化铵结晶温度、氯化铵潮解点温度和相对湿度。结果表明：相较于经验的露点温度预测方法，通过引入潮解点、划分系统“湿环境”温度范围判断氯化铵垢下腐蚀风险区域的方法与实际腐蚀案例更为切合；在3种油相含水条件下，换热器管束存在氯化铵垢下腐蚀的“湿环境”温度范围分别为：50~103 ℃,50~161 ℃,50~176 ℃；随着油相中含水量的提高，“湿环境”腐蚀区域逐渐向高温部位迁移，预计铵盐导致的垢下腐蚀将会愈加严重。     

影响干式磁选机在石英除铁过程中的因素研究

本文通过对陕西某地石英矿进行干式磁选试验研究,介绍了给料速度、尾矿抛尾率、矿样含水率及含泥量等几个因素对干式磁选作用的影响,分析了干式磁选各因素在石英除铁过程中的规律,为后续工业应用提供一定的理论基础。     

天然气新型气液分离器性能试验研究

为了解决天然气含有饱和水汽和少量烃降低输气效率、堵塞管线和设备等问题,利用旋风子、稳流元件、叶栅式分离元件、折流板式分离元件组合成新型天然气分离器。利用相位多普勒粒子分析仪对新型天然气分离器进出口粒子粒径与液态水含量的进行对比测试,以研究新型分离器的分离效率。结果表明:新型分离器具有良好的气液分离作用;在流量为10～64 m~3/h时,分离器的分离效率成抛物线形式,在33 m~3/h时分离器的分离效率降到最低值95.16%,主要原因是流量在33 m~3/h时,试验气液混合不均匀,导致内部流态紊乱,以至于试验测得分离效率相对偏低;在流量为10 m~3/h时分离器分离效率最高,为99.29%;分离器对该进口条件的气体中雾状液粒有较高的分离作用,且可以明显降低分离器出口气体中液粒的平均粒径;从进口到气相出口压力逐渐降低,总压降为950 Pa;流动区域速度梯度大不利于气液相分离,流动掺混会导致分离效率降低。     

正弦波纹挡板式沉降器内流动特性

采用VOF模型对正弦波纹式入口挡板的重力非均相沉降器内流场进行数值模拟研究。对比了正弦波纹挡板与平挡板的平均流场分布情况，分析了沉降器的轴向流速均一程度（λ₁）随时间演化特性，探究了λ₁和面积加权平均湍流强度（I_a）在沉降器内空间分布特性；引入流场均稳指标USC，研究了冲击间距（L_b/D）对USC的影响。结果表明：正弦波纹挡板作为入口构件可以有效降低返混。在0.84＜L_b/D＜2.17范围内，正弦波纹板沉降器内流场的均一程度整体高于平面挡板；随着L_b/D减小，平挡板沉降器内流场的λ₁基本不变，但正弦波纹挡板沉降器内流场的λ₁降低，且对I_a的影响不明显。对比平挡板，正弦波纹挡板可以有效降低轴向速度的梯度，使返混区面积减小，流场稳定性提高。随着L_b/D增加，USC值呈现多峰值趋势，L_b/D=2.17时正弦波纹板沉降器的USC取得极大值为14.68，较平挡板提高了93.67%。     

油浸变压器消防排水系统的计算与设计

油浸变压器的消防及排水系统关系着电厂安全,但目前其消防排水的设计多凭经验估算。本文提出一套较为完整的变压器消防排水系统的计算方法,有利于提高设计质量。     

Strain‐rate‐dependent mechanical properties of polypropylene separator for lithium‐ion batteries

The mechanical integrity of battery separators is critical for battery safety and durability. A comprehensive study of strain‐rate‐dependent tensile and puncture properties of a polypropylene lithium‐ion battery separator is presented here with a new model. Due to anisotropy of the polymeric membrane, tensile testing was conducted for different directions. Results showed that tensile strength and elastic modulus were increased 1000% and 500%, respectively, for different directions. It was also demonstrated that tensile strength changed 10 to 25% with strain rate (1.67 × 10^?4 to 1.67 × 10^?1 s^?1) for different directions. An equation was obtained for the first time for flow stress versus strain rate at varied tensile directions with respect to machine direction. Moreover, puncture testing was performed and it was shown that puncture strength was increased 140% with increasing strain rate from 0.25 to 250 mm min^?1. Two failure modes were also observed in puncture samples. Finally, Eyring's model was used to calculate activation enthalpy of the porous polypropylene separator. © 2020 Society of Chemical Industry     

Effect of the Wet Outlet Geometry on the Shockwave Position in Supersonic Separators

Supersonic separators (3Ss) are applied in gas separation processes. Two-dimensional simulation is employed to investigate the effect of operational and thermophysical parameters on the shockwave position. In addition, the impact of the cyclonic part and wet outlet geometry is evaluated by proposing four cases. Increasing the length of the cyclonic part exerts positive and negative influences on the performance of the 3S and the pressure recovery coefficient, respectively. The optimum length is determined between 10 and 15 cm. To demonstrate negative effects of wasted air from the wet outlet, its flow has been increased from 3.6 to 8.1 % of the inlet flow. Improved performance of the 3S is obtained by reducing the flow disturbances around the wet outlet and moving the shockwave towards the outlet.     

BRISOL钠同位素放射性核束的产生

北京放射性核束装置在线同位素分离器（BRISOL）采用100 MeV、200 μA回旋加速器提供的质子束打靶产生中、短寿命放射性核束，在线分析后供物理用户使用，其质量分辨率好于20 000。为开展²⁰Na核的奇异衰变特性研究，研制了氧化镁靶，并采用100 MeV质子束轰击氧化镁靶在线产生了^20～26Na⁺的钠同位素放射性核束。当质子束流强为8 μA时，²⁰Na⁺离子束的最大产额为2×10⁵ s^-1，²¹Na⁺离子束的最大产额为4×10⁸ s^-1。完成了北京放射性核束装置首个放射性核束物理实验，累计供束近200 h。     

Radiative and conductive heat transfer in a 4-K helium phase separator with minimum heat loss

Improvements in simulation and practice for the heat load of a helium phase separator are discussed. The separator cryostat (volume 100 L, cooling capacity 1.5 W at 4.2 K) re-condenses and stores liquid helium. An additional radiation shield was designed to minimize the radiative heat transfer and to decrease the heat conduction. The experimental results indicate that the heat load of the separator was decreased from 5.56 W to 1.555 W, a gain about 4 W of heat load, which is an improvement by 72%. Liquid helium (50 L) was stored in the separator stably for more than 90 h. Software implementing the finite-element method (FEM) was used to predict the temperature distribution of pipe fittings and the separator heat load with or without the additional radiation shield. The results of these simulations show that the temperatures of the pipe fittings were significantly decreased in the separator with additional radiation shields. For the heat load, the trends of simulation and experimental results were similar. This work provides a simple and effective method to minimize the radiation heat load of a separator. In this paper, we discuss in detail the improvements of the model, the experimental setup and the results of comparisons between experiments and simulations.     

Analytical Model to Characterize the Efficiency of Disk Stack Separators

Up to now the prediction of separation efficiency for disk stack separators is largely based on the concept of equivalent clarification area, short Σ-theory, firstly published in 1949. An improved analytical model with a closed-form solution is presented in which the assumptions of uniform flow and unhindered solids transport are dropped. The contributions of distributor and solids holding space to the total separation efficiency are considered. The model is validated by comprehensive experiments with different geometry parameters and particle systems. The results are presented in a universal form for a combination of dimensionless numbers.