基于光纤光栅技术测力锚杆及保护结构的研究

本文介绍了光纤光栅技术在测力锚杆上的应用,并且基于常用托盘的力学结构,增大了托盘内部的空间、设计了与之相连接的金属保护套筒使之成为一体式结构,从而有效地保护了光纤测力锚杆的主体结构。     

A Novel Strategy for Preparing Stretchable and Reliable Biphasic Liquid Metal

Low‐melting liquid metal is a hugely promising material for flexible conductive patterns due to its excellent conductivity and supercompliance, especially low‐cost and environmental liquid processing technology. However, the ever‐present fluidity characteristic greatly limits the stable shape and reliability of prepared liquid metal conductive electronics. Herein, a novel solidification strategy of liquid GaIn alloys by Ni doping and heat treatment is first reported, which can efficiently create a solid phase in the liquid metal and provide an effective solution for practical applications. Particularly, the liquid characteristic is preserved for conveniently fabricating different flexible electronic circuits, and then the solidification is carried out on prepared conductive patterns by heat treatment. The solidification mechanism is revealed by the interface chemical reaction between Ni and GaIn, creating the solid phase of intermetallic compound (Ga₄Ni₃ and InNi₃) during heat treatment. Moreover, a biphasic GaInNi can be obtained by regulating the atomic ratio of gallium, indium, and nickel. As a result, the obtained GaInNi possesses extremely low sheet resistance (15 ± 4.5 to 135 ± 2.5 mΩ sq^?1) and the variation of ΔR/R₀ exhibits low level (0–2) when strained up to 100%, which offers a promising strategy to prepare stretchable and reliable liquid metal electronics.     

吸收烟气中低浓度CO2的操作条件分析

Mg(OH)2浆液是一种具备低再生能耗潜力的CO2吸收剂，为了推进其在CO2捕集领域的应用而展开研究。在填料塔中，使用真实烟气研究了各种操作条件下Mg(OH)2浆液对CO2的捕集效率。研究发现,填料种类、气体名义停留时间、液气比均对CO2捕集效率有影响。结果表明，增加气体名义停留时间无法有效改善液相传质，而提高液气比能够有效改善液相传质；在试验条件下，拉西环、鲍尔环和IMTP的总体积传质系数分别为8.5×10-7～5.0×10-6、1.8×10-6～4.0×10-6和1.9×10-7～2.9×10-6 mol/(m3·s·Pa)。     

高炉喷吹煤粉燃烧性与反应性的研究与应用

为了研究高炉喷吹煤粉的冶金性能，采用热重分析法对6种无烟煤和1种烟煤进行燃烧性与反应性研究。结果表明，与无烟煤相比，烟煤在不同温度下的燃烧性和反应性均明显高于无烟煤。混煤的燃烧率实测值大于加权值，使用混煤可以发挥无烟煤和烟煤各自的优点，加快燃烧过程，提高混煤燃烧率。随着混煤中粒度小于74 μm煤粉所占比例的增加，燃烧率增大。在高煤比喷吹条件下，混煤煤粉粒度小于74 μm的比例控制在75%左右。结合无烟煤的燃烧性和反应性试验结果，建议喷吹煤粉采购中应尽可能多地采购无烟煤C资源，同时控制无烟煤E的采购量；高炉提煤比操作中应将无烟煤C确定为喷吹用无烟煤的首选煤种，以提升混煤燃烧率和发挥未燃煤粉保护焦炭的作用。     

Fabrication of poly(ε‐caprolactone) (PCL)/poly(propylene carbonate) (PPC)/ethylene‐α‐octene block copolymer (OBC) triple shape memory blends with cycling performance by constructing a co‐continuous phase morphology

In this paper, a triple shape memory material was prepared by ultra‐simple melt blending from poly(ε‐caprolactone) (PCL), poly(propylene carbonate) (PPC) and ethylene‐α‐octene block copolymer (OBC). The obtained material possessed a co‐continuous phase morphology and presented an excellent triple shape memory effect (triple‐SME). Theoretical prediction demonstrated that a special continuous phase morphology could be constructed by adjusting the proportions of the blend. Moreover, the results indicated that a close relationship existed between the phase morphology and the triple‐SME of PCL/PPC/OBC. The sample with 35 vol% PPC content contributed to the formation of a continuous phase morphology and exhibited the optimal triple‐SME. Additionally, the sample PCL/PPC/OBC (32.5/35/32.5) showed outstanding structure and performance stability during cycle loading–unloading tests, which evidenced the prominent cycling shape memory property (nearly 100% shape fixing and recovery of temporary shape). Overall, this work could provide an efficient, convenient and recyclable method to obtain high‐performance shape memory materials. © 2020 Society of Chemical Industry     

12R22.5全钢轮胎成型机扇形块形状仿真优化

针对12R22.5全钢轮胎出现的轮胎胎圈部位内凹和胎体帘线抽出等缺陷，利用有限元分析技术对成型机扇形块轮廓形状进行优化。通过扇形块参数调整使其横向压紧力、垂向压紧力和胎圈部位面积达到优化目标，使用优化后的扇形块提高了成型胎坯工艺质量和稳定性，同时延长了成型胶囊使用寿命。     

Properties of polyamide 6,10/poly(vinyl alcohol) blends and impact on oxygen barrier performance

The oxygen transmission rate, average volume of free‐volume cavities (V_f) and fractional free volume (F_v) of polyamide 6,10 (PA610)/poly(vinyl alcohol) (PVA) (i.e. PA610_xPVA⁰⁵_y, PA610_xPVA⁰⁸_y and PA610_xPVA¹⁴_y) blend films reduced to minimum values when their PVA contents reached corresponding optimal values. Oxygen transmission rate, V_f and F_v values obtained for optimal PA610_xPVA^z_y blown films were reduced considerably with decreasing PVA degrees of polymerization. The oxygen transmission rate of the optimal bio‐based PA610₈₀PVA⁰⁵₂₀ blown film was only 2.4 cm³ (m²·day·atm)^?1, which is about the same as that of the most often used high‐barrier polymer, ethylene–vinyl alcohol copolymer. Experimental findings from dynamic mechanical analysis, differential scanning calorimetry, wide‐angle X‐ray diffraction and Fourier transform infrared spectroscopy of the PA610_xPVA^z_y blends indicate that PA610 and PVA in the blends are miscible to some extent at the molecular level when the PVA contents are less than or equal to the corresponding optimal values. The considerably enhanced oxygen barrier properties of the PA610_xPVA^z_y blend films with optimized compositions are attributed to the significantly reduced local free‐volume characteristics. © 2017 Society of Chemical Industry     

550L板坯升级轧制600L牌号带钢试验研究

针对高强汽车钢生产合同量小、规格繁多，混浇坯和合同余材多的问题，以550L带钢的生产为例，研究了终轧温度、冷却速率对550L带钢组织以及力学性能的影响。结果表明，粗轧在再结晶区利用大变形量获得细小均匀的奥氏体组织；精轧采用低温轧制，获得内部有大量变形带的扁平状奥氏体组织，可以提高晶界面积，增加相变形核核心和驱动力，在随后的超快密集冷却过程中形成晶粒细小的铁素体组织，充分发挥细晶强化、相变强化、析出强化、位错强化的作用，使其性能达到高级别600L牌号带钢性能，实现了升级轧制，解决了上述问题。     

SnO2纳米颗粒对Sn0.6Cu钎料微观组织及界面金属间化合物的影响

本文利用超声波辅助法制备了SnO2纳米颗粒增强Sn0.6Cu钎料。研究了SnO2对钎料的微观组织、熔化性能的影响，以及Cu/Sn0.6Cu-XSnO2/Cu钎焊接头界面反应产物的变化，测量了金属间化合物层的厚度和晶粒尺寸。结果表明：1.0wt.% SnO2很好的抑制了钎料中β-Sn的长大，细化了晶粒尺寸；含SnO2钎料的熔点与不含SnO2钎料熔点基本相同，但熔程明显减小；钎料熔炼过程中施加超声波可以细化晶粒，制得的钎料熔点和液相线温度也低于普通熔炼钎料。用含SnO2钎料钎焊接头界面处的IMC层更薄且晶粒尺寸更小，主要是因为SnO2纳米颗粒吸附在界面金属间化合物的晶面处阻碍铜板与钎料基体之间的相互扩散，导致IMC的形成驱动力较低，从而抑制了界面化合物的生长。     

1.5 mm厚热轧高强耐候SPA-H带钢的开发

薄规格带钢生产中面临温降大、板形控制难、穿带速度快、轧制稳定性差等难题，通过对SPA-H带钢化学成分、连铸工艺、温度和板形控制的分析研究，确定了合理的工艺参数，开发出1.5 mm极限规格高强耐候SPA-H带钢。结合连铸拉速和结晶器液面控制，过程温度控制和设备精度控制，实现了1.5 mm热轧集装箱用SPA-H带钢的稳定轧制和批量供应，其板形和尺寸精度高，力学性能稳定，满足了用户的要求。