A novel fabrication procedure for producing high strength hydroxyapatite ceramic scaffolds with high porosity

Hydroxyapatite (HA) scaffolds were fabricated using the space holder method with a pressureless sintering process in a systematically developed manner at different fabrication stages to increase the strength of the scaffold at high porosity. Polyvinyl alcohol (PVA) and Polymethyl methacrylate (PMMA) were used as binders and space holder agents, respectively. The physical properties of the HA scaffolds were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), linear shrinkage test, and porosity measurements. The mechanical properties of the HA scaffolds were analyzed using compressive strength measurements. The results revealed that the HA scaffold met the expected quality requirements with a compressive strength of 2.2 MPa at a porosity of 65.6% with pore sizes distributed in the range of 126–385 μm. The shrinkage of the scaffold diameter occurred by 20.27%, this diameter shrinkage predominantly to the shrinkage of the HA scaffold caused by sintering. Besides, suspect that a higher PMMA concentration causes pore size shrinkage upon sintering. The formation of pore interconnections was evidenced by SEM observations and the ‘translucent light method’ developed in this study. The results of the scaffold phase test using XRD showed that the final scaffold consisted only of the HA phase, as the PVA and PMMA phases burned out during the sintering process.     

空间红外大口径折射式低温镜头设计与验证

针对目标探测类空间红外相机大范围成像、高灵敏度探测、高精度定位等应用需求,文中提出采用像方远心光路和低温光学技术结合的解决方案,设计了物方视场角8°×8°、入瞳口径265 mm、工作温度200 K的像方远心折射式光学系统。镜头最大口径280 mm,采用多级分散的弹性支撑设计,解决大口径低温透镜装框、透镜组件支撑和镜头整体安装各环节的热应力卸载问题。在保证高刚度和低漏热的情况下,使低温下透镜的热应力对镜头能量集中度的影响降低到可接受范围内。镜头完成装调及室温下像质确认后,进行了力学振动试验,并将其制冷到200 K水平测试像质,测试结果表明,镜头能量集中度达到轴上75%,边缘视场72%。     

高精度测微计在车轴测量机上的应用方案

介绍了高精度测微计用于车轴直径测量的基本结构、关键技术及其在车轴测量设备上的应用。     

ZY齿轮减速机重点零件工艺分析

输入偏心轴是ZY减速机中的重要零件,其加工精度直接影响减速机的整体性能。偏心距的加工较为困难,为保证它的加工精度,需设计专用的工艺装备。文中通过分析对比,选择了合理高效的工艺方案,满足了生产需要。     

钢材深加工是搞活钢铁企业的一条有效途径

钢铁企业开展钢材深加工,是搞活钢铁企业,提高经济效益不可忽视的一条途径。本文特对钢铁企业内部开展钢材深加工的意义及有利条件进行了概述,重点介绍了稀油密封多边形干式煤气柜、钢质干贷集装箱等钢材深加工产品的可行性,以及对如何搞好钢材深加工工作,提出了几点建议。     

低压下蒸发式稳定器结构对燃烧效率的影响

在低压条件,对蒸发式稳定器结构进行了优化,对不同方案开展了冷、热态流场三维数值研究,分析了稳定器后方冷态流场、燃油浓度场和热态流场、温度场特点。分析认为,在原蒸发式稳定器基础上,通过增大稳定器一次风进气量和U型蒸发管的长度,可以促进油气的掺混,增大回流区范围,同时采用断续进气,并将蒸发管出气孔与二次风夹角由90°减小到37.5°,可以进一步强化回流效果。最终得到的稳定器模型可以在0.08 MPa的压力条件下,将原稳定器燃烧效率由0.820提高到0.977。     

变压器磁铁固定座全自动级进式精密注塑模设计

根据变压器磁铁固定座结构特点,用辅助料带将金属端子串联在一起,再通过气缸和双推板脱模机构,使注塑模具能够像冲压模具那样可以进行全自动级进式进料和脱模。同时模具采用浮动式侧向抽芯机构,巧妙地解决了料带定位镶件和滑块相互干涉的问题。模具结构先进合理、快速高效,塑件尺寸精度得到了大幅提高。     

基于NaCl Beads制备的泡沫Al孔结构控制与表征

以淀粉、蒸馏水、NaCl粉末为原料,混合制成胶状盐团后70℃油浴加热,同时在机械搅拌切削的作用下得到球形度较高的NaCl小球,然后经高温烧结获得粒径分布主要在0.4-2.4mm,表面分布有少量微孔（孔径约10-20μm）且纯净度很高的NaCl小球。选用0.6-1.0mm的盐球作为造孔剂,利用Autotap震动将铝粉填入“盐床”缝隙,再经200MPa冷压成型后获得生坯,然后在蒸馏水中浸泡将盐球溶解去除,最后在460℃下烧结2h得到结构可控且工艺重现性很高的三维连通开孔性泡沫铝,其相对密度与孔隙率分别为0.217和78.3%。泡沫铝胞洞之间的连通窗口数量平均在4-6个,窗口尺寸约在120-200μm之间;压缩载荷-位移曲线表明泡沫铝在压缩变形过程中经历了弹性变形阶段-坪应力区-应力陡增阶段,表现出典型的泡沫金属压缩力学性能特点,其最大抗压强度与杨氏模量分别是2.42MPa和0.38GPa。