浅谈不同给液方式在铜电解车间的应用

不同给液方式对铜电解过程中有重要的影响,不同的循环方式会影响槽内温度分布、电解液成分及阳极泥沉降等,因此,根据铜电解生产不同情况的需要,分析对比了多种给液方式在贵冶电解车间的应用,总结了这几种给液方式的优缺点和适用条件。     

加压酸浸法从烟化炉冰铜中浸出铜和镍的试验研究

烟化炉冰铜主要是采用烟化炉处理低品位铜、锡、镍、锌等物料时产生的中间产物，主要含铜、镍、铁、硫等元素，从中浸出铜和镍具有重要价值。采用加压酸浸法从烟化炉冰铜中浸出铜和镍，试验研究了时间、温度、氧分压、液固比、粒度等因素对铜、镍、铁浸出率的影响。试验结果表明：烟化炉冰铜粒度球磨至小于75μm、温度433K、时间3h、氧分压为0.6MPa、液固比4/1mL/g、木质素磺酸钠用量为2‰的优化条件下，铜、镍、铁浸出率分别平均为98.18%、98.42%和26.46%。     

Influence of Reaction Conditions on the Settling Behavior of Liquid-Liquid Dispersions

The settling behavior of liquid-liquid dispersions at ambient temperature and pressure is well investigated. However, little is known about the settling behavior of those systems at high pressure and high temperature. In this work, a novel stainless steel settling cell is presented, enabling investigations on liquid-liquid settling behavior at high pressures up to 130 bar. The settling behavior of a promising CO₂ hydrogenation reaction system is investigated by sequentially determining influences of dissolved CO₂, side components, and temperature.     

多级堆排尾矿沉积固结特性实验研究

基于多级堆排尾矿浆体沉积柱一维沉积固结实验,近似模拟一级尾矿子坝内堆排尾矿的沉积固结过程,针对不同排水控制条件下实验尾矿的沉积固结结果进行比较分析,探讨多级堆排尾矿的沉积固结规律。结果表明:尾矿浆体的沉积固结过程明显分为沉积和固结二个阶段;超静孔隙水压力前期消散迅速,后期消散缓慢;排水实验每日平均渗透系数前期逐日下降,后期小幅上升;不同排水控制条件下,固结完成尾矿的干密度及相对密实度均随深度的增加而增大,二者在排水实验各深度处均大于不排水实验。     

高温烟气中煤焦气化行为

针对高温烟气中煤焦的气化行为，本文采用FactSage 6.1计算了煤焦在高温烟气下的高温反应特性，并利用热重分析仪分析了煤焦气化行为。通过沉降炉实验进一步研究了不同温度、气体配比、粒径条件下气体产物的动态析出特性，同时计算了评价指标α、β、LHV值。结果表明：随着温度的升高，气体产物H₂和CO的含量增加，β、α、LHV值增大，CH₄和CO₂的含量下降。在温度为1200℃时，β、α值分别由CO₂/CO比为10∶70时的10.80%、5.21%增加到CO₂/CO比为50∶30时的24.71%、41.06%。同时，随着CO₂/CO比值的增大，高温烟气对煤焦气化反应抑制减弱。通过对比反应温度和粒径对煤焦气化反应的影响，得出反应温度远大于粒径对煤焦气化反应的影响。通过实验验证了向高温烟气中喷吹煤焦制备高品质可燃气体方法的可行性。     

Effect of CaO on the liquid/spinel/matte/gas equilibria in the Si–Fe–O–Cu–S system at controlled P(SO2) 0.3 and 0.6 atm

Herein the phase equilibria in the Si–Fe–Ca–O–S–Cu system in equilibrium with matte at controlled P(SO₂) of 0.3 and 0.6 atm and fixed matte grade of 72 wt % Cu were experimentally investigated in the spinel primary phase field. The high-temperature equilibrations were realized in spinel substrate and the sample after quenching were characterized using Electron Probe Micro-analysis (EPMA). The effect of CaO on the liquidus temperature of slags was quantified with varying CaO content from 0 to 6 wt %. It was found that, the presence of CaO increased the liquidus temperature of slags and moreover, the increment effect got enhanced with increasing CaO content in the present range. The influence of P(SO₂) was further clarified and it was found that, the equilibrium SiO₂ content in the liquid phase, at the same temperature, remarkably increased with increasing P(SO₂). The present study will not only deepen the understanding of the equilibration in the present liquid/spinel/matte/gas system, but also provide useful guidance for the industrial operations.     

干扰床分选机分选粗煤泥的规律研究

介绍了干扰床分选机的工作原理,在比较了各种粗煤泥自由沉降速度计算方法的基础上,提出了适用于粗煤泥自由沉降速度的计算公式。筹建了试验室干扰床分选机试验系统,并对新汶矿业集团汶南煤矿不同粒度级别的粗煤泥进行了干扰床分选试验,探讨了干扰床分选机分选粗煤泥的一般规律。     

絮凝剂对金岭铁矿选矿厂尾矿絮凝沉降速度影响的研究

采用山东金岭铁矿选矿厂尾矿为矿样，选用试图加入18m尾矿大井中的几种絮凝剂分别做絮凝沉降试验，筛选出最佳絮凝剂。确定最佳絮凝剂后，研究了介质pH值、温度对尾矿絮凝沉降的影响。试验结果表明聚丙烯酰胺能够显著提高尾矿絮凝沉降速度，有利于在生产实践中推广使用。     

非均质流速度分布与水力坡度的研究

进行了非均质流固体粒子加速过程中的清水与固体粒子的速度变化、动量传递、相关质量计算等基本分析。提出了水平管道内固体粒子处于悬移运动状态下预计非均质流速度断面与水力坡度的新方法和模型。     

TCL—1418沉降过滤离心机大修技术标准的制定

制定TCL— 14 18沉降过滤离心机大修技术标准 ,规范其设备的大修标准 ,确保设备的大修质量。