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1.
A new aqueous slurry-based laminated object manufacturing process for porous ceramics is proposed: firstly, an organic mesh sheet is pre-paved as a pore-forming template before slurry layer scraping; secondly, the 2D pattern is built with laser outline cutting of the dried mesh–ceramic composite layer; finally, the pore structure is formed after degreasing and sintering. Alumina parts with porosities of 51.5 %, round hole diameters of 80 ± 5 μm were fabricated using 70 wt. % solid content slurry and 100 mesh nylon net. Using an organic mesh as the framework and template not only reduces the risk of damage of the green body but also ensures the regularity, uniformity and connectivity of the micron scaled pore network. The layer-by-layer drying method avoids the delamination phenomenon and improves the paving density. The new method can realize the flexible design of the pore structure by using various organic mesh templates. 相似文献
2.
A. Kathalingam S. Valanarasu Tansir Ahamad Saad M. Alshehri Hyun-Seok Kim 《Ceramics International》2021,47(6):7608-7616
Herein, we report the photosensing property of CdS thin films. CdS thin films were coated onto glass substrates via a spray pyrolysis method using different spray pressures. Prepared films were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and optical and photoluminescence spectroscopy. XRD analysis demonstrated the growth of crystalline CdS films with crystallite sizes varying from 26 to 29 nm depending on the pressure. The SEM and EDAX analyses revealed nearly-stoichiometric CdS films with smooth surfaces and slight variation in grain morphology due to pressure changes. Optical measurements showed a direct bandgap varying from 2.37 eV to 2.42 eV due to pressure changes. A photodetector was also fabricated using the grown CdS films; the fabricated photodetector exhibited good performance depending on the spray pressure. A spray pressure of 1.5 GPa resulted in high photoresponsivity and external quantum efficiency. 相似文献
3.
Mauro Zammarano John R. Shields Isaac Leventon Ickchan Kim Shonali Nazare Andre Thompson Rick D. Davis Artur Chernovsky Matthew Bundy 《火与材料》2021,45(1):114-126
Herein, we describe a reduced‐scale test (“Cube” test), measuring the fire performance of specimens including a fire barrier (FB) and a flammable core material, which acts as the main fuel load. The specimen is intended to reproduce a cross‐section of a composite product where heat/mass transfer occurs primarily in a direction perpendicular to the FB. The Cube test procedure and benefits are discussed in this work by adopting residential upholstery furniture as an exemplary study. One flexible polyurethane foam, one polypropylene cover fabric, and 10 commercially available FBs were selected. They were used to compare the fire performance of FBs, measured in terms of peak of heat release rate, in the ASTM E1474‐14 standard test and the newly developed Cube test. Edge effects severely affected the performance of FBs in the ASTM E1474‐14 standard test but not in the Cube test. Furthermore, appropriate test conditions were determined in the Cube test to measure the so‐called “wetting point,” that is, the time and value of heat release rate measured when flammable liquid products were first observed on the bottom of the specimen. The relevance of the “wetting point” in terms of full‐scale fire performance and failure mechanism of FBs is discussed. 相似文献
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磁声发射(MAE)是铁磁性材料磁化过程中产生的声发射信号,在构件应力检测和微观损伤检测中有着广泛的应用。针对MAE信号非稳态、复杂性、衰减性等特点,提出海鸥算法结合变分模态分解(SOA-VMD)的去噪方法,为克服海鸥算法求解过程中易陷入局部最优解问题,利用柯西变异算子产生随机迭代过程,使改进算法即柯西变异海欧算法(CVSOA)跳出早熟收敛。采用以幅值谱熵为适应度函数,优化VMD算法中分解模态个数K和二次惩戒因子α ![]()
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两个参数,将含噪声的MAE信号进行VMD分解重构。经仿真信号和实际检测信号分析表明,改进后的CVSOA-VMD算法全局寻优能力和去噪性能优于传统的SOA-VMD算法,降噪后的MAE信号特征值对于不同应力下均方根、偏斜度特征值的重复性更好,可靠性更高。 相似文献
7.
《International Journal of Hydrogen Energy》2022,47(59):25007-25021
Fluid sloshing usually causes serious safety issues on the dynamic stability and propellant thermal management during the powered-flight phase of launch vehicle. With the wide using of cryogenic propellants, the coupled thermo-mechanical performance during fluid sloshing becomes more prominent. In the present study, one numerical model is established to simulate fluid sloshing by using the VOF method coupled with the mesh motion treatment. The phase change occurring within the tank is considered. Both the experimental validation and mesh sensitivity analysis are made. It shows that present numerical model is acceptable. Based on the developed numerical model, the effect of different super gravity accelerations on fluid sloshing hydrodynamic characteristic is numerically researched. The fluid pressure variation, the sloshing force and sloshing moment, the interface dynamic response and the interface shape variation are investigated, respectively. It shows that the gravity acceleration has caused obvious influences on fluid sloshing characteristic. When the gravity acceleration is higher than 4g0, fluid sloshing becomes more obvious and must be paid enough attention. With some valuable conclusions obtained, the present work is of great significance for in-depth understanding of fluid sloshing mechanism. 相似文献
8.
为了准确地从复杂干扰背景下检测出真实弱小目标,本文引入视觉显著性,设计了基于快速光谱尺度空间与动态管道滤波的红外目标检测算法。基于真实目标与背景内容之间的整体差异,引入快速光谱尺度空间与阈值分割技术,设计视觉显著性机制,对红外图像完成处理,输出全局显著性映射,以高效过滤干扰背景内容。考虑目标与背景的局部特征差异,构建自适应局部对比度增强机制,对粗检测结果实施处理,获取对应的局部显著性映射,改善视觉显著性区域内目标的对比度。引入高斯差分理论,通过估算每一帧红外图像中的目标像素直径,形成动态管道滤波,充分消除虚警,准确识别出弱小目标。多组实验数据显示:较已有的红外目标检测技术而言,在各种不同的复杂背景干扰下,所提算法呈现出更好的检测能力,拥有更理想的接收机工作特性R O C ![]()
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曲线。 相似文献
9.
Lingfeng Zhou Zhipeng Zeng Michael P. Brady Donovan N. Leonard Harry M. Meyer Yukinori Yamamoto Wenyuan Li Greg Collins Xingbo Liu 《International Journal of Hydrogen Energy》2021,46(41):21619-21633
The chromium (Cr) evaporation behavior of several different types of iron (Fe)-based AFA alloys and benchmark Cr2O3-forming Fe-based 310 and Ni-based 625 alloys was investigated for 500 h exposures at 800 °C to 900 °C in air with 10% H2O. The Cr evaporation rates from alumina-forming austenitic (AFA) alloys were ~5 to 35 times lower than that of the Cr2O3-forming alloys depending on alloy and temperature. The Cr evaporation behavior was correlated with extensive characterization of the chemistry and microstructure of the oxide scales, which also revealed a degree of quartz tube Si contamination during the test. Long-term oxidation kinetics were also assessed at 800 to 1000 °C for up to 10,000 h in air with 10% H2O to provide further guidance for SOFC BOP component alloy selection. 相似文献
10.
Pin Liu Yujing Zhang Yiwei Zhu Baoyan Fan Wenru Li Haibo Zhang Shenglin Jiang 《Journal of the American Ceramic Society》2019,102(4):1912-1920
Energy storage capacitors with high recoverable energy density and efficiency are greatly desired in pulse power system. In this study, the energy density and efficiency were enhanced in Mn-modified (Pb0.93Ba0.04La0.02)(Zr0.65Sn0.3Ti0.05)O3 antiferroelectric ceramics via a conventional solid-state reaction process. The improvement was attributed to the change in the antiferroelectric-to-ferroelectric phase transition electric field (EF) and the ferroelectric-to-antiferroelectric phase transition electric field (EA) with a small Mn addition. Mn ions as acceptors, which gave rise to the structure variation, significantly influenced the microstructures, dielectric properties and energy storage performance of the antiferroelectric ceramics. A maximum recoverable energy density of 2.64 J/cm3 with an efficiency of 73% was achieved when x = 0.005, which was 40% higher than that (1.84 J/cm3, 68%) of the pure ceramic counterparts. The results demonstrate that the acceptor modification is an effective way to improve the energy storage density and efficiency of antiferroelectric ceramics by inducing a structure variation and the (Pb0.93Ba0.04La0.02)(Zr0.65Sn0.3Ti0.05)O3-xMn2O3 antiferroelectric ceramics are a promising energy storage material with high-power density. 相似文献