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1.
Crystallization of calcium carbonate (CC) in aqueous solutions by gas‐liquid diffusion procedure was investigated systematically in the presence of poly(4‐sulfonic acid diphenylamine)‐block‐poly(ethylene glycol) (PSDA‐b‐PEG), wherein the PSDA block is a polymeric zwitterion. PSDA‐b‐PEG was synthesized with the reaction of tosylated PEG and amine‐functionalized PSDA and was characterized by nuclear magnetic resonance. The parameters such as, block copolymer concentration, crystallization time and initial pH were considered as indicators of block copolymer's capability in controlling the morphology of CC particles. The particles were characterized by Fourier transform infrared, scanning electron microscopy, and X‐ray diffraction. The results suggest that PSDA‐b‐PEG is a suitable template to control the growth mechanism of CC to produce meso‐sized particles with different morphologies. POLYM. ENG. SCI., 59:96–102, 2019. © 2018 Society of Plastics Engineers  相似文献   
2.
The use of graphite modified polymer films has been investigated, on stainless steel. Polythiophene and polypyrrole films have been synthesized electrochemically on stainless steel, and then very thin graphite layers were realized on polymer films. Since the graphite layer is not applicable as a top coat, polymeric top films were also electrosynthesized on graphite layers. Following this procedure, polypyrrole-graphite-polypyrrole and polythiophene-graphite-polythiophene coatings have been obtained on stainless steel. The corrosion behaviours of coated samples have been investigated in 0.1 M H2SO4 solution, by means of electrochemical impedance spectroscopy (EIS) and anodic polarization curves. The intercalation of graphite layer altered the performance and properties of coatings significantly. Especially, polypyrrole coating system was found to exhibit almost an excellent coating behaviour that hindered the attack of corrosive environment within 96 h exposure time. The EIS results of polypyrrole coating system were indicating to almost a perfect capacitive behaviour that the response was reflecting capacitive behaviour in a wide frequency region. This property was also examined with successive cyclic voltammograms in a potential range between 0.10 and 0.40 V (vs. Ag/AgCl). The charge densities involved in oxidation and reduction regions were determined for successive cycles and it was shown that coated sample was able to exhibit charge-discharge (i.e. oxidation and reduction) behaviour successfully, without any degradation.  相似文献   
3.
Continuously reducing transistor sizes and aggressive low power operating modes employed by modern architectures tend to increase transient error rates. Concurrently, multicore machines are dominating the architectural spectrum today in various application domains. These two trends require a fresh look at resiliency of multithreaded applications against transient errors from a software perspective. In this paper, we propose and evaluate a new metric called the Thread Vulnerability Factor (TVFTVF). A distinguishing characteristic of TVFTVF is that its calculation for a given thread (which is typically one of the threads of a multithreaded application) does not depend on its code alone, but also on the codes of the threads that share resources and data with that thread. As a result, we decompose TVFTVF of a thread into two complementary parts: local and remote. While the former captures the TVFTVF induced by the code of the target thread, the latter represents the vulnerability impact of the threads that interact with the target thread. We quantify the local and remote TVFTVF values for three architectural components (register file, ALUs, and caches) using a set of ten multithreaded applications from the Parsec and Splash-2 benchmark suites. Our experimental evaluation shows that TVFTVF values tend to increase as the number of cores increases, which means the system becomes more vulnerable as the core count rises. We further discuss how TVFTVF metric can be employed to explore performance–reliability tradeoffs in multicores. Reliability-based analysis of compiler optimizations and redundancy-based fault tolerance are also mentioned as potential usages of our TVFTVF metric.  相似文献   
4.
We design and investigate the performance of fuzzy logic-controlled (FLC) active suspensions on a nonlinear vehicle model with four degrees of freedom, without causing any degeneration in suspension working limits. Force actuators were mounted parallel to the suspensions. In this new approach, linear combinations of the vertical velocities of the suspension ends and accelerations of the points of connection of the suspension to the body have been used as input variables. The study clearly demonstrates the effectiveness of the fuzzy logic controller for active suspension systems. Suspension working space degeneration is the most important problem in various applications. Decreasing the amplitudes of vehicle body vibrations improves ride comfort. Body bounce and pitch motion of the vehicle are presented both in time domain when travelling over a ramp-step road profile and in frequency domain. The results are compared with those of uncontrolled systems. At the end of this study, the performance and the advantage of the suggested approach and the improvement in ride comfort are discussed.  相似文献   
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6.
The effect of brewing process on 5-hydroxymethylfurfural, 2-furylmethylketone, and 2-furoic acid levels of traditionally prepared and instant Turkish coffee samples containing different amounts of table sugar (0, 2, 4, or 8 g in 20 mL of coffee) were analyzed by high pressure liquid chromatography with diode array detector. The highest change at the levels of furfurals was observed in sample of traditional and instant Turkish coffee named T4 and S4 both of containing 8 g of sugar, respectively. The results showed that 5-hydroxymethylfurfural, 2-furylmethylketone, and 2-furoic acid concentrations in both traditionally prepared and instant Turkish coffee samples increased with increasing sugar concentration. The brewing method and sugar concentration had a significant effect on furfural contents of Turkish coffee (p < 0.05). Daily intakes of furfurals for Turkish population were calculated as 8.14–13.54 and 9.36–10.25 µg kg?1 body weight for traditionally prepared and instant Turkish coffee samples, respectively, and daily intakes of furfurals were lower than the acceptable daily intake value of 0.5 mg kg?1 body weight.  相似文献   
7.
We have produced the (BiPb)2V x Sr2Ca3Cu4−y Ti y O12+δ compounds by a melt-quenching method. For two different sintering times (185 and 192 hours), the effects of vanadium adding and Ti doping on the structure have been investigated by electrical resistance, scanning electron micrographs (SEM), XRD patterns and magnetic hysteresis loop measurements. It has been found that the high-T c superconducting phase, (2223), is formed in the samples annealed at 845 C for 185 and 192 h, with concentration x=0.2 and y=0.05. However, with increasing Ti doping the (2223) phase gradually transforms into the (2212) phase. The hysteresis loop areas decrease with increasing Ti concentration and sintering time. Our data have indicated that the critical current, J c , decreases with increasing magnetic field.  相似文献   
8.
For stability assessments as well as for support design, it is important to understand the factors leading to detrimental stress changes. Stress changes not only influence the demand on the rock support, they also change the support capacity of frictional support components such as plain cablebolts. Stress and stress changes are commonly predicted by numerical models but it is rarely possible to verify these predictions. This study presents a practical example illustrating the usefulness of stress change measurements in providing an accurate picture of the mining-induced stress changes and their value for numerical model calibration. Stress changes, associated with mining of the 565#6 stope at Winston Lake Mine, were measured by four CSIRO HI stress cells, two in the hangingwall and two in the back of a sill drift. In order to obtain the full stress history of the hangingwall, stresses at the installation time were calculated by use of a three-dimensional boundary element program — MAP3D. Two types of rockmass failure were observed at this mine: hangingwall delamination and collapse leading to ore dilution, and wedge-like failures in the backs of sill drifts. All stress cells were located such that they were affected by these failure mechanisms. Using measured and predicted stress paths, this study explains the nature of these two failure modes, as experienced at Winston Lake Mine. Excellent correspondence between measured and predicted stresses is achieved for both the hangingwall and the back of the sill drifts. Modelled stress rotations in the hangingwall follow closely the stress rotations determined in the field, except at the end of the monitoring campaign when the stress cells were affected by inelastic straining of the host rock. These measurements assist in understanding the failure processes and in defining the limitations of the adopted numerical models.  相似文献   
9.
The effect of soy protein concentrate (0, 1.5, 3, and 4.5%) on the physical, chemical, and sensory properties of strawberry flavored (0, 0.01 and 0.02%) ice cream samples was examined. All samples were analyzed for pH, titratable acidity, total solids, nitrogen, fat, ash, overrun, viscosity, meltdown, Hunter L-, a-, b- values, flavor, body and texture, and appearance. Substituting soy protein concentrate (SPC) in ice cream formula for non-fat dry milk (NFDM) positively influenced the nitrogen content, viscosity values, and melting and appearance properties of the ice cream samples while overrun values and flavor scores were negatively affected. SPC could be incorporated into the ice cream formula in the range of 1.5–3% devoid of significantly diminishing the physical, chemical, and sensory properties.  相似文献   
10.
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