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排序方式: 共有122条查询结果,搜索用时 234 毫秒
1.
Alan Royce Jiwaji Suryawanshi Udayan Shah Krishna Vishnupad 《Drug development and industrial pharmacy》1996,22(9):917-924
A melt granulation process has been investigated (1, 2) which efficiently agglomerates pharmaceutical powders for use in both immediate- and sustained-release solid dosage forms. The process utilizes materials that are effective as granulating fluids when they are in the molten state. Cooling of the agglomerated powders and the resultant solidification of the molten materials completes the granulation process. Both the molten agglomeration and cooling solidification were accomplished in a high shear Collette Gral mixer equipped with a jacketed bowl. Hence, the melt granulation process replaces the conventional granulation and drying operations which use water or alcohol solutions. The melt granulation process has been investigated using immediate- and sustained-release TAVIST® (clemastine fumarate USP) tablet formulations. The TAVIST granulations have been characterized by power consumption monitoring, measurement of the granulation particle size distribution, bulk and tapped density determinations, and loss-on-drying measurements. Scale-up of the melt granulation process for the sustained release TAVIST tablet formulation was judged successful based on a comparison of the hardness, friability, weight uniformity during compression, disintegration time, and dissolution rate data obtained at different manufacturing scales. 相似文献
2.
Manu Kumar Sang-Min Chung Ganuskh Enkhtaivan Rahul V. Patel Han-Seung Shin Bhupendra M. Mistry 《International journal of molecular sciences》2021,22(5)
In this study, we have introduced newly synthesized substituted benzothiazole based berberine derivatives that have been analyzed for their in vitro and in silico biological properties. The activity towards various kinds of influenza virus strains by employing the cytopathic effect (CPE) and sulforhodamine B (SRB) assay. Several berberine–benzothiazole derivatives (BBDs), such as BBD1, BBD3, BBD4, BBD5, BBD7, and BBD11, demonstrated interesting anti-influenza virus activity on influenza A viruses (A/PR/8/34, A/Vic/3/75) and influenza B viral (B/Lee/40, and B/Maryland/1/59) strain, respectively. Furthermore, by testing neuraminidase activity (NA) with the neuraminidase assay kit, it was identified that BBD7 has potent neuraminidase activity. The molecular docking analysis further suggests that the BBD1–BBD14 compounds’ antiviral activity may be because of interaction with residues of NA, and the same as in oseltamivir. 相似文献
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Bhupendra Singh Nitika Devi Lakshya Mathur Rajesh K. Singh Aman Bhardwaj Sun-Ju Song Dirk Henkensmeier 《Ceramics International》2018,44(6):6170-6175
In the present work, we report a method of fabrication of dense 10 mol% Mg2+-doped cerium pyrophosphate-phosphate (Ce0.9Mg0.1P2O7-PmOn; CMP-P) composites by microwave heat-treatment of the preformed Ce0.9Mg0.1P2O7 substrates in the presence of phosphoric acid. The composite was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and electrochemical impedance spectroscopy (EIS). The microwave heating at 375 °C for 5 min resulted in the formation of dense CMP-P composites which retained most of the pyrophosphate phase. The electrical conductivity was extracted from the EIS data and for the CMP-P composite prepared by H3PO4 loading for 10 h and microwave heat-treatment for 5 min it was found to be >10?2 S m?1 in 100–250 °C range with a maximum of 0.062 S cm?1 at 190 °C, which was significant for its application as electrolyte in intermediate temperature fuel cells. 相似文献
5.
Drug‐loaded polyurethane/clay nanocomposite nanofibers for topical drug‐delivery application 下载免费PDF全文
In this study, polyurethane/nanoclay nanocomposite nanofibrous webs were prepared by electrospinning. An antiseptic drug, chlorhexidine acetate (CA), was loaded onto montmorillonite clay and was then incorporated into polyurethane nanofibers. For comparison, the CA drug was loaded directly into the polyurethane solution dope used to electrospin the nanofibers. The emphasis was on investigating the effect of the drug loading into the nanoclay vis‐à‐vis direct drug loading on the drug‐release behavior of nanofibrous webs. The nanofibrous webs were also evaluated for other properties, such as moisture vapor transmission, porosity determination, contact angle measurement, and antibacterial activity, which are important for topical drug‐delivery application. © 2013 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2014 , 131, 40230. 相似文献
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The present study aims at studying ageing characteristics of conventional bitumen, polymer modified bitumen (PMB) and warm mix asphalt (WMA) by using FTIR. Results of obtained FTIR spectrum were quantified by calculating different indices and finally based on these indices ageing index of the binders for short- and long-term ageing were calculated. Results showed ageing increased amount of complex and high molecular weight components of the binders. PMB was found to have greater ageing resistance than conventional asphalt binders. In case of WMA, results found to be inconclusive, requiring further investigation. 相似文献
9.
Lalchand A Patil Dinesh N Suryawanshi Idris G Pathan Dhanashri G Patil 《Bulletin of Materials Science》2014,37(3):425-432
Nanostructured pure and Pt-doped TiO2 thin films were prepared by chemical spray pyrolysis technique. Aqueous solution of TiCl3·6H2O (0·01 M) was chosen as the starting solution for the preparation of pure TiO2 thin film. Aqueous solutions of PtCl6·6H2O (0·01 M) and TiCl3·6H2O (0·01 M) were mixed in volume % of 1 : 99, 2·5 : 97·5 and 5 : 95 respectively to obtain Pt-doped TiO2 thin films. The solutions were sprayed onto quartz substrate heated at 350 °C temperature to obtain the films. These thin films were fired for one hour at 550 °C. The sensing performance of these films was tested for various gases such as LPG, H2, CO2, ethanol, NH3 and Cl2 (1000 ppm). The Pt-doped TiO2 (1 : 99) was observed to be most sensitive (572) to H2 at 400 °C with high selectivity against other gases. Its response time was short (10 s) and recovery was also fast (14 s). To understand the reasons behind the gas-sensing performance of the films, their structural and microstructral properties were studied using X-ray diffraction and electron microscopy (FE–SEM and TEM), respectively. Thicknesses of all these samples were determined using Surface Profiler. The results are interpreted. 相似文献
10.
Suryawanshi H.M. Kulwal A.K. Chaudhari M.A. Borghate V.B. 《Industrial Electronics, IEEE Transactions on》2008,55(4):1637-1646
This paper presents a novel approach to improve the power factor (PF) and reduce the harmonics generated by an adjustable-speed drive (ASD). A high-frequency (HF) current injection technique is used to improve the PF and harmonic performance. The HF current at the same switching frequency (33 kHz) is injected into the input of a front-end rectifier from the output of an HF inverter. The main feature of the circuit is that it does not require any additional active devices for current injection. The inverter driving the induction motor is operated using a sinusoidal pulsewidth-modulation technique. The circuit simulation and experimental prototype results are presented for 67-hp (50 kW) and 3-hp three-phase induction motors, respectively. 相似文献