Novel Flexible Electrochemical Microreactor and its Validation by Three Model Electrosyntheses

A novel flexible electrochemical microreactor has been developed. Flexibility is reached by a modular design, suitability for a broad process parameter range including high pressure operation, and accessibility of production scale. Selected reactor aspects have been validated by applying the reactor to three different electrosyntheses: synthesis of tailor-made mixtures of paraffins by Kolbe electrolysis, cation flow method, and synthesis of peroxodicarbonate. High conversion rates, yields, selectivities, and Faraday efficiency levels have been observed, showing precise process control.     

聚能射流侵彻混凝土靶板的数值模拟研究

在基于有限元法中心差分包软件LS-DYNA-970的平台上对圆锥罩型聚能射流侵彻素混凝土试样进行了3-D数值仿真,揭示了金属射流的形成过程和侵彻过程机理。研究表明：装药结构在爆炸荷载作用下能形成头部速度高、弹身长径比大、整体质量分布合理的高速杆式侵彻体。在分析混凝土受力失效过程的同时,获得了金属射流在不同侵彻深度下,混凝土开孔孔径大小的数值结果。计算结果与文献中的实验数据吻合较好。     

某银多金属矿工艺矿物学及选矿试验结果

本论文针对某银多金属矿矿物组成种类繁多、矿石性质复杂、选矿难度大、选矿指标不理想等问题,开展了详细工艺矿物学研究,分析了原矿矿物组成、有价组分种类、矿石结构构造及赋存状态,并在此基础上报道了选矿试验研究结果。研究结果表明,该矿主要有价金属为铜铅锌银,主要金属矿物有黄铜矿、方铅矿、闪锌矿及黄铁矿,银金属主要赋存于黄铜矿与方铅矿中,小型闭路试验成功实现该银铜铅锌多金属矿浮选分离富集,并获得了理想的选矿指标。     

SEM and EDS investigation of a pyrolytic carbon covered C/C composite maxillofacial implant retrieved from the human body after 8 years

The long term effect of the human body on a pyrolytic carbon covered C/C composite maxillofacial implant (CarBulat^Tm) was investigated by comparing the structure, the surface morphology and composition of an implant retrieved after 8 years to a sterilized, but not implanted one. Although the thickness of the carbon fibres constituting the implants did not change during the 8 year period, the surface of the implant retrieved was covered with a thin surface layer not present on the unimplanted implant. The composition of this layer is identical to the composition of the underlying carbon fibres. Calcium can only be detected on the surface as a trace element implying that the new layer is not formed by bone tissue. Residual soft tissue penetrating the bulk material between the carbon fibre bunches was found on the retrieved implant indicating the importance of the surface morphology in tissue growth and adhering to implants.     

Background and foreground interaction: Influence of complementary colors on the search task

Labels are indispensable visual (communication) elements that completely deliver the geospatial message of maps. The objective of this study is to investigate the impact of complementary colors between the map's background and text on the readability of cartographic texts and thus on the efficiency of the map user's search task. This is compared with the use of the “traditional” black labels on the corresponding colored backgrounds. Furthermore, a number of user characteristics, such as gender and expertise, are taken into account as well. The users' eye movements were registered to study their attentive behavior during the visual search task. In addition to the complement of the color's hue, the analyses were based on the difference in luminance, which could also affect the labels' readability. The difference between the black and colored label design was significantly different versus the eye‐tracking metrics. A correlation was found between the color difference and reaction time measurement and between the luminance difference and fixation duration. © 2014 Wiley Periodicals, Inc. Col Res Appl, 40, 437–445, 2015     

A Lagrangean heuristic for a two-echelon storage capacitated lot-sizing problem

In this paper, we study a structure issued from a real case. Raw materials (RMs) are sent by suppliers to a distribution center (DC) and then transported to a unique plant where they can be stored. The inventory capacity is limited in the plant as well as in the DC. The transportation capacity between the DC and the plant is also limited. The objective is to determine the flows between suppliers and the DC, and from the DC to the plant in order to satisfy the demand during the planning horizon while minimizing the global cost. A mixed-integer programming (MIP) formulation is presented and a Lagrangean relaxation solution procedure is proposed. Computational experiments are carried out.     

阿瓦提凹陷沙井子断裂带特征及控油气作用

沙井子断裂为塔里木盆地阿瓦提凹陷北部的控凹边界断裂,呈北东—南西向展布,倾向北西,长约180 km.通过对该断裂带的平面分布和剖面特征、断裂发育演化及其对油气聚集成藏控制作用等的分析,指出沙井子断裂带具有明显的分段特征,可分为西、中、东3段。沙井子断裂带自海西运动早期开始发育,主断裂持续活动至今,控制了阿瓦提凹陷北部地区的构造格架和沉积作用、圈闭形成和油气运移,对油气的聚集成藏起到重要的控制作用。     

铈(Ⅲ)-组氨酸-邻菲啰啉三元配合物的合成及其电化学活性

在乙醇水溶液介质中,60℃水浴加热的条件下,合成了标题化合物.经络合滴定、摩尔电导、元素分析、红外光谱、紫外光谱、热重-差热和循环伏安等测试对配合物进行了表征,确定配合物的化学组成为:[Ce(Ⅲ)(His)3phen]Cl3·3H2O.重点通过循环伏安测定了配合物在玻碳工作电极上的电化学行为,在HAc-NaAc缓冲溶液...     

脉冲电沉积法制备Al基Pb—WC—Ce02复合惰性阳极

为了制备性能优良的Al基Pb—WC—CeO：惰性阳极材料,考察了WC、CeO：颗粒浓度对阴极极化的影响,正向脉冲参数、温度和搅拌对沉积速率以及复合镀层表面形貌的影响,并研究了其在锌电解液中的耐蚀性能,确定了脉冲电沉积制备Al基Pb-WC-C02复合镀层的最佳工艺条件：基础镀铅液中添加40g／LWC（粒径1斗m）,30g...